ES8204484A1 - Un procedimiento de preparacion de 4,1',6'-tricloro-4,1',6' tridesoxigalactosacarosa - Google Patents

Un procedimiento de preparacion de 4,1',6'-tricloro-4,1',6' tridesoxigalactosacarosa

Info

Publication number
ES8204484A1
ES8204484A1 ES497862A ES497862A ES8204484A1 ES 8204484 A1 ES8204484 A1 ES 8204484A1 ES 497862 A ES497862 A ES 497862A ES 497862 A ES497862 A ES 497862A ES 8204484 A1 ES8204484 A1 ES 8204484A1
Authority
ES
Spain
Prior art keywords
galactosucrose
trideoxy
trichloro
crystalline
pentahydrate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES497862A
Other languages
English (en)
Other versions
ES497862A0 (es
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tate & Lyle Patent Holdings
Original Assignee
Tate & Lyle Patent Holdings
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from GB7943491A external-priority patent/GB2034323B/en
Application filed by Tate & Lyle Patent Holdings filed Critical Tate & Lyle Patent Holdings
Publication of ES497862A0 publication Critical patent/ES497862A0/es
Publication of ES8204484A1 publication Critical patent/ES8204484A1/es
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07HSUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Saccharide Compounds (AREA)
  • Seasonings (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

PROCEDIMIENTO PARA LA OBTENCION DE 4,186-TRICLORO-4,1,6-TRIDESOXIGALACTOSACAROSA CRISTALINA ANHIDRA Y DE SU PENTAHIDRATO CRISTALINO. CONSISTE EN REALIZAR UNA CLORACION DE LA SACAROSA EN LAS POSICIONES 4,5 Y 6; FORMAR UNA SOLUCION ACUOSA SATURADA CON EL COMPUESTO OBTENIDO Y, POR ULTIMO, EFECTUAR UNA CRISTALIZACION A UNA TEMPERATURA COMPRENDIDA ENTRE 38 Y 100 C O ENTRE 38 Y 3 C, SEGUN SE QUIERA OBTENER LA 4,1,6-TRICLORO-4,1,6-TRIDESOXIGALACTOSACAROSA ANHIDRA O SU PENTAHIDRATO.
ES497862A 1979-12-18 1980-12-17 Un procedimiento de preparacion de 4,1',6'-tricloro-4,1',6' tridesoxigalactosacarosa Expired ES8204484A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB7943491A GB2034323B (en) 1978-12-18 1979-12-18 Production of dna comprising the b hepatitis viral genome
GB8023819 1980-07-21

Publications (2)

Publication Number Publication Date
ES497862A0 ES497862A0 (es) 1982-05-01
ES8204484A1 true ES8204484A1 (es) 1982-05-01

Family

ID=26273904

Family Applications (1)

Application Number Title Priority Date Filing Date
ES497862A Expired ES8204484A1 (es) 1979-12-18 1980-12-17 Un procedimiento de preparacion de 4,1',6'-tricloro-4,1',6' tridesoxigalactosacarosa

Country Status (17)

Country Link
US (1) US4343934A (es)
EP (1) EP0030804B1 (es)
AR (1) AR229023A1 (es)
AU (1) AU538458B2 (es)
CA (1) CA1154760A (es)
DE (1) DE3065399D1 (es)
DK (1) DK157196C (es)
ES (1) ES8204484A1 (es)
FI (1) FI69470C (es)
GR (1) GR72757B (es)
IE (1) IE50634B1 (es)
IL (1) IL61667A (es)
NO (1) NO149242C (es)
NZ (1) NZ195867A (es)
PH (1) PH17320A (es)
PT (1) PT72207B (es)
YU (1) YU40784B (es)

Families Citing this family (44)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4435440A (en) * 1976-01-08 1984-03-06 Tate & Lyle Limited Sweeteners
CA1183133A (en) * 1980-10-28 1985-02-26 Tate & Lyle Public Limited Company Sweet chlorine-substituted disaccharides
DE3271880D1 (en) * 1981-04-29 1986-08-07 Tate & Lyle Plc Sweetening agents
EP0067535B1 (en) * 1981-05-22 1985-01-30 TATE & LYLE PUBLIC LIMITED COMPANY Brominated sucrose derivatives
GB8500862D0 (en) * 1985-01-14 1985-02-20 Tate & Lyle Plc Composition
GB8525953D0 (en) * 1985-10-21 1985-11-27 Mcneilab Inc Preparation of galactopyranoside
GB8525954D0 (en) * 1985-10-21 1985-11-27 Mcneilab Inc Chlorination of carbohydrates &c alcohols
GB8617222D0 (en) * 1986-07-15 1986-08-20 Tate & Lyle Plc Sweetener
GB8627139D0 (en) * 1986-11-13 1986-12-10 Tate & Lyle Plc Sweetening composition
US4820528A (en) * 1987-03-27 1989-04-11 Nabisco Brands, Inc. Sweetener composition
US4986991A (en) * 1987-05-15 1991-01-22 Wm Wrigley, Jr., Company Chewing gum having an extended sweetness
ATE83612T1 (de) * 1987-05-15 1993-01-15 Wrigley W M Jun Co Kaugummi mit geregelter suesse.
US4950746A (en) * 1988-07-18 1990-08-21 Noramco, Inc. Process for synthesizing sucrose derivatives by regioselective reaction
US5169658A (en) * 1989-04-19 1992-12-08 Wm. Wrigley Jr. Company Polyvinyl acetate encapsulation of crystalline sucralose for use in chewing gum
US5059429A (en) * 1989-10-27 1991-10-22 Warner-Lambert Company Sucralose sweetened chewing gum
WO1990007859A2 (en) * 1989-11-22 1990-07-26 Wm. Wrigley Jr. Company Method of controlling release of sucralose in chewing gum and gum produced thereby
US5059428A (en) * 1990-03-12 1991-10-22 Warner-Lambert Company Synergistic sweetening compositions containing polydextrose and a chlorodeoxysurgar and methods for preparing same
US5089608A (en) * 1990-03-23 1992-02-18 Mcneil-Ppc, Inc. Selective 6-acylation of sucrose mediated by cyclic adducts of dialkyltin oxides and diols
US5023329A (en) * 1990-04-23 1991-06-11 Noramco, Inc. Sucrose-6-ester production process
US5139798A (en) * 1990-11-21 1992-08-18 Wm. Wrigley Jr. Company Polyvinyl acetate encapsulation of codried sucralose for use in chewing gum
NZ240818A (en) 1990-12-14 1993-08-26 Mcneil Ppc Inc Liquid sucralose concentrate compositions containing preservative, buffer and liquid
US5169657A (en) * 1991-07-17 1992-12-08 Wm. Wrigley Jr. Company Polyvinyl acetate encapsulation of sucralose from solutions for use in chewing gum
US5747091A (en) * 1992-03-30 1998-05-05 Tate & Lyle Public Limited Company Sweetened extruded food products
US8202257B2 (en) 1998-07-29 2012-06-19 Becton, Dickinson And Company Splatter prevention mechanism for a syringe
US7798993B2 (en) 1998-07-29 2010-09-21 Becton, Dickinson And Company Single use syringe
US6322774B1 (en) 1999-12-20 2001-11-27 Ultradent Products, Inc. Dental bleaching compositions containing sucralose
US6312671B1 (en) 1999-12-20 2001-11-06 Ultradent Products, Inc. Dental bleaching compositions containing sucralose
RU2279437C2 (ru) * 2000-11-17 2006-07-10 Тейт Энд Лайл Паблик Лимитед Компани Усовершенствованная сукралозная композиция и способ ее получения
US8263150B2 (en) 2001-12-19 2012-09-11 The Procter & Gamble Company Beverage compositions having low levels of preservative with enhanced microbial stability
US6998480B2 (en) 2002-03-08 2006-02-14 Tate & Lyle Public Limited Company Process for improving sucralose purity and yield
US20040170735A2 (en) * 2002-04-05 2004-09-02 Mcneil-Ppc, Inc. Methods and compositions for altering the sweetness delivery profile of sucralose
US6943248B2 (en) * 2003-04-30 2005-09-13 Tate & Lyle Public Limited Company Crystalline form of sucralose, and method for producing it
JP2007529505A (ja) * 2004-03-19 2007-10-25 ファームド メディケア プライベート リミティッド 塩素化スクロース製造の改良された方法
US20050214425A1 (en) * 2004-03-23 2005-09-29 Roma Vazirani Sugar substitute prepared with nutritive and high-intensity sweeteners
US20080202503A1 (en) * 2004-07-29 2008-08-28 Ensuiko Sugar Refining Co., Ltd Crystalline Lactosucrose or Syrup Containing Crystalline Lactosucrose and Use Thereof
US20060247180A1 (en) * 2005-04-29 2006-11-02 Bergey James L Purgative composition and uses thereof
CN100567319C (zh) * 2006-07-12 2009-12-09 上海迪赛诺维生素有限公司 一种三氯蔗糖的结晶方法
US8575333B2 (en) * 2006-09-14 2013-11-05 Bahram Memarzadeh Halogenated alkyl di- and trisaccharides, pharmaceutical formulations, diagnostic kits and methods of treatment
CN100591684C (zh) * 2006-12-27 2010-02-24 盐城捷康三氯蔗糖制造有限公司 三氯蔗糖结晶方法
CN101260126B (zh) * 2007-03-06 2010-12-22 盐城捷康三氯蔗糖制造有限公司 三氯蔗糖的结晶方法
CN101245085B (zh) 2007-12-19 2012-02-01 上海同辰生物科技有限公司 一种三氯蔗糖的合成及纯化工艺
WO2009108842A1 (en) * 2008-02-29 2009-09-03 Tate & Lyle Technology Ltd Agglomerates of sucralose and polyols, and their use in chewing gums
CN102336786A (zh) * 2011-11-01 2012-02-01 安徽万和制药有限公司 一种三氯蔗糖的高效结晶方法
CN103242384B (zh) * 2013-05-27 2015-12-02 南通市常海食品添加剂有限公司 三氯蔗糖母液萃取工艺

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3978678A (en) * 1975-10-14 1976-09-07 Hydrotech International, Inc. Method and apparatus for plugging a pipeline
GB1543167A (en) 1976-01-08 1979-03-28 Tate & Lyle Ltd Sweeteners
IL58275A0 (en) * 1978-09-22 1979-12-30 Tate & Lyle Patent Holdings Compositions for prevention of tooth decay comprising chlorodeoxysucrose derivative

Also Published As

Publication number Publication date
DK537880A (da) 1981-06-19
EP0030804A1 (en) 1981-06-24
FI803959L (fi) 1981-06-19
DK157196C (da) 1990-04-23
FI69470B (fi) 1985-10-31
IE802658L (en) 1981-06-18
US4343934A (en) 1982-08-10
AU6515180A (en) 1981-06-25
YU40784B (en) 1986-06-30
NO149242B (no) 1983-12-05
NO149242C (no) 1984-03-14
IE50634B1 (en) 1986-05-28
PH17320A (en) 1984-07-20
NZ195867A (en) 1982-11-23
CA1154760A (en) 1983-10-04
FI69470C (fi) 1986-02-10
GR72757B (es) 1983-12-02
ES497862A0 (es) 1982-05-01
AR229023A1 (es) 1983-05-31
IL61667A (en) 1984-05-31
IL61667A0 (en) 1981-01-30
PT72207B (en) 1981-10-28
PT72207A (en) 1981-01-01
DK157196B (da) 1989-11-20
NO803848L (no) 1981-06-19
EP0030804B1 (en) 1983-10-19
DE3065399D1 (en) 1983-11-24
AU538458B2 (en) 1984-08-16
YU316980A (en) 1983-12-31

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Legal Events

Date Code Title Description
FD1A Patent lapsed

Effective date: 20020223