ES2193052T3 - Procedimiento continuo para preparar un latex de poliuretano. - Google Patents

Procedimiento continuo para preparar un latex de poliuretano.

Info

Publication number
ES2193052T3
ES2193052T3 ES00906009T ES00906009T ES2193052T3 ES 2193052 T3 ES2193052 T3 ES 2193052T3 ES 00906009 T ES00906009 T ES 00906009T ES 00906009 T ES00906009 T ES 00906009T ES 2193052 T3 ES2193052 T3 ES 2193052T3
Authority
ES
Spain
Prior art keywords
prepare
latex
polyurethane
polyurethane latex
continuous procedure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES00906009T
Other languages
English (en)
Inventor
Kenneth W Skaggs
Paul T Louks
Rick L Tabor
Wayne R Willkomm
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Global Technologies LLC
Original Assignee
Dow Global Technologies LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Global Technologies LLC filed Critical Dow Global Technologies LLC
Application granted granted Critical
Publication of ES2193052T3 publication Critical patent/ES2193052T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/0838—Manufacture of polymers in the presence of non-reactive compounds
    • C08G18/0842—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents
    • C08G18/0861—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of a dispersing phase for the polymers or a phase dispersed in the polymers
    • C08G18/0866—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of a dispersing phase for the polymers or a phase dispersed in the polymers the dispersing or dispersed phase being an aqueous medium
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
    • C08G18/12—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step using two or more compounds having active hydrogen in the first polymerisation step
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805—Compounds having only one group containing active hydrogen
    • C08G18/2815—Monohydroxy compounds
    • C08G18/283—Compounds containing ether groups, e.g. oxyalkylated monohydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2375/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)

Abstract

Un procedimiento para preparar un látex de poliuretano/urea/tiourea con alto contenido en sólidos que comprende las etapas de: a) Hacer confluir, de forma continua, en presencia de una cantidad emulsionante y estabilizante de un tensioactivo, una primera corriente que contiene agua fluyendo a un caudal r1, con una segunda corriente que contiene un prepolímero de poliuretano/urea/tiourea, fluyendo a un caudal r2, para formar un prepolímero de látex de poliuretano/urea/tiourea, y b) poner en contacto el prepolímero de látex con un reactivo prolongador de cadena en condiciones tales que se forme un látex de poliuretano/urea/tiourea; en el que la relación r2:r1 no es menor de 65:35 y es menor de 74:26.
ES00906009T 1999-02-16 2000-02-07 Procedimiento continuo para preparar un latex de poliuretano. Expired - Lifetime ES2193052T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US09/250,640 US6087440A (en) 1999-02-16 1999-02-16 Continuous process for preparing a polyurethane latex

Publications (1)

Publication Number Publication Date
ES2193052T3 true ES2193052T3 (es) 2003-11-01

Family

ID=22948567

Family Applications (1)

Application Number Title Priority Date Filing Date
ES00906009T Expired - Lifetime ES2193052T3 (es) 1999-02-16 2000-02-07 Procedimiento continuo para preparar un latex de poliuretano.

Country Status (16)

Country Link
US (1) US6087440A (es)
EP (1) EP1169368B1 (es)
JP (1) JP2002537424A (es)
KR (1) KR100660441B1 (es)
CN (1) CN1340068A (es)
AT (1) ATE234874T1 (es)
AU (1) AU769772B2 (es)
BR (1) BR0010036B1 (es)
CA (1) CA2362158C (es)
DE (1) DE60001723T2 (es)
DK (1) DK1169368T3 (es)
ES (1) ES2193052T3 (es)
PL (1) PL349283A1 (es)
PT (1) PT1169368E (es)
TW (1) TW524811B (es)
WO (1) WO2000049062A1 (es)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6911487B2 (en) * 2000-11-02 2005-06-28 Dow Global Technologies Inc. Process for preparing aqueous dispersions of hybrid polyurethane particles
WO2003099891A1 (en) * 2002-05-24 2003-12-04 Crompton Corporation Polyurethane dispersions
US7098291B2 (en) 2002-06-10 2006-08-29 Rohm And Haas Company Urethane polymer compositions
US20040116594A1 (en) 2002-12-11 2004-06-17 Debkumar Bhattacharjee Polyurethane prepolymer, stable aqueous dispersions with high solids containing the same and method of using and preparing the aqueous dispersions
US20060111506A1 (en) * 2004-11-22 2006-05-25 Bedri Erdem Filled polyurethane dispersions
US20060116454A1 (en) * 2004-12-01 2006-06-01 Bedri Erdem Stable thermally coaguable polyurethane dispersions
US7435787B2 (en) * 2005-09-14 2008-10-14 Momentive Performance Materials Inc. Process for the continuous production of silylated resin
KR100665864B1 (ko) * 2005-12-31 2007-01-10 주식회사 케이씨씨 수지 조성물 및 그의 제조방법
CN101610832B (zh) * 2006-12-19 2015-01-21 陶氏环球技术有限责任公司 制备分散体的设备和制备分散体的方法
WO2008077118A2 (en) * 2006-12-19 2008-06-26 Dow Global Technologies Inc. An ultra-high solid content polyurethane dispersion and a continuous process for producing ultra-high solid content polyurethane dispersions
DE102006062186A1 (de) * 2006-12-22 2008-06-26 Carl Freudenberg Kg Verfahren zur Herstellung von Harnstoff-Partikeln oder Polyurethan-Harnstoff-Partikeln, Zusammensetzung und deren Verwendung
EP2028223A1 (de) * 2007-08-23 2009-02-25 Bayer MaterialScience AG EO/PO-Blockcopolymere als Stabilisatoren für PUR-Schäume
US10752727B1 (en) 2015-07-10 2020-08-25 Covestro Deutschland Ag Process and apparatus for continuous production of aqueous polyurethane dispersions
CN107082860B (zh) * 2017-04-25 2019-09-20 周建明 一种自乳化型水性聚氨酯固化剂及其制备方法
CN107936211A (zh) * 2017-11-24 2018-04-20 湖南新力华纳米科技有限公司 一种涂料染色用的水性聚氨酯及其制备方法
NL2020093B1 (en) * 2017-12-15 2019-06-25 Stahl Int B V Process for producing aqueous polyurethane dispersions in a continuous manner; apparatus suitable for performing such a process; and products obtained by said process
CN109553747B (zh) * 2018-12-05 2021-06-08 长春工业大学 一种高固含可生物降解水性聚氨酯的制备方法
NL2023089B1 (en) 2019-05-08 2019-10-04 Stahl Int B V Process for producing aqueous polyurethane dispersions in a continuous manner; apparatus suitable for performing such a process; and products obtained by said process
WO2023117854A1 (en) * 2021-12-20 2023-06-29 Basf Se Process for the continuous production of aqueous polyurethane dispersions

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US3178310A (en) * 1962-03-01 1965-04-13 Du Pont Aqueous polyurethane coating emulsions
US3294724A (en) * 1964-11-23 1966-12-27 Wyandotte Chemicals Corp Film-forming urethane latices, and preparation by chain extending a prepolymer of anorganic dhsocyanate and a polymeric diol with a piperazine compound
US3410817A (en) * 1965-04-29 1968-11-12 Wyandotte Chemicals Corp Polyurethane latices
SU523643A3 (ru) * 1973-03-09 1976-07-30 Байер Аг, (Фирма) Способ получени полиуретанмочевины в высокодисперсном виде
US3919173A (en) * 1973-11-23 1975-11-11 Contech Inc Moisture curable polyurethane systems
DE2811148A1 (de) * 1978-03-15 1979-09-20 Bayer Ag Verfahren zur herstellung von waessrigen polyurethan-dispersionen und -loesungen
US4442259A (en) * 1982-04-26 1984-04-10 W. R. Grace & Co. Aqueous-based polyurethane compositions and method of preparation
US4444976A (en) * 1982-12-20 1984-04-24 The Goodyear Tire & Rubber Company Sag resistant two component adhesive and sealant
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CA1304869C (en) * 1986-10-21 1992-07-07 Peter H. Markusch Continuous process for the production of aqueous polyurethane-urea dispersions
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GB8913644D0 (en) * 1989-06-14 1989-08-02 Ici America Inc Aqueous dispersions
CA2020629C (en) * 1989-07-21 2000-02-01 Frank Landy Shelf stable fast-cure aqueous coating
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JPH06166735A (ja) * 1992-12-01 1994-06-14 Dai Ichi Kogyo Seiyaku Co Ltd 活性アミノ基含有ポリウレタンエマルジョン組成物
DE4433929A1 (de) * 1994-09-23 1996-03-28 Basf Ag Wasseremulgierbare Polyisocyanate
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Also Published As

Publication number Publication date
CA2362158C (en) 2009-08-04
US6087440A (en) 2000-07-11
EP1169368A1 (en) 2002-01-09
EP1169368B1 (en) 2003-03-19
DE60001723D1 (de) 2003-04-24
JP2002537424A (ja) 2002-11-05
BR0010036A (pt) 2002-01-02
WO2000049062A1 (en) 2000-08-24
KR20010102124A (ko) 2001-11-15
TW524811B (en) 2003-03-21
KR100660441B1 (ko) 2006-12-22
CN1340068A (zh) 2002-03-13
DK1169368T3 (da) 2003-07-14
DE60001723T2 (de) 2003-12-18
AU2757900A (en) 2000-09-04
PL349283A1 (en) 2002-07-15
ATE234874T1 (de) 2003-04-15
PT1169368E (pt) 2003-07-31
AU769772B2 (en) 2004-02-05
CA2362158A1 (en) 2000-08-24
BR0010036B1 (pt) 2010-02-09

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