ES2599203T3 - Materiales de tinta líquida y películas hechas a partir de los mismos - Google Patents
Materiales de tinta líquida y películas hechas a partir de los mismos Download PDFInfo
- Publication number
- ES2599203T3 ES2599203T3 ES12733372.2T ES12733372T ES2599203T3 ES 2599203 T3 ES2599203 T3 ES 2599203T3 ES 12733372 T ES12733372 T ES 12733372T ES 2599203 T3 ES2599203 T3 ES 2599203T3
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- ES
- Spain
- Prior art keywords
- grams
- films made
- liquid ink
- film
- ink materials
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/02—Emulsion paints including aerosols
- C09D5/024—Emulsion paints including aerosols characterised by the additives
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/22—Luminous paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K9/00—Tenebrescent materials, i.e. materials for which the range of wavelengths for energy absorption is changed as a result of excitation by some form of energy
- C09K9/02—Organic tenebrescent materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paints Or Removers (AREA)
- Silicon Compounds (AREA)
- Luminescent Compositions (AREA)
- Silicon Polymers (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
Un material de teñido líquido filmógeno que comprende: una dispersión acuosa polimérica; un agente de teñido dispersado en la dispersión polimérica acuosa, en donde el agente de teñido está encapsulado en una pluralidad de partículas híbridas orgánicas-inorgánicas; en donde tras entrar en contacto con un sustrato, el material de teñido líquido filmógeno se seca para formar una película que sea transparente y que se pueda teñir.
Description
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DS-10: Dodecilbencenosulfonato de sodio.
HJB: Una pasta acuosa de pigmento de color negro, obtenida con la designación comercial “1-11-JET BLACK30B465” de Penn Color, Inc., Doylestown, Pennsylvania.
M-600: Una polieteramina, obtenida con la designación comercial “JEFFAMINE M-600” de Huntsman Chemical Corporation, The Woodlands, Texas.
NMP: N-Metil-2-pirrolidona.
PPES: Polipropilenoxisilano, preparada de la siguiente forma: Se añadieron 50 gramos de M-600 a un frasco de cristal con una barra agitadora. Se añadieron gota a gota 19:6 gramos de isocianato de trietoxisililpropano a Jeffamine y se agitaron durante 2 horas a 21 °C. El producto de reacción, PPES, se usó sin purificación.
PSSA: Ácido poliestireno sulfonato co málieco).
PTMS: Feniltrimetoxisilano.
RM-8W: Un modificador de la reología no iónico, obtenido con la designación comercial “ACRYSOL RM-8W” de Dow Chemical Company, Midland, Michigan.
RM-12W: Un modificador de la reología no iónico, obtenido con la designación comercial “ACRYSOL RM-12W” de Dow Chemical Company.
RSP: Un tinte fotocrómico, obtenido con la designación comercial “REVERSACOL STORM PURPLE” de Vivimed Labs Ltd., Hyderabad, India.
RU 13-825: Un poliuretano, obtenido con la designación comercial “RU 13-825” de Stahl USA, Inc., Peabody, Massachusetts.
EPCD1: Un tinte fotocrómico encapsulado, preparado de la siguiente forma. A un matraz de fondo redondo de 1000 ml provisto de un agitador se añadieron 437,5 ml de una solución de hidróxido sódico 6 milimolar, 35 gramos de BTC, y la mezcla se agitó a 21 °C hasta que el BTC se disolvió. 35 gramos de una solución de tinte de silano que contenía un 0,33% en peso de RSP, 33% en peso de PTMS, y 66,67% en peso de A1230 se añadió usando una minibomba VWR de flujo variable a un caudal de 0,1 ml/minuto. La agitación continuó durante al menos dos horas tras completar la adición de la solución de tinte-silano. A continuación se añadieron 437,5 ml de acetato de etilo y el contenido se transfirió a un embudo de decantación grande. La capa orgánica, un 8,2% en peso de ECDP1, a continuación se recogió en un matraz de fondo redondo.
EPCD2: Un tinte fotocrómico encapsulado, se preparó como se ha descrito de forma general en ECDP1, en donde el A1230 se sustituyó por un peso igual de PPES.
EPCD3: Un tinte fotocrómico encapsulado, preparado de la siguiente forma. 178 gramos de una solución de hidróxido sódico 30 milimolar se añadieron a un frasco de vidrio de 473 ml (16 oz), seguido por 11 gramos de DS-l0, y la mezcla se agitó a 21 °C hasta que el DS-10 se disolvió. Continuando con la agitación, se añadieron 11 gramos de una solución de silano-tinte al 1% en peso en PTMS usando la minibomba VWR de flujo variable a un caudal de 0,1 ml/minuto. La agitación continuó durante al menos 2 h a 21 °C, tras completar la adición de la solución RSP-PTMS. El tamaño de partículas promedio de las partículas resultantes se determinó en 30,0 nm de diámetro. La distribución de tamaño de partículas se determinó mediante dispersión de luz dinámica (DLS) usando un analizador de tamaño de partículas modelo “ZETASIZER-NANOZSTM” obtenido con Malvern Instruments, Malvern, Reino Unido. Los soles de muestra se prepararon en agua para realizar mediciones de DLS. Una pequeña alícuota (0,1 — 0,5 ml) se extrajo del sol y se diluyó con 2 ml de agua. La muestra diluida resultante se mezcló bien y después se transfirió a una cubeta de plástico. Se registraron los datos de dispersión de luz después de ajustar la temperatura de la muestra a 25 °C. Para transformar la función de autocorrelación en tamaño de partículas, se utilizaron valores normalizados para la viscosidad (0,8872 x 10-3 Pa.s; 0,8 cps) y el índice de refracción (1,33) del agua a 25 °C. Se usó un valor de 1,428 como el índice de refracción de la sílice amorfa. El diámetro promedio en Z notificado (diámetro de partícula promedio, d, en nm) se basó en una distribución ponderada según la intensidad. Todos los resultados se notificaron en términos del tamaño de partículas, d (nm).
Ejemplo 1
103,3 gramos de n-metil-2-pirrolidona (NMP) se combinaron con 393,4 gramos de 8,2% en peso de EPCD1 en acetato de etilo. El acetato de etilo se eliminó de la mezcla con un evaporador rotatorio, dando como resultado 34% en peso de sol de EPCD1 en NMP. Se añadieron a continuación 5 gramos de cada uno de RU 13-825 y EPCD1-NMP y se mezclaron a 2500 revoluciones usando un mezclador por vortización, modelo “MV 1 MINI VORTEXER” obtenido de IKA Works, Inc., Wilmington, Carolina del Norte. Se introdujeron aproximadamente 1-2 gramos de la mezcla en un porta
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Claims (1)
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imagen1 imagen2
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161501799P | 2011-06-28 | 2011-06-28 | |
US201161501799P | 2011-06-28 | ||
US13/532,307 US9382428B2 (en) | 2011-06-28 | 2012-06-25 | Liquid tint materials and films made therefrom |
US201213532307 | 2012-06-25 | ||
PCT/US2012/044303 WO2013003404A1 (en) | 2011-06-28 | 2012-06-27 | Liquid tint materials and films made therefrom |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2599203T3 true ES2599203T3 (es) | 2017-01-31 |
Family
ID=47389782
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES12733372.2T Active ES2599203T3 (es) | 2011-06-28 | 2012-06-27 | Materiales de tinta líquida y películas hechas a partir de los mismos |
Country Status (8)
Country | Link |
---|---|
US (2) | US9382428B2 (es) |
EP (2) | EP2726571B1 (es) |
JP (1) | JP5963856B2 (es) |
CN (2) | CN103619990A (es) |
BR (1) | BR112013033698A2 (es) |
CA (1) | CA2840605A1 (es) |
ES (1) | ES2599203T3 (es) |
WO (2) | WO2013003264A1 (es) |
Families Citing this family (14)
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CN104736256B (zh) | 2012-06-25 | 2018-09-14 | 3M创新有限公司 | 用于涂覆波状外形表面的装置 |
ITPZ20130008A1 (it) * | 2013-12-17 | 2015-06-18 | Ct Studi S R L | Metodo per la segnalazione di applicazioni di nanotecnologie dei materiali su una superficie |
US10160864B2 (en) | 2014-06-24 | 2018-12-25 | 3M Innovative Properties Company | Polyurethane aerosol compositions, articles, and related methods |
US10139627B2 (en) | 2014-08-13 | 2018-11-27 | 3M Innovative Properties Company | Head-mounted display system and components |
JP2016044227A (ja) * | 2014-08-22 | 2016-04-04 | パナソニック株式会社 | 蛍光体含有硬化物とその製造方法 |
EP3057149A1 (en) | 2015-02-11 | 2016-08-17 | Nitto Europe N.V | Kits comprising TOLED-containing multilayer films for providing windows with an image display |
EP3282290B1 (en) * | 2016-08-09 | 2018-10-17 | Essilor International | Composition for the manufacture of an ophtalmic lens comprising an encapsulated light-absorbing additive |
KR20180032108A (ko) * | 2016-09-21 | 2018-03-29 | 엘지전자 주식회사 | 고신뢰성 유무기 하이브리드 양자점 복합체 및 이의 제조방법 |
CN113234333B (zh) * | 2021-04-09 | 2021-11-05 | 苏州吉人高新材料股份有限公司 | 一种光致变色硫酸钡粉体的制备方法 |
CN113521381B (zh) * | 2021-07-22 | 2024-02-23 | 上海市第六人民医院 | 促进细胞增殖的医用膜材料及其制备方法和应用 |
CN113804592B (zh) * | 2021-09-24 | 2024-06-18 | 中国石油化工股份有限公司 | 一种pan纺丝原液中凝胶粒子的检测方法 |
CN114181575A (zh) * | 2021-12-30 | 2022-03-15 | 济南济润新材料科技有限公司 | 一种水性漆及其制备方法 |
CN114906855B (zh) * | 2022-05-13 | 2023-03-21 | 西安工程大学 | 用于展示指进现象的可视化人造岩芯的制备方法 |
CN118027743B (zh) * | 2024-03-26 | 2024-10-18 | 佛山市西泰陶瓷科技有限公司 | 一种耐酸碱无机复合墨水及其制备方法 |
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2012
- 2012-06-25 CN CN201280030140.2A patent/CN103619990A/zh active Pending
- 2012-06-25 EP EP12803808.0A patent/EP2726571B1/en not_active Not-in-force
- 2012-06-25 US US13/532,307 patent/US9382428B2/en active Active
- 2012-06-25 JP JP2014518883A patent/JP5963856B2/ja not_active Expired - Fee Related
- 2012-06-25 WO PCT/US2012/043960 patent/WO2013003264A1/en active Application Filing
- 2012-06-25 US US14/126,860 patent/US9163145B2/en not_active Expired - Fee Related
- 2012-06-27 CN CN201280032044.1A patent/CN103649241B/zh not_active Expired - Fee Related
- 2012-06-27 BR BR112013033698A patent/BR112013033698A2/pt not_active Application Discontinuation
- 2012-06-27 EP EP12733372.2A patent/EP2726563B1/en not_active Not-in-force
- 2012-06-27 WO PCT/US2012/044303 patent/WO2013003404A1/en active Application Filing
- 2012-06-27 ES ES12733372.2T patent/ES2599203T3/es active Active
- 2012-06-27 CA CA2840605A patent/CA2840605A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
US20140128608A1 (en) | 2014-05-08 |
WO2013003404A1 (en) | 2013-01-03 |
CN103649241B (zh) | 2016-08-17 |
EP2726563B1 (en) | 2016-07-20 |
US20130001830A1 (en) | 2013-01-03 |
EP2726571B1 (en) | 2016-05-25 |
BR112013033698A2 (pt) | 2018-07-03 |
CA2840605A1 (en) | 2013-01-03 |
EP2726571A4 (en) | 2015-02-25 |
EP2726571A1 (en) | 2014-05-07 |
JP2014527094A (ja) | 2014-10-09 |
US9382428B2 (en) | 2016-07-05 |
EP2726563A1 (en) | 2014-05-07 |
WO2013003264A1 (en) | 2013-01-03 |
CN103649241A (zh) | 2014-03-19 |
JP5963856B2 (ja) | 2016-08-03 |
US9163145B2 (en) | 2015-10-20 |
CN103619990A (zh) | 2014-03-05 |
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