ES484113A1 - Procedimiento para la fabricacion de metilolmelaminas sus- tancialmente monomeras - Google Patents
Procedimiento para la fabricacion de metilolmelaminas sus- tancialmente monomerasInfo
- Publication number
- ES484113A1 ES484113A1 ES484113A ES484113A ES484113A1 ES 484113 A1 ES484113 A1 ES 484113A1 ES 484113 A ES484113 A ES 484113A ES 484113 A ES484113 A ES 484113A ES 484113 A1 ES484113 A1 ES 484113A1
- Authority
- ES
- Spain
- Prior art keywords
- formaldehyde
- melamine
- mols
- preparation
- methylated methylol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/54—Three nitrogen atoms
- C07D251/64—Condensation products of melamine with aldehydes; Derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G12/00—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08G12/02—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
- C08G12/40—Chemically modified polycondensates
- C08G12/42—Chemically modified polycondensates by etherifying
- C08G12/424—Chemically modified polycondensates by etherifying of polycondensates based on heterocyclic compounds
- C08G12/425—Chemically modified polycondensates by etherifying of polycondensates based on heterocyclic compounds based on triazines
- C08G12/427—Melamine
Abstract
Procedimiento para la fabricación de metilolmelaminas sustancialmente monómeras, eterificadas con metilo, que contienen por mol de melanina arriba de 5 moles de formaldehído y arriba de 4 moles de grupos metilol eterificados con metilo y que con un contenido de sólidos de por lo menos 95% en peso a 25ºC tienen una viscosidad inferior a 20 Pa.s, caracterizado porque la melamina se somete a metilolación con una solución acuosa de formalina que contiene entre 30 y 50% en peso de formaldehído y que ha sido ajustada a un pH de ó, 7 a 7, 3 en una relación molar de 1: 6,5 a 1: 8 durante 1-1/2 a 5 horas a 50 - 85º C y la suspensión así obtenida de metilolmelamina se eterifica con 15 a 30 moles de metanol por mol de melamina a temperaturas comprendidas entre 30 y 60ºC en presencia de un ácido fuerte.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19782839713 DE2839713A1 (de) | 1978-09-13 | 1978-09-13 | Verfahren zur herstellung weitgehend monomerer methylveraetherter methylolmelamine |
Publications (1)
Publication Number | Publication Date |
---|---|
ES484113A1 true ES484113A1 (es) | 1980-05-16 |
Family
ID=6049278
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES484113A Expired ES484113A1 (es) | 1978-09-13 | 1979-09-12 | Procedimiento para la fabricacion de metilolmelaminas sus- tancialmente monomeras |
Country Status (5)
Country | Link |
---|---|
US (1) | US4223141A (es) |
EP (1) | EP0008683B1 (es) |
AT (1) | ATE754T1 (es) |
DE (2) | DE2839713A1 (es) |
ES (1) | ES484113A1 (es) |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3112808A1 (de) * | 1981-03-31 | 1982-10-14 | Lentia GmbH Chem. u. pharm. Erzeugnisse - Industriebedarf, 8000 München | Verfahren zur herstellung von mischungen teilveraetherter methylolmelamine |
IT1138115B (it) * | 1981-07-28 | 1986-09-17 | Pomponesco Chim | Processo per la produzione di esacis(metossimetil)melammina |
AT378369B (de) * | 1983-08-26 | 1985-07-25 | Krems Chemie Gmbh | Verfahren zur herstellung von methylolierten melaminen |
US5017699A (en) * | 1990-07-19 | 1991-05-21 | Suen Tzeng J | Process for preparing polyalkoxymethylmelamines |
DE19709696A1 (de) * | 1997-03-10 | 1998-09-17 | Basf Ag | Wässerige Holzwerkstoff-Bindemittel |
DE19835114A1 (de) * | 1998-08-04 | 2000-02-10 | Basf Ag | Mikrokapseln aus formaldehydarmen Melamin-Formaldehydharzen |
DE102005058855A1 (de) * | 2005-12-09 | 2007-06-14 | Basf Ag | Veretherte Melamin-Formaldehydkondensate mit hohem Feststoffgehalt und geringer Viskosität |
CN108623766A (zh) * | 2018-05-23 | 2018-10-09 | 重庆建峰浩康化工有限公司 | 高亚氨基甲醚化阻燃密胺树脂及其生产方法 |
CN108727548B (zh) * | 2018-05-23 | 2021-03-23 | 重庆建峰浩康化工有限公司 | 环保型阻燃水溶性高亚氨基密胺树脂及其生产方法 |
CN108623994A (zh) * | 2018-05-23 | 2018-10-09 | 重庆建峰浩康化工有限公司 | 以三羟甲基三聚氰胺生产丁醚化阻燃密胺树脂 |
WO2020041921A1 (zh) * | 2018-08-27 | 2020-03-05 | 江苏国立化工科技有限公司 | 六甲氧基甲基密胺树脂橡胶粘合剂的制备工艺 |
CN109293863A (zh) * | 2018-09-07 | 2019-02-01 | 沈阳化工大学 | 一种一锅法制备三聚氰胺甲醛树脂方法 |
CN111808250B (zh) * | 2020-06-30 | 2023-06-16 | 杭州传化精细化工有限公司 | 一种低甲醛硬挺剂的制备方法 |
CN112011021A (zh) * | 2020-09-28 | 2020-12-01 | 山东阳谷华泰化工股份有限公司 | 一种甲醚化三聚氰胺甲醛树脂的制备方法 |
CN113956415A (zh) * | 2021-11-09 | 2022-01-21 | 山东阳谷华泰化工股份有限公司 | 一种水性亚氨基甲醚化三聚氰胺甲醛树脂的制备方法 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB611013A (en) * | 1942-02-05 | 1948-10-25 | Chem Ind Basel | Manufacture of highly etherified aminotriazine-formaldehyde condensation products |
US2645625A (en) * | 1951-10-31 | 1953-07-14 | Monsanto Chemicals | Methods of concentrating solutions |
FR1086826A (fr) * | 1952-06-28 | 1955-02-16 | Cassella Farbwerke Mainkur Ag | Composés méthylolés d'aminotriazines éthérifiés par du méthanol, insolubles dans l'eau ou miscibles avec peu d'eau seulement et leur préparation |
US2998410A (en) * | 1956-07-09 | 1961-08-29 | American Cyanamid Co | Process for the manufacture of methylol melamines and alkylated methylol melamines |
CH432839A (de) * | 1962-03-01 | 1967-03-31 | Sueddeutsche Kalkstickstoff | Verfahren zur Herstellung mit Wasser mischbarer Methylolmelaminalkylätherharze |
DE2005166C3 (de) * | 1970-02-05 | 1975-05-15 | Chemische Fabrik Pfersee Gmbh, 8900 Augsburg | Verfahren zur Herstellung wasserlöslicher, verätherter Methylolmelamine |
DE2716006A1 (de) * | 1977-04-09 | 1978-10-19 | Cassella Farbwerke Mainkur Ag | Verfahren zur herstellung weitgehend monomerer methylveraetherter methylolmelamine |
-
1978
- 1978-09-13 DE DE19782839713 patent/DE2839713A1/de not_active Withdrawn
-
1979
- 1979-06-25 US US06/051,851 patent/US4223141A/en not_active Expired - Lifetime
- 1979-08-02 EP EP79102771A patent/EP0008683B1/de not_active Expired
- 1979-08-02 AT AT79102771T patent/ATE754T1/de not_active IP Right Cessation
- 1979-08-02 DE DE7979102771T patent/DE2962287D1/de not_active Expired
- 1979-09-12 ES ES484113A patent/ES484113A1/es not_active Expired
Also Published As
Publication number | Publication date |
---|---|
DE2839713A1 (de) | 1980-03-27 |
US4223141A (en) | 1980-09-16 |
DE2962287D1 (en) | 1982-04-15 |
EP0008683A1 (de) | 1980-03-19 |
EP0008683B1 (de) | 1982-03-17 |
ATE754T1 (de) | 1982-04-15 |
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