FR3047004B1 - Procede de purification d'esters (meth)acryliques - Google Patents

Procede de purification d'esters (meth)acryliques Download PDF

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Publication number
FR3047004B1
FR3047004B1 FR1650469A FR1650469A FR3047004B1 FR 3047004 B1 FR3047004 B1 FR 3047004B1 FR 1650469 A FR1650469 A FR 1650469A FR 1650469 A FR1650469 A FR 1650469A FR 3047004 B1 FR3047004 B1 FR 3047004B1
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FR
France
Prior art keywords
column
meth
section
partition
purified
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1650469A
Other languages
English (en)
French (fr)
Other versions
FR3047004A1 (fr
Inventor
Serge Tretjak
Nathalie Hess
Rose AGUIAR
Pierre-Emmanuel CONOIR
Christophe OSES
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1650469A priority Critical patent/FR3047004B1/fr
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to US16/068,974 priority patent/US10508074B2/en
Priority to KR1020187022465A priority patent/KR102647454B1/ko
Priority to BR112018013060-5A priority patent/BR112018013060B1/pt
Priority to EP17702671.3A priority patent/EP3405450A1/fr
Priority to PCT/FR2017/050005 priority patent/WO2017125657A1/fr
Priority to CN201780007542.3A priority patent/CN108473412A/zh
Priority to JP2018538078A priority patent/JP2019504078A/ja
Priority to TW106101041A priority patent/TW201738199A/zh
Publication of FR3047004A1 publication Critical patent/FR3047004A1/fr
Application granted granted Critical
Publication of FR3047004B1 publication Critical patent/FR3047004B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/006—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/62—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
FR1650469A 2016-01-20 2016-01-21 Procede de purification d'esters (meth)acryliques Active FR3047004B1 (fr)

Priority Applications (9)

Application Number Priority Date Filing Date Title
FR1650469A FR3047004B1 (fr) 2016-01-21 2016-01-21 Procede de purification d'esters (meth)acryliques
KR1020187022465A KR102647454B1 (ko) 2016-01-21 2017-01-03 (메트)아크릴 에스테르의 정제 방법
BR112018013060-5A BR112018013060B1 (pt) 2016-01-21 2017-01-03 Processo para a recuperação de um éster (meta) acrílico purificado e processo para a produção de um éster (meta) acrílico purificado por esterificação direta
EP17702671.3A EP3405450A1 (fr) 2016-01-21 2017-01-03 Procede de purification d'esters (meth)acryliques
US16/068,974 US10508074B2 (en) 2016-01-20 2017-01-03 Method for purifying (meth)acrylic esters
PCT/FR2017/050005 WO2017125657A1 (fr) 2016-01-21 2017-01-03 Procede de purification d'esters (meth)acryliques
CN201780007542.3A CN108473412A (zh) 2016-01-21 2017-01-03 用于纯化(甲基)丙烯酸酯的方法
JP2018538078A JP2019504078A (ja) 2016-01-21 2017-01-03 （メタ）アクリル酸エステルの精製方法
TW106101041A TW201738199A (zh) 2016-01-21 2017-01-12 純化（甲基）丙烯酸酯之方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1650469A FR3047004B1 (fr) 2016-01-21 2016-01-21 Procede de purification d'esters (meth)acryliques
FR1650469 2016-01-21

Publications (2)

Publication Number Publication Date
FR3047004A1 FR3047004A1 (fr) 2017-07-28
FR3047004B1 true FR3047004B1 (fr) 2019-08-09

Family

ID=55542938

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1650469A Active FR3047004B1 (fr) 2016-01-20 2016-01-21 Procede de purification d'esters (meth)acryliques

Country Status (9)

Country Link
US (1) US10508074B2 (enExample)
EP (1) EP3405450A1 (enExample)
JP (1) JP2019504078A (enExample)
KR (1) KR102647454B1 (enExample)
CN (1) CN108473412A (enExample)
BR (1) BR112018013060B1 (enExample)
FR (1) FR3047004B1 (enExample)
TW (1) TW201738199A (enExample)
WO (1) WO2017125657A1 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110114335A (zh) 2016-12-21 2019-08-09 巴斯夫欧洲公司 从粗(甲基)丙烯酸叔丁酯中通过蒸馏分离出纯(甲基)丙烯酸叔丁酯的方法
US10894223B2 (en) 2016-12-21 2021-01-19 Basf Se Process for isolating pure 2-ethylhexyl acrylate or pure 2-propylheptyl acrylate from the corresponding crude alkyl acrylate by distillation
US10906862B2 (en) 2016-12-21 2021-02-02 Basf Se Process for isolating pure butyl acrylate from crude butyl acrylate by distillation, where butyl is n-butyl or isobutyl
FR3083233B1 (fr) 2018-06-27 2020-05-29 Arkema France Procede de purification d'acrylates legers.
FR3091871B1 (fr) * 2019-01-22 2020-12-18 Arkema France Procede de purification d’esters (meth)acryliques a l’aide d’une colonne a partition
EP3956284B1 (en) * 2019-04-16 2023-03-29 Rohm and Haas Company Acid catalyzed synthesis of methyl acrylate from acrylic acid and methanol
KR102902334B1 (ko) * 2019-04-16 2025-12-18 롬 앤드 하아스 컴패니 아크릴산 및 메탄올로부터의 메틸 아크릴레이트의 산 촉매화 합성
CN112552174B (zh) * 2020-12-23 2023-04-11 江门谦信化工发展有限公司 一种精馏乙酸酯的装置及方法
CN114011341B (zh) * 2021-11-15 2024-12-06 丹东明珠特种树脂有限公司 催化精馏塔和深脱除异丁烯之高纯度mtbe制备系统
CN122422029A (zh) * 2023-12-21 2026-07-17 巴斯夫欧洲公司 用于制造(甲基)丙烯酸酯的装置和方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6299345A (ja) * 1985-10-24 1987-05-08 Nippon Kayaku Co Ltd アクリル酸エステル又はメタクリル酸エステルの回収法
JP3999926B2 (ja) * 2000-05-12 2007-10-31 三菱レイヨン株式会社 メタクリル酸エステルの精製方法
JP3672818B2 (ja) * 2000-12-26 2005-07-20 三菱レイヨン株式会社 （メタ）アクリル酸エステルの精製方法
JP4733275B2 (ja) * 2001-01-10 2011-07-27 三菱レイヨン株式会社 （メタ）アクリル酸エステルの精製方法
JP2005239564A (ja) * 2004-02-24 2005-09-08 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの製造方法
JP2007045803A (ja) * 2005-08-12 2007-02-22 Asahi Kasei Chemicals Corp 精製されたメタクリル酸メチルを得る方法
CN101367720A (zh) * 2008-09-18 2009-02-18 中国石油大学(华东) 一种隔壁共沸精馏塔提纯丙烯酸的工艺方法及装置
WO2012071158A1 (en) * 2010-11-22 2012-05-31 Rohm And Haas Company Acrylate production process
KR101496488B1 (ko) * 2010-12-29 2015-02-26 주식회사 엘지화학 고순도 2-에틸헥실-아크릴레이트 생산을 위한 분리벽형 증류탑 및 이를 이용한 제조방법

Also Published As

Publication number Publication date
KR20180108644A (ko) 2018-10-04
KR102647454B1 (ko) 2024-03-13
FR3047004A1 (fr) 2017-07-28
BR112018013060A2 (pt) 2018-12-11
US20190016665A1 (en) 2019-01-17
EP3405450A1 (fr) 2018-11-28
BR112018013060B1 (pt) 2022-02-15
US10508074B2 (en) 2019-12-17
JP2019504078A (ja) 2019-02-14
TW201738199A (zh) 2017-11-01
CN108473412A (zh) 2018-08-31
WO2017125657A1 (fr) 2017-07-27

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