FR3061708B1 - Procede de preparation de materiaux hybrides cœur-coquille - Google Patents

Procede de preparation de materiaux hybrides cœur-coquille Download PDF

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Publication number
FR3061708B1
FR3061708B1 FR1750145A FR1750145A FR3061708B1 FR 3061708 B1 FR3061708 B1 FR 3061708B1 FR 1750145 A FR1750145 A FR 1750145A FR 1750145 A FR1750145 A FR 1750145A FR 3061708 B1 FR3061708 B1 FR 3061708B1
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France
Prior art keywords
shell
hybrid materials
shell hybrid
preparing
preparing heart
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Active
Application number
FR1750145A
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English (en)
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FR3061708A1 (fr
Inventor
Thu-Hoa Tran-Thi
Christophe Theron
William Bamogo
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Centre National de la Recherche Scientifique CNRS
Commissariat a lEnergie Atomique et aux Energies Alternatives CEA
Original Assignee
Centre National de la Recherche Scientifique CNRS
Commissariat a lEnergie Atomique CEA
Commissariat a lEnergie Atomique et aux Energies Alternatives CEA
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Priority to FR1750145A priority Critical patent/FR3061708B1/fr
Priority to KR1020197023045A priority patent/KR20190105040A/ko
Priority to US16/476,166 priority patent/US11318442B2/en
Priority to PCT/FR2018/050030 priority patent/WO2018127671A1/fr
Priority to CN201880010738.2A priority patent/CN110312682A/zh
Priority to EP18700794.3A priority patent/EP3565783A1/fr
Publication of FR3061708A1 publication Critical patent/FR3061708A1/fr
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Publication of FR3061708B1 publication Critical patent/FR3061708B1/fr
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016—Particle form
    • B01J20/28021—Hollow particles, e.g. hollow spheres, microspheres or cenospheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/30—Active carbon
    • C01B32/354—After-treatment
    • C01B32/372—Coating; Grafting; Microencapsulation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/103—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/20—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004—Sorbent size or size distribution, e.g. particle size
    • B01J20/28007—Sorbent size or size distribution, e.g. particle size with size in the range 1-100 nanometers, e.g. nanosized particles, nanofibers, nanotubes, nanowires or the like
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016—Particle form
    • B01J20/28019—Spherical, ellipsoidal or cylindrical
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28023—Fibres or filaments
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28047—Gels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
    • B01J20/3204—Inorganic carriers, supports or substrates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3214—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the method for obtaining this coating or impregnating
    • B01J20/3225—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the method for obtaining this coating or impregnating involving a post-treatment of the coated or impregnated product
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3234—Inorganic material layers
    • B01J20/3236—Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3291—Characterised by the shape of the carrier, the coating or the obtained coated product
    • B01J20/3293—Coatings on a core, the core being particle or fiber shaped, e.g. encapsulated particles, coated fibers
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/16—Preparation of silica xerogels
    • C01B33/163—Preparation of silica xerogels by hydrolysis of organosilicon compounds, e.g. ethyl orthosilicate
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/283—Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/288—Treatment of water, waste water, or sewage by sorption using composite sorbents, e.g. coated, impregnated, multi-layered
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/102—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/106—Silica or silicates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/25—Coated, impregnated or composite adsorbents
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents

Abstract

L'invention concerne un procédé de préparation d'un matériau hybride cœur-coquille constitué d'un cœur de charbon actif entouré d'une coquille de silice sol-gel mésoporeuse, ledit procédé comprenant la formation d'une coquille de silice sol-gel mésoporeuse autour de particules de charbon actif.
FR1750145A 2017-01-06 2017-01-06 Procede de preparation de materiaux hybrides cœur-coquille Active FR3061708B1 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
FR1750145A FR3061708B1 (fr) 2017-01-06 2017-01-06 Procede de preparation de materiaux hybrides cœur-coquille
KR1020197023045A KR20190105040A (ko) 2017-01-06 2018-01-08 코어-쉘 하이브리드 물질의 제조방법
US16/476,166 US11318442B2 (en) 2017-01-06 2018-01-08 Method for producing core-shell hybrid materials
PCT/FR2018/050030 WO2018127671A1 (fr) 2017-01-06 2018-01-08 Procede de preparation de materiaux hybrides coeur-coquille
CN201880010738.2A CN110312682A (zh) 2017-01-06 2018-01-08 制备芯壳杂化材料的方法
EP18700794.3A EP3565783A1 (fr) 2017-01-06 2018-01-08 Procede de preparation de materiaux hybrides coeur-coquille

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1750145A FR3061708B1 (fr) 2017-01-06 2017-01-06 Procede de preparation de materiaux hybrides cœur-coquille
FR1750145 2017-01-06

Publications (2)

Publication Number Publication Date
FR3061708A1 FR3061708A1 (fr) 2018-07-13
FR3061708B1 true FR3061708B1 (fr) 2021-10-22

Family

ID=58739071

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1750145A Active FR3061708B1 (fr) 2017-01-06 2017-01-06 Procede de preparation de materiaux hybrides cœur-coquille

Country Status (6)

Country Link
US (1) US11318442B2 (fr)
EP (1) EP3565783A1 (fr)
KR (1) KR20190105040A (fr)
CN (1) CN110312682A (fr)
FR (1) FR3061708B1 (fr)
WO (1) WO2018127671A1 (fr)

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CN107188173B (zh) * 2017-05-17 2020-08-11 安徽省舒城华竹实业有限公司 巯基功能化介孔竹炭材料的制备方法
FR3083682B1 (fr) * 2018-07-12 2020-12-11 Ethera Couvercle anti-odeur
EP3860755A1 (fr) * 2018-10-02 2021-08-11 Waters Technologies Corporation Sorbants, dispositifs, kits et procédés utiles pour le traitement d'échantillons biologiques
CN109225139A (zh) * 2018-11-06 2019-01-18 南方科技大学 城市生活污水污泥基重金属吸附剂及其制备方法、应用
US20230149893A1 (en) * 2020-03-31 2023-05-18 National University Of Singapore Activated Carbon and Method of Fabrication Thereof
CN112156729B (zh) * 2020-08-25 2021-10-12 安徽壹石通材料科技股份有限公司 一种氧化硅/碳复合结构微球的制备方法
CN112675814B (zh) * 2020-12-10 2022-03-29 四川大学 一种富硅生物质基生物炭/介孔二氧化硅复合材料及其制备方法与应用
CN112517083B (zh) * 2020-12-10 2023-05-05 李通 一种用于制氯乙烯的催化剂及其制备方法
CN112645327B (zh) * 2020-12-21 2022-09-23 中国烟草总公司郑州烟草研究院 多孔碳核壳复合材料的制备方法
CN112645324B (zh) * 2020-12-21 2022-10-04 中国烟草总公司郑州烟草研究院 具有核壳结构的多孔碳复合材料及其制备方法和应用
CN113426429B (zh) * 2021-06-30 2022-12-27 西安大望山化工科技有限公司 一种脱氯剂的制备方法
DE102022103174A1 (de) * 2022-02-10 2023-08-10 Volkswagen Aktiengesellschaft Funktionalisierte Aktivkohle als Adsorptionsmittel für die Abscheidung von CO2 aus der Atmosphärenluft

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DE4343358A1 (de) * 1993-12-18 1995-06-22 Hasso Von Bluecher Aktivkohle enthaltende poröse Körper
KR100708331B1 (ko) * 2005-07-04 2007-04-17 최성우 휘발성탄화수소 회수용 흡착제 및 그 제조방법
KR101770549B1 (ko) 2009-08-06 2017-08-23 주식회사 쿠라레 활성탄 성형체 및 이를 사용한 정수기
CN102059022B (zh) 2010-11-23 2012-10-03 苏州市维欧泰克精密制造有限公司 用于去除饮用水中钠的过滤介质
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CN102773073A (zh) * 2011-11-30 2012-11-14 南京工业大学 一种疏水SiO2气凝胶-活性炭复合材料的制备方法
CN104058542B (zh) 2013-03-18 2016-12-28 王颖 动静组合多级滤床旋流磁化净水器
CN104801279A (zh) * 2015-04-13 2015-07-29 运城学院 溶胶凝胶法改性活性炭粒子的方法
CN105688848A (zh) * 2016-03-12 2016-06-22 常州大学 一种炭-硅复合吸附剂的制备方法
CN106000320B (zh) * 2016-05-30 2019-03-15 济南大学 一种亲水性活性炭以及活性炭粉的亲水处理方法
CN105800607A (zh) * 2016-05-30 2016-07-27 济南大学 一种不易氧化的活性炭粉及活性炭粉的防氧化处理方法

Also Published As

Publication number Publication date
US20190351392A1 (en) 2019-11-21
CN110312682A (zh) 2019-10-08
US11318442B2 (en) 2022-05-03
KR20190105040A (ko) 2019-09-11
EP3565783A1 (fr) 2019-11-13
WO2018127671A9 (fr) 2019-05-16
FR3061708A1 (fr) 2018-07-13
WO2018127671A1 (fr) 2018-07-12

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