GB1099061A - m-dioxane derivatives, methyl isogeraniol and its esters - Google Patents

m-dioxane derivatives, methyl isogeraniol and its esters

Info

Publication number
GB1099061A
GB1099061A GB50033/65A GB5003365A GB1099061A GB 1099061 A GB1099061 A GB 1099061A GB 50033/65 A GB50033/65 A GB 50033/65A GB 5003365 A GB5003365 A GB 5003365A GB 1099061 A GB1099061 A GB 1099061A
Authority
GB
United Kingdom
Prior art keywords
methyl
isogeroniol
esters
isogeraniol
dioxane derivatives
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB50033/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
International Flavors and Fragrances Inc
Original Assignee
International Flavors and Fragrances Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by International Flavors and Fragrances Inc filed Critical International Flavors and Fragrances Inc
Publication of GB1099061A publication Critical patent/GB1099061A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0069—Heterocyclic compounds
    • C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
    • C11B9/008—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing six atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D319/00—Heterocyclic compounds containing six-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D319/04—1,3-Dioxanes; Hydrogenated 1,3-dioxanes
    • C07D319/06—1,3-Dioxanes; Hydrogenated 1,3-dioxanes not condensed with other rings
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0007—Aliphatic compounds
    • C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
    • C11B9/0019—Aliphatic compounds containing oxygen as the only heteroatom carbocylic acids; Salts or esters thereof

Abstract

The invention comprises the compound of the formula <FORM:1099061/C2/1> This compound, methyl isogeroniol and/or C1- 6 alkanoic esters of methyl isogeroniol are produced by reacting myrcene sulphone with formaldehyde or a polymer of formaldehyde, if desired in the presence of a C1- 6 alkanoic acid or anhydride thereof, at a temperature below 90 DEG C. and then pyrolyzing the product formed. When the acid or its anhydride is present the dioxane is not formed but an ester of methyl isogeroniol is formed and may, if desired, be saponified to give methyl isogeroniol. Any odour of sulphur may be removed from the methyl isogeroniol product by treatment with Raney nickel.
GB50033/65A 1964-12-18 1965-11-24 m-dioxane derivatives, methyl isogeraniol and its esters Expired GB1099061A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US41957964A 1964-12-18 1964-12-18

Publications (1)

Publication Number Publication Date
GB1099061A true GB1099061A (en) 1968-01-10

Family

ID=23662858

Family Applications (1)

Application Number Title Priority Date Filing Date
GB50033/65A Expired GB1099061A (en) 1964-12-18 1965-11-24 m-dioxane derivatives, methyl isogeraniol and its esters

Country Status (6)

Country Link
BE (1) BE673628A (en)
CH (1) CH447141A (en)
DE (1) DE1271707B (en)
FR (1) FR1466583A (en)
GB (1) GB1099061A (en)
NL (1) NL6516080A (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0018833B1 (en) * 1979-05-04 1983-10-19 BUSH BOAKE ALLEN Limited Compounded perfumery composition

Also Published As

Publication number Publication date
BE673628A (en) 1966-06-13
DE1271707B (en) 1968-07-04
FR1466583A (en) 1967-01-20
NL6516080A (en) 1966-06-20
CH447141A (en) 1967-11-30

Similar Documents

Publication Publication Date Title
GB799270A (en) Production of intermediates for the synthesis of reserpine and allied compounds
GB1099061A (en) m-dioxane derivatives, methyl isogeraniol and its esters
GB1065173A (en) Descarbamoylbluensidine and its derivatives
ES449817A1 (en) Substituted 2-phenylimino-thiazolines a process for their preparation and their use as ectoparasiticides
CH413810A (en) Process for the production of metal soaps for epoxidized fatty acids
GB939941A (en) Improvements in or relating to the manufacture of derivatives of 5-nitrofuran
GB827638A (en) Preparation of citraconic anhydride
ES251886A1 (en) New series of carboxylic acid esters of 5-nitro-2-furyl alkylidene hydroxyalkyl semicbazones
GB935610A (en) 3ªá-amino-pregnane compounds
FR1174285A (en) Process for the production of sulfonamides of the o-dialkyl-amino-thionophosphoric ester of p-aminophenols
GB723948A (en) Improvements in or relating to thiazole derivatives
FR1432428A (en) Aminodiol, its production process, and the fatty acid salt of this aminodiol
ES416936A1 (en) Procedure for preparing beta- (3,4-dialcanyloxyphenyl) -l-alamines esters. (Machine-translation by Google Translate, not legally binding)
GB1019569A (en) Esters of 1ª‡,2ª‡-methylene-í¸-androstene-3,17ª‰-diol and a process for their manufacture
GB880421A (en) Improvements in or relating to the production of esters of bis-(carboxymethylthio)-methane
GB1070762A (en) Enol esters and a process for their manufacture
GB530269A (en) Improvements in or relating to the manufacture of the nitriles of organic carboxylicacids
GB606193A (en) Improvements in or relating to thiophene compounds and processes of preparing the same
GB647173A (en) A process for the manufacture of a benzilic acid derivative
GB882844A (en) Glucuronic acid derivatives useful as intermediates in the production of antibacterials, and the production of said derivatives
GB1004470A (en) Improvements in or relating to compounds of the androstane series
GB1006134A (en) The pyrrolidide of trimethoxy benzoylamino acetic acid
GB667009A (en) Improvements in gentisic acid compounds of substituted pyrazolones and process for the manufacture of same
GB750873A (en) Improvements in or relating to the preparation of progesterone
GB569524A (en) Nitriles and method of making the same