ES343480A1 - Controlling Continuous Reactions Between Gases and Liquids. - Google Patents

Controlling Continuous Reactions Between Gases and Liquids.

Info

Publication number
ES343480A1
ES343480A1 ES343480A ES343480A ES343480A1 ES 343480 A1 ES343480 A1 ES 343480A1 ES 343480 A ES343480 A ES 343480A ES 343480 A ES343480 A ES 343480A ES 343480 A1 ES343480 A1 ES 343480A1
Authority
ES
Spain
Prior art keywords
extent
differences
reaction
reaction mixture
gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES343480A
Other languages
Spanish (es)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Unilever NV
Original Assignee
Unilever NV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Unilever NV filed Critical Unilever NV
Publication of ES343480A1 publication Critical patent/ES343480A1/en
Expired legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G05CONTROLLING; REGULATING
    • G05DSYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
    • G05D11/00Control of flow ratio
    • G05D11/006Control of flow ratio involving a first fluid acting on the feeding of a second fluid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1862Stationary reactors having moving elements inside placed in series
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/12Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by hydrogenation
    • C11C3/123Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by hydrogenation using catalysts based principally on nickel or derivates
    • GPHYSICS
    • G05CONTROLLING; REGULATING
    • G05DSYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
    • G05D11/00Control of flow ratio
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081Tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00164Controlling or regulating processes controlling the flow
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00186Controlling or regulating processes controlling the composition of the reactive mixture
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00189Controlling or regulating processes controlling the stirring velocity
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00768Baffles attached to the reactor wall vertical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Automation & Control Theory (AREA)
  • General Physics & Mathematics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Fats And Perfumes (AREA)

Abstract

In a continuous controlled process of chemically reacting a gas with a liquid reaction mixture containing a reactant, liquid reaction mixture from 18 is passed through a plurality of reactors 1-5 in series within which the liquid is in surface contact with a gas from 26 introduced to reactor 5 via pipe 25 and optionally introduced via similar pipes to reactors 2, 3, 4. The degree of surface contact of the gas with the reaction mixture caused by rotation of stirrers 10 and 34 in at least the last reactor 5 is controlled by differences between the extent of reaction required and achieved, respectively, where essentially only those differences between the extent of reaction required in the product and the extent of reaction achieved in the reaction mixture at a position subsequent to the penultimate reactor 4 are used for such control, and the differences thus used are employed to reduce the differences between the extent of the reaction required and achieved in the product, respectively. Thus the refractive index of a sample drawn through tube 31 may be measured at 32, a corresponding signal transmitted to controller 33 which compares the signal with a standard representing the extent of reaction required and transmits a further signal controlling the motor of stirrer 34 and possibly the motors controlling the similar stirrers 10.
ES343480A 1966-07-28 1967-07-27 Controlling Continuous Reactions Between Gases and Liquids. Expired ES343480A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL6610611A NL148933B (en) 1966-07-28 1966-07-28 PROCESS FOR THE CONTINUOUS PERTIALLY HARDENING OF EDIBLE OILS AND FATS.

Publications (1)

Publication Number Publication Date
ES343480A1 true ES343480A1 (en) 1968-11-01

Family

ID=19797282

Family Applications (1)

Application Number Title Priority Date Filing Date
ES343480A Expired ES343480A1 (en) 1966-07-28 1967-07-27 Controlling Continuous Reactions Between Gases and Liquids.

Country Status (7)

Country Link
BE (1) BE702051A (en)
DE (1) DE1667316C3 (en)
ES (1) ES343480A1 (en)
GB (1) GB1167955A (en)
LU (1) LU54201A1 (en)
NL (1) NL148933B (en)
SE (1) SE329829B (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NO176361C (en) * 1992-11-12 1995-03-22 Norsk Hydro As Process and equipment for curing oil, grease and fatty acids
FR3122103A1 (en) * 2021-04-27 2022-10-28 Ipsomedic Cascade of Gas - Liquid - Solid reactor for the realization of chemical reactions in continuous flow under high pressure
CN114405449B (en) * 2022-02-19 2024-08-09 鲍熙来 Chemical experiment device based on micro-flow control
FR3134996A1 (en) * 2022-04-27 2023-11-03 Ipsomedic Gas-Liquid-Solid and Liquid-Solid reactor cascade for carrying out chemical reactions in continuous flow under pressure or high pressure

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB723887A (en) * 1951-09-20 1955-02-16 Bamag Ltd In Voluntary Liquida Improvements relating to the continuous hydrogenation of fatty oils and fatty acids
BE605321A (en) * 1960-07-04

Also Published As

Publication number Publication date
SE329829B (en) 1970-10-26
NL6610611A (en) 1967-01-25
DE1667316C3 (en) 1981-05-27
LU54201A1 (en) 1969-05-21
GB1167955A (en) 1969-10-22
NL148933B (en) 1976-03-15
BE702051A (en) 1968-01-29
DE1667316A1 (en) 1971-06-16
DE1667316B2 (en) 1980-10-09

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