ES2182127T3 - Procedimiento de preparacion de un 4-hidroxibenzaldehido y derivados. - Google Patents

Procedimiento de preparacion de un 4-hidroxibenzaldehido y derivados.

Info

Publication number
ES2182127T3
ES2182127T3 ES97947095T ES97947095T ES2182127T3 ES 2182127 T3 ES2182127 T3 ES 2182127T3 ES 97947095 T ES97947095 T ES 97947095T ES 97947095 T ES97947095 T ES 97947095T ES 2182127 T3 ES2182127 T3 ES 2182127T3
Authority
ES
Spain
Prior art keywords
hydroxybenzaldehyde
preparation
derivatives
group
formyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES97947095T
Other languages
English (en)
Inventor
Pascal Metivier
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhodia Chimie SAS
Original Assignee
Rhodia Chimie SAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhodia Chimie SAS filed Critical Rhodia Chimie SAS
Application granted granted Critical
Publication of ES2182127T3 publication Critical patent/ES2182127T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/673—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by change of size of the carbon skeleton
    • C07C45/676—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by change of size of the carbon skeleton by elimination of carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/02—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring monocyclic with no unsaturation outside the aromatic ring
    • C07C39/11—Alkylated hydroxy benzenes containing also acyclically bound hydroxy groups, e.g. saligenol
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/18—Preparation of ethers by reactions not forming ether-oxygen bonds
    • C07C41/30—Preparation of ethers by reactions not forming ether-oxygen bonds by increasing the number of carbon atoms, e.g. by oligomerisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/37—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups
    • C07C45/38—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups being a primary hydroxyl group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/23—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups
    • C07C51/235—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups of —CHO groups or primary alcohol groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)

Abstract

LA PRESENTE INVENCION SE REFIERE A UN PROCEDIMIENTO DE PREPARACION DE UN 4 - HIDROXIBENZALDEHIDO Y DERIVADOS. LA INVENCION SE REFIERE MAS CONCRETAMENTE A LA PREPARACION DE 3 METOXI - 4 - HIDROXIBENZALDEHIDO Y DE 3 - ETOXI - 4 HIDROXIBENZALDEHIDO LLAMADOS RESPECTIVAMENTE "VANILINA" Y ETILVANILINA". EL PROCEDIMIENTO DE PREPARACION DE UN 4 HIDROXIBENZALDEHIDO Y DERIVADOS SE CARACTERIZA PORQUE CONSISTE EN OXIDAR SELECTIVAMENTE EL GRUPO EN POSICION 2 RESPECTO AL GRUPO HIDROXILO, EN GRUPO CARBOXILICO, PRESENTE EN LOS COMPUESTOS FENOLICOS DE UNA MEZCLA QUE COMPRENDE AL MENOS: UN COMPUESTO FENOLICO (A) PORTADOR DE GRUPO FORMILO Y/O HIDROXIMETILO EN POSICION 2 Y 4, UN COMPUESTO FENOLICO (B) PORTADOR DE UN GRUPO FORMILO O HIDROXIMETILO EN POSICION 4, UN COMPUESTO FENOLICO (C) PORTADOR DE UN GRUPO FORMILO O HIDROXIMETILO EN POSICION 3, QUE CONDUCE A UN MEZCLA QUE COMPRENDE UN 3 - CARBOXI - 4 - HIDROXIBENZALDEHIDO, UN 4 HIDROXIBENZALDEHIDO, UN ACIDO 2 - HIDROXIBENZOICO, QUE SE SOMETE A CONTIUACION A UNA OPERACION DE DECARBOXILACION QUE PERMITE OBTENER EL 4 - HIDROXIBENZALDEHIDO Y UN FENOL QUE PUEDE OPCIONALMENTE RECICLARSE.
ES97947095T 1996-11-22 1997-11-19 Procedimiento de preparacion de un 4-hidroxibenzaldehido y derivados. Expired - Lifetime ES2182127T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9614275A FR2756278B1 (fr) 1996-11-22 1996-11-22 Procede de preparation d'un 4-hydroxybenzaldehyde et derives

Publications (1)

Publication Number Publication Date
ES2182127T3 true ES2182127T3 (es) 2003-03-01

Family

ID=9497896

Family Applications (1)

Application Number Title Priority Date Filing Date
ES97947095T Expired - Lifetime ES2182127T3 (es) 1996-11-22 1997-11-19 Procedimiento de preparacion de un 4-hidroxibenzaldehido y derivados.

Country Status (18)

Country Link
US (1) US6184421B1 (es)
EP (1) EP0946482B1 (es)
JP (1) JP4282768B2 (es)
KR (1) KR20000053360A (es)
CN (1) CN1229319C (es)
AT (1) ATE221040T1 (es)
AU (1) AU5226898A (es)
BR (1) BR9713123A (es)
CA (1) CA2271090C (es)
DE (1) DE69714288T2 (es)
ES (1) ES2182127T3 (es)
FR (1) FR2756278B1 (es)
HK (1) HK1023336A1 (es)
NO (1) NO325066B1 (es)
RU (1) RU2194032C2 (es)
TW (1) TW533194B (es)
WO (1) WO1998022419A1 (es)
ZA (1) ZA9710453B (es)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7858666B2 (en) 2007-06-08 2010-12-28 Mannkind Corporation IRE-1α inhibitors
KR100892233B1 (ko) * 2007-10-17 2009-04-09 (주)에스에이치제약 벤즈알데하이드 유도체의 신규한 제조방법
CN102206146B (zh) * 2011-03-23 2014-04-16 中山大学 一种香兰素的制备方法
EP3251526A1 (en) * 2016-05-31 2017-12-06 Borregaard AS Process for preparing mixtures comprising vanillin and ethyl vanillin
CN107537540B (zh) * 2017-08-28 2020-06-16 浙江工业大学 一种MXene(Ti3C2)负载钯催化剂及其制备方法和应用
CN108947780A (zh) * 2018-07-23 2018-12-07 重庆欣欣向荣精细化工有限公司 一种处理乙基香兰素制备中精馏高沸物的方法
CN109503332B (zh) * 2018-11-26 2021-08-06 青岛科技大学 一种利用水杨酸残渣分解回收苯酚钠的方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE72600C (de) * Firma Dr. F. VON HEYDEN NACHFOLGER in Radebeul bei Dresden Verfahren zur Darstellung von Vanillin
GB774696A (en) * 1954-04-30 1957-05-15 Distillers Co Yeast Ltd Process for the production of ortho-methylol phenols
FR2305420A1 (fr) * 1975-03-28 1976-10-22 Rhone Poulenc Ind Procede de preparation d'hydroxybenzaldehydes
DE2943805A1 (de) * 1979-10-30 1981-05-27 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von 3-phenoxy-benzaldehyden
US4351962A (en) * 1980-07-11 1982-09-28 Rhone Poulenc Inc. Process for the preparation of hydroxy benzene carboxaldehydes
FR2730730B1 (fr) * 1995-02-20 1997-04-04 Rhone Poulenc Chimie Procede de preparation d'un 4-hydroxybenzaldehyde substitue
FR2734565B1 (fr) * 1995-05-24 1997-07-04 Rhone Poulenc Chimie Procede de preparation de 3-carboxy-4-hydroxybenzaldehydes et derives

Also Published As

Publication number Publication date
ZA9710453B (en) 1998-06-10
ATE221040T1 (de) 2002-08-15
EP0946482A1 (fr) 1999-10-06
WO1998022419A1 (fr) 1998-05-28
CA2271090A1 (fr) 1998-05-28
DE69714288T2 (de) 2003-03-06
AU5226898A (en) 1998-06-10
NO992437D0 (no) 1999-05-20
HK1023336A1 (en) 2000-09-08
US6184421B1 (en) 2001-02-06
RU2194032C2 (ru) 2002-12-10
JP2001504825A (ja) 2001-04-10
FR2756278B1 (fr) 1998-12-31
NO992437L (no) 1999-07-22
DE69714288D1 (de) 2002-08-29
KR20000053360A (ko) 2000-08-25
EP0946482B1 (fr) 2002-07-24
CN1238752A (zh) 1999-12-15
CA2271090C (fr) 2009-02-17
FR2756278A1 (fr) 1998-05-29
JP4282768B2 (ja) 2009-06-24
NO325066B1 (no) 2008-01-28
TW533194B (en) 2003-05-21
CN1229319C (zh) 2005-11-30
BR9713123A (pt) 2000-04-11

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