ES2647271T3 - Procedimiento para la obtención de fitosteroles y/o tocoferoles a partir de los residuos de una destilación de ésteres de aceites vegetales, de manera preferida a partir de los residuos de destilación procedentes de una transesterificación de aceites vegetales - Google Patents

Procedimiento para la obtención de fitosteroles y/o tocoferoles a partir de los residuos de una destilación de ésteres de aceites vegetales, de manera preferida a partir de los residuos de destilación procedentes de una transesterificación de aceites vegetales Download PDF

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Publication number
ES2647271T3
ES2647271T3 ES11784965.3T ES11784965T ES2647271T3 ES 2647271 T3 ES2647271 T3 ES 2647271T3 ES 11784965 T ES11784965 T ES 11784965T ES 2647271 T3 ES2647271 T3 ES 2647271T3
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ES
Spain
Prior art keywords
range
transesterification
phase
sterols
methanol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
ES11784965.3T
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English (en)
Spanish (es)
Inventor
Joachim Lemp
Nico Baade
Emanuel PÖHLS
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Verbio Vereinigte Bioenergie AG
Original Assignee
Verbio Vereinigte Bioenergie AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/58—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/58—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
    • C07D311/70—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with two hydrocarbon radicals attached in position 2 and elements other than carbon and hydrogen in position 6
    • C07D311/72—3,4-Dihydro derivatives having in position 2 at least one methyl radical and in position 6 one oxygen atom, e.g. tocopherols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07J—STEROIDS
    • C07J9/00—Normal steroids containing carbon, hydrogen, halogen or oxygen substituted in position 17 beta by a chain of more than two carbon atoms, e.g. cholane, cholestane, coprostane
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pyrane Compounds (AREA)
  • Fats And Perfumes (AREA)
  • Steroid Compounds (AREA)
ES11784965.3T 2010-11-03 2011-11-02 Procedimiento para la obtención de fitosteroles y/o tocoferoles a partir de los residuos de una destilación de ésteres de aceites vegetales, de manera preferida a partir de los residuos de destilación procedentes de una transesterificación de aceites vegetales Active ES2647271T3 (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102010050293 2010-11-03
DE102010050293 2010-11-03
PCT/EP2011/069236 WO2012059512A1 (de) 2010-11-03 2011-11-02 Verfahren zur gewinnung von phytosterolen und/oder tocopherolen aus rückständen einer destillation von estern pflanzlicher öle, vorzugsweise aus destillationsrückständen aus einer umesterung von pflanzlichen ölen

Publications (1)

Publication Number Publication Date
ES2647271T3 true ES2647271T3 (es) 2017-12-20

Family

ID=44999744

Family Applications (1)

Application Number Title Priority Date Filing Date
ES11784965.3T Active ES2647271T3 (es) 2010-11-03 2011-11-02 Procedimiento para la obtención de fitosteroles y/o tocoferoles a partir de los residuos de una destilación de ésteres de aceites vegetales, de manera preferida a partir de los residuos de destilación procedentes de una transesterificación de aceites vegetales

Country Status (14)

Country Link
US (1) US9884837B2 (no)
EP (1) EP2635592B1 (no)
CA (1) CA2816964C (no)
DE (1) DE102011117510A1 (no)
DK (1) DK2635592T3 (no)
ES (1) ES2647271T3 (no)
HU (1) HUE037028T2 (no)
LT (1) LT2635592T (no)
NO (1) NO2635592T3 (no)
PL (1) PL2635592T3 (no)
PT (1) PT2635592T (no)
RS (1) RS56519B1 (no)
SI (1) SI2635592T1 (no)
WO (1) WO2012059512A1 (no)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MY185625A (en) * 2015-07-02 2021-05-26 Malaysian Palm Oil Board Mpob Method of extracting and concentrating phytosterol from palm oil by-product
PL3287014T3 (pl) 2016-08-22 2020-08-24 Verbio Vereinigte Bioenergie Ag Sposób wytwarzania kompozycji fitosteroli-fitostanoli
CN114466856A (zh) 2019-09-27 2022-05-10 巴斯夫欧洲公司 生产和纯化甾醇的方法
WO2021058648A1 (en) 2019-09-27 2021-04-01 Basf Se Process for the purification of phytosterol
CN114450386A (zh) * 2019-09-27 2022-05-06 巴斯夫欧洲公司 用于生产甾醇和/或生育酚并回收副产物的方法
FI130917B1 (en) 2019-12-20 2024-05-28 Neste Oyj Flexible integrated production facility system and procedure

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1008767A (en) 1961-06-01 1965-11-03 Eastman Kodak Co Improvements in or relating to sterols and tocopherols
US3335154A (en) 1963-06-04 1967-08-08 Eastman Kodak Co Separation of tocopherols and sterols from deodorizer sludge and the like
JPS5512080B2 (no) 1973-09-18 1980-03-29
DE2750722A1 (de) 1977-11-12 1979-05-17 Bayer Ag Heterocyclische polyisocyanate
DE2936125A1 (de) 1979-09-07 1981-03-26 Henkel KGaA, 40589 Düsseldorf Neue sterinkonzentrate, verfahren zu ihrer gewinnung und ihre verwendung in der fermentativen sterintransformation
DE4228476C2 (de) 1992-08-27 2002-05-02 Cognis Deutschland Gmbh Verfahren zum Gewinnen von Tocopherol und/oder Sterin
US5424457A (en) 1994-05-27 1995-06-13 Eastman Chemical Company Process for the production of sterol and tocopherol concentrates
DE19652522C2 (de) 1996-12-17 2000-10-26 Cognis Deutschland Gmbh Verfahren zur Gewinnung von Tocopherolen und/oder Sterinen
WO1999016785A1 (en) 1997-09-29 1999-04-08 International Paper Company Method for separating sterols from tall oil
CA2230373A1 (en) 1998-02-20 1999-08-20 Forbes Medi-Tech Inc. Method for the preparation of phytosterols from tall oil pitch
US6297353B1 (en) 1998-04-22 2001-10-02 Harting, S.A. Process for obtaining unsaponifiable compounds from black-liquor soaps, tall oil and their by-products
DE19906551C1 (de) 1999-02-13 2000-06-29 Cognis Deutschland Gmbh Verfahren zur Herstellung von Phytosterinen
DE19916034C1 (de) 1999-04-09 2000-08-03 Cognis Deutschland Gmbh Verfahren zur Gewinnung von Phytosterinen
NZ506676A (en) 1999-09-03 2002-09-27 Thomas Harting Recovery of pure sterols from black liquor soap skimmings or tall oil pitch
EP1226157B1 (en) 1999-11-04 2006-03-22 Kao Corporation Process for the purification of phytosterol from fatty acids and their esters
DE10038456A1 (de) 2000-08-07 2002-02-21 Cognis Deutschland Gmbh Verfahren zur Gewinnung von Sterinen
DE10038442A1 (de) 2000-08-07 2002-02-21 Cognis Deutschland Gmbh Verfahren zur Gewinnung von Sterinen aus fettsäurehaltigen Rückständen
DE10038457B4 (de) 2000-08-07 2008-09-25 Cognis Ip Management Gmbh Verfahren zur Gewinnung von Sterinen und Tocopherolen
FR2815962B1 (fr) 2000-10-30 2003-03-07 Isochem Sa Procede de preparation des n-carboxyanhydrides
US6780831B2 (en) 2001-02-02 2004-08-24 Raisio Benecol, Ltd. Process for separating unsaponifiable valuable substances from sulphate soap based materials
BR0106522A (pt) 2001-12-17 2003-09-09 Resitec Ind Quimica Ltda Processo para separar produtos valiosos insaponificáveis obtidos de matérias primas diversas
FR2856067B1 (fr) 2003-06-10 2005-09-09 Novance Procede de recuperation de sterols
MY173044A (en) 2003-11-19 2019-12-20 Carotech Bhd Recovery of phytonutriens from oils
EP1586624B1 (en) 2004-02-06 2013-04-03 Härting Glade, Thomas Francis Process of refinement of crude tall oil using short path distillation
US20080015367A1 (en) 2006-07-11 2008-01-17 Wiley Organics, Inc. Process for isolating phytosterols and tocopherols from deodorizer distillate
JP6057313B2 (ja) 2008-03-10 2017-01-11 サンパイン アーベーＳｕｎｐｉｎｅ Ａｂ 残留植物油ストリームからの植物性ステロールの再生
CN101434633B (zh) 2008-12-22 2011-11-02 西安蓝天生物工程有限责任公司 高含量β-谷甾醇的生产方法
CN101701029B (zh) 2009-01-09 2012-05-23 天津工业大学 一种从植物油脂脱臭馏出物渣油中提取天然植物甾醇的方法
CN101851561A (zh) 2010-06-04 2010-10-06 江南大学 一种利用油脂脱臭馏出物联产生物柴油、植物甾醇和生育酚的方法

Also Published As

Publication number Publication date
LT2635592T (lt) 2017-12-27
EP2635592A1 (de) 2013-09-11
US20130274489A1 (en) 2013-10-17
US9884837B2 (en) 2018-02-06
HUE037028T2 (hu) 2018-08-28
WO2012059512A1 (de) 2012-05-10
EP2635592B1 (de) 2017-08-16
DK2635592T3 (da) 2017-11-20
PT2635592T (pt) 2017-11-16
CA2816964C (en) 2019-02-05
NO2635592T3 (no) 2018-01-13
CA2816964A1 (en) 2012-05-10
DE102011117510A1 (de) 2012-05-03
PL2635592T3 (pl) 2018-05-30
RS56519B1 (sr) 2018-02-28
SI2635592T1 (en) 2018-04-30

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