MY185625A - Method of extracting and concentrating phytosterol from palm oil by-product - Google Patents
Method of extracting and concentrating phytosterol from palm oil by-productInfo
- Publication number
- MY185625A MY185625A MYPI2015001728A MYPI2015001728A MY185625A MY 185625 A MY185625 A MY 185625A MY PI2015001728 A MYPI2015001728 A MY PI2015001728A MY PI2015001728 A MYPI2015001728 A MY PI2015001728A MY 185625 A MY185625 A MY 185625A
- Authority
- MY
- Malaysia
- Prior art keywords
- product
- phytosterol
- solvent
- feed material
- extracting
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07J—STEROIDS
- C07J9/00—Normal steroids containing carbon, hydrogen, halogen or oxygen substituted in position 17 beta by a chain of more than two carbon atoms, e.g. cholane, cholestane, coprostane
Abstract
A method of extracting and concentrating phytosterol from phytosterol-rich by-products (100) is disclosed, wherein the method (100) includes the steps of (a) selecting a feed material (102); (b) subjecting the feed material to a solid-liquid extraction process at a temperature in a range of 35?C to 40?C to yield an extracted product (104); (c) subjecting the extracted product to a reaction process in a 10% ethanolic basic solution(106) at a reflux temperature in a range of 60?C to 80?C for a duration of 30 to 90 minutes; (d) extracting unsaponifiable material by conducting a liquid extraction using non-polar solvent (108); (e) conducting a neutralization process using a non-reacting liquid such as water until neutral pH is obtained (110); and (f) conducting a product purification process via crystallization of product as obtained from step (e) using single solvent wherein ratio between a solvent to the feed material is 10:1 (mass to volume ratio) and the feed material to basic reactant is 2:1 (mass ratio), further wherein a solvent used is a hydrocarbon solvent at a minimum 5 extraction cycles. Most illustrative drawing is FIG. 1.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
MYPI2015001728A MY185625A (en) | 2015-07-02 | 2015-07-02 | Method of extracting and concentrating phytosterol from palm oil by-product |
PCT/MY2016/000037 WO2017003279A2 (en) | 2015-07-02 | 2016-06-28 | Method of extracting and concentrating phytosterol from palm oil by-product |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
MYPI2015001728A MY185625A (en) | 2015-07-02 | 2015-07-02 | Method of extracting and concentrating phytosterol from palm oil by-product |
Publications (1)
Publication Number | Publication Date |
---|---|
MY185625A true MY185625A (en) | 2021-05-26 |
Family
ID=57609391
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MYPI2015001728A MY185625A (en) | 2015-07-02 | 2015-07-02 | Method of extracting and concentrating phytosterol from palm oil by-product |
Country Status (2)
Country | Link |
---|---|
MY (1) | MY185625A (en) |
WO (1) | WO2017003279A2 (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107383138A (en) * | 2017-06-27 | 2017-11-24 | 广西南宁桂知科技有限公司 | A kind of method that natural phytosterin is extracted from dragon fruit bough |
CN108485817B (en) * | 2018-06-08 | 2021-07-23 | 白山市科学技术研究所 | Method for extracting herba Filipendulae extract |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AU618791B2 (en) * | 1988-03-16 | 1992-01-09 | Bioindustry Development Centre | Production of high concentration tocopherols and tocotrienols from palm oil by-product |
US20030144536A1 (en) * | 2002-01-28 | 2003-07-31 | Forbes Medi-Tech Inc. | Process of extracting and purifying phytosterols and phytostanols from tall oil pitch |
MY142319A (en) * | 2002-08-20 | 2010-11-15 | Malaysian Palm Oil Board Mpob | Extraction of palm vitamin e, phytosterols and squalene from palm oil |
US9078850B2 (en) * | 2009-07-30 | 2015-07-14 | The Thailand Research Fund | System and method for extracting vitamin E from fatty acid distillates |
LT2635592T (en) * | 2010-11-03 | 2017-12-27 | Verbio Vereinigte Bioenergie Ag | Method for obtaining phytosterols and/or tocopherols from residue of a distillation of the esters of vegetable oils, preferably from distillation residue from a transesterification of vegetable oils |
-
2015
- 2015-07-02 MY MYPI2015001728A patent/MY185625A/en unknown
-
2016
- 2016-06-28 WO PCT/MY2016/000037 patent/WO2017003279A2/en active Application Filing
Also Published As
Publication number | Publication date |
---|---|
WO2017003279A2 (en) | 2017-01-05 |
WO2017003279A3 (en) | 2017-02-16 |
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