GB1061700A - The preparation of ?-caprolactone - Google Patents
The preparation of ?-caprolactoneInfo
- Publication number
- GB1061700A GB1061700A GB445766A GB445766A GB1061700A GB 1061700 A GB1061700 A GB 1061700A GB 445766 A GB445766 A GB 445766A GB 445766 A GB445766 A GB 445766A GB 1061700 A GB1061700 A GB 1061700A
- Authority
- GB
- United Kingdom
- Prior art keywords
- iron
- reaction mixture
- caprolactone
- ferric
- hydrocarbon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 abstract 6
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 abstract 4
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 abstract 4
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 abstract 4
- 150000002505 iron Chemical class 0.000 abstract 4
- 239000011541 reaction mixture Substances 0.000 abstract 4
- 239000005711 Benzoic acid Substances 0.000 abstract 3
- 235000010233 benzoic acid Nutrition 0.000 abstract 3
- ITAUHKJMPRCVIH-UHFFFAOYSA-K iron(3+);tribenzoate Chemical compound [Fe+3].[O-]C(=O)C1=CC=CC=C1.[O-]C(=O)C1=CC=CC=C1.[O-]C(=O)C1=CC=CC=C1 ITAUHKJMPRCVIH-UHFFFAOYSA-K 0.000 abstract 3
- PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical compound O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 abstract 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 abstract 2
- 239000004215 Carbon black (E152) Substances 0.000 abstract 2
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 abstract 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 abstract 2
- 229910001882 dioxygen Inorganic materials 0.000 abstract 2
- 150000002148 esters Chemical class 0.000 abstract 2
- 239000007789 gas Substances 0.000 abstract 2
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 abstract 2
- 150000002506 iron compounds Chemical class 0.000 abstract 2
- 159000000014 iron salts Chemical class 0.000 abstract 2
- HOIQWTMREPWSJY-GNOQXXQHSA-K iron(3+);(z)-octadec-9-enoate Chemical compound [Fe+3].CCCCCCCC\C=C/CCCCCCCC([O-])=O.CCCCCCCC\C=C/CCCCCCCC([O-])=O.CCCCCCCC\C=C/CCCCCCCC([O-])=O HOIQWTMREPWSJY-GNOQXXQHSA-K 0.000 abstract 2
- 239000007791 liquid phase Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 125000005609 naphthenate group Chemical group 0.000 abstract 2
- 230000001590 oxidative effect Effects 0.000 abstract 2
- QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- 235000011037 adipic acid Nutrition 0.000 abstract 1
- 239000001361 adipic acid Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D315/00—Heterocyclic compounds containing rings having one oxygen atom as the only ring hetero atom according to more than one of groups C07D303/00 - C07D313/00
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
- C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Pyrane Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL6501333A NL6501333A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1965-02-03 | 1965-02-03 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1061700A true GB1061700A (en) | 1967-03-15 |
Family
ID=19792262
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB445766A Expired GB1061700A (en) | 1965-02-03 | 1966-02-01 | The preparation of ?-caprolactone |
Country Status (8)
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0548774A1 (en) * | 1991-12-25 | 1993-06-30 | Sumitomo Chemical Company, Limited | Process for producing a lactone or an ester |
| RU2326861C1 (ru) * | 2007-01-10 | 2008-06-20 | Курский государственный технический университет (КГТУ) | Способ получения бензоата железа (iii) |
| RU2398758C1 (ru) * | 2008-12-22 | 2010-09-10 | Государственное образовательное учреждение высшего профессионального образования Курский государственный технический университет (КурскГТУ) | Способ получения ацетата свинца (ii) |
| RU2412153C2 (ru) * | 2007-02-13 | 2011-02-20 | Государственное образовательное учреждение высшего профессионального образования "Юго-Западный государственный университет" | Способ получения бензоата железа (iii) |
-
1965
- 1965-02-03 NL NL6501333A patent/NL6501333A/xx unknown
-
1966
- 1966-01-30 IL IL2506966A patent/IL25069A/xx unknown
- 1966-02-01 CH CH135266A patent/CH462795A/de unknown
- 1966-02-01 BE BE675887D patent/BE675887A/xx unknown
- 1966-02-01 GB GB445766A patent/GB1061700A/en not_active Expired
- 1966-02-01 AT AT89266A patent/AT260890B/de active
- 1966-02-02 DE DE19661593529 patent/DE1593529A1/de active Pending
- 1966-02-02 ES ES0322528A patent/ES322528A1/es not_active Expired
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0548774A1 (en) * | 1991-12-25 | 1993-06-30 | Sumitomo Chemical Company, Limited | Process for producing a lactone or an ester |
| US5405974A (en) * | 1991-12-25 | 1995-04-11 | Sumitomo Chemical Company, Limited | Process for producing a lactone or an ester |
| RU2326861C1 (ru) * | 2007-01-10 | 2008-06-20 | Курский государственный технический университет (КГТУ) | Способ получения бензоата железа (iii) |
| RU2412153C2 (ru) * | 2007-02-13 | 2011-02-20 | Государственное образовательное учреждение высшего профессионального образования "Юго-Западный государственный университет" | Способ получения бензоата железа (iii) |
| RU2398758C1 (ru) * | 2008-12-22 | 2010-09-10 | Государственное образовательное учреждение высшего профессионального образования Курский государственный технический университет (КурскГТУ) | Способ получения ацетата свинца (ii) |
Also Published As
| Publication number | Publication date |
|---|---|
| BE675887A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1966-08-01 |
| CH462795A (de) | 1968-09-30 |
| DE1593529A1 (de) | 1970-10-22 |
| IL25069A (en) | 1969-05-28 |
| NL6501333A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1966-08-04 |
| ES322528A1 (es) | 1966-11-16 |
| AT260890B (de) | 1968-03-25 |
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