JP2019504078A - （メタ）アクリル酸エステルの精製方法 - Google Patents

（メタ）アクリル酸エステルの精製方法 Download PDF

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Publication number
JP2019504078A
JP2019504078A JP2018538078A JP2018538078A JP2019504078A JP 2019504078 A JP2019504078 A JP 2019504078A JP 2018538078 A JP2018538078 A JP 2018538078A JP 2018538078 A JP2018538078 A JP 2018538078A JP 2019504078 A JP2019504078 A JP 2019504078A
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Japan
Prior art keywords
meth
column
acrylic acid
ester
purified
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JP2018538078A
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English (en)
Japanese (ja)
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JP2019504078A5 (enExample
Inventor
トレチャク，セルジュ
エス，ナタリー
アギアル，ローズ
コノアール，ピエール−エマニュエル
オズ，クリストフ
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Arkema France SA
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Arkema France SA
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Application filed by Arkema France SA filed Critical Arkema France SA
Publication of JP2019504078A publication Critical patent/JP2019504078A/ja
Publication of JP2019504078A5 publication Critical patent/JP2019504078A5/ja
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/006—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/62—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2018538078A 2016-01-21 2017-01-03 （メタ）アクリル酸エステルの精製方法 Pending JP2019504078A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1650469A FR3047004B1 (fr) 2016-01-21 2016-01-21 Procede de purification d'esters (meth)acryliques
FR1650469 2016-01-21
PCT/FR2017/050005 WO2017125657A1 (fr) 2016-01-21 2017-01-03 Procede de purification d'esters (meth)acryliques

Publications (2)

Publication Number Publication Date
JP2019504078A true JP2019504078A (ja) 2019-02-14
JP2019504078A5 JP2019504078A5 (enExample) 2020-01-23

Family

ID=55542938

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2018538078A Pending JP2019504078A (ja) 2016-01-21 2017-01-03 （メタ）アクリル酸エステルの精製方法

Country Status (9)

Country Link
US (1) US10508074B2 (enExample)
EP (1) EP3405450A1 (enExample)
JP (1) JP2019504078A (enExample)
KR (1) KR102647454B1 (enExample)
CN (1) CN108473412A (enExample)
BR (1) BR112018013060B1 (enExample)
FR (1) FR3047004B1 (enExample)
TW (1) TW201738199A (enExample)
WO (1) WO2017125657A1 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110114335A (zh) 2016-12-21 2019-08-09 巴斯夫欧洲公司 从粗(甲基)丙烯酸叔丁酯中通过蒸馏分离出纯(甲基)丙烯酸叔丁酯的方法
US10894223B2 (en) 2016-12-21 2021-01-19 Basf Se Process for isolating pure 2-ethylhexyl acrylate or pure 2-propylheptyl acrylate from the corresponding crude alkyl acrylate by distillation
US10906862B2 (en) 2016-12-21 2021-02-02 Basf Se Process for isolating pure butyl acrylate from crude butyl acrylate by distillation, where butyl is n-butyl or isobutyl
FR3083233B1 (fr) 2018-06-27 2020-05-29 Arkema France Procede de purification d'acrylates legers.
FR3091871B1 (fr) * 2019-01-22 2020-12-18 Arkema France Procede de purification d’esters (meth)acryliques a l’aide d’une colonne a partition
EP3956284B1 (en) * 2019-04-16 2023-03-29 Rohm and Haas Company Acid catalyzed synthesis of methyl acrylate from acrylic acid and methanol
KR102902334B1 (ko) * 2019-04-16 2025-12-18 롬 앤드 하아스 컴패니 아크릴산 및 메탄올로부터의 메틸 아크릴레이트의 산 촉매화 합성
CN112552174B (zh) * 2020-12-23 2023-04-11 江门谦信化工发展有限公司 一种精馏乙酸酯的装置及方法
CN114011341B (zh) * 2021-11-15 2024-12-06 丹东明珠特种树脂有限公司 催化精馏塔和深脱除异丁烯之高纯度mtbe制备系统
CN122422029A (zh) * 2023-12-21 2026-07-17 巴斯夫欧洲公司 用于制造(甲基)丙烯酸酯的装置和方法

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6299345A (ja) * 1985-10-24 1987-05-08 Nippon Kayaku Co Ltd アクリル酸エステル又はメタクリル酸エステルの回収法
JP2001322968A (ja) * 2000-05-12 2001-11-20 Mitsubishi Rayon Co Ltd メタクリル酸エステルの精製方法
JP2002194022A (ja) * 2000-12-26 2002-07-10 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの精製方法、（メタ）アクリル酸エステルおよび（メタ）アクリル樹脂
JP2002205971A (ja) * 2001-01-10 2002-07-23 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの精製方法および（メタ）アクリル酸エステル
JP2005239564A (ja) * 2004-02-24 2005-09-08 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの製造方法
JP2007045803A (ja) * 2005-08-12 2007-02-22 Asahi Kasei Chemicals Corp 精製されたメタクリル酸メチルを得る方法
JP2014506235A (ja) * 2010-11-22 2014-03-13 ローム アンド ハース カンパニー アクリレートの製造方法
JP2014508736A (ja) * 2010-12-29 2014-04-10 エルジー・ケム・リミテッド 高純度の２−エチルヘキシル−アクリレート生産のための分離壁型蒸留塔及びこれを利用した製造方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101367720A (zh) * 2008-09-18 2009-02-18 中国石油大学(华东) 一种隔壁共沸精馏塔提纯丙烯酸的工艺方法及装置

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6299345A (ja) * 1985-10-24 1987-05-08 Nippon Kayaku Co Ltd アクリル酸エステル又はメタクリル酸エステルの回収法
JP2001322968A (ja) * 2000-05-12 2001-11-20 Mitsubishi Rayon Co Ltd メタクリル酸エステルの精製方法
JP2002194022A (ja) * 2000-12-26 2002-07-10 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの精製方法、（メタ）アクリル酸エステルおよび（メタ）アクリル樹脂
JP2002205971A (ja) * 2001-01-10 2002-07-23 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの精製方法および（メタ）アクリル酸エステル
JP2005239564A (ja) * 2004-02-24 2005-09-08 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの製造方法
JP2007045803A (ja) * 2005-08-12 2007-02-22 Asahi Kasei Chemicals Corp 精製されたメタクリル酸メチルを得る方法
JP2014506235A (ja) * 2010-11-22 2014-03-13 ローム アンド ハース カンパニー アクリレートの製造方法
JP2014508736A (ja) * 2010-12-29 2014-04-10 エルジー・ケム・リミテッド 高純度の２−エチルヘキシル−アクリレート生産のための分離壁型蒸留塔及びこれを利用した製造方法

Also Published As

Publication number Publication date
KR20180108644A (ko) 2018-10-04
KR102647454B1 (ko) 2024-03-13
FR3047004B1 (fr) 2019-08-09
FR3047004A1 (fr) 2017-07-28
BR112018013060A2 (pt) 2018-12-11
US20190016665A1 (en) 2019-01-17
EP3405450A1 (fr) 2018-11-28
BR112018013060B1 (pt) 2022-02-15
US10508074B2 (en) 2019-12-17
TW201738199A (zh) 2017-11-01
CN108473412A (zh) 2018-08-31
WO2017125657A1 (fr) 2017-07-27

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