ES2164760T3 - Espuma de polimeros extruida con particulas de carga y procedimiento para producirla. - Google Patents

Espuma de polimeros extruida con particulas de carga y procedimiento para producirla.

Info

Publication number
ES2164760T3
ES2164760T3 ES95907992T ES95907992T ES2164760T3 ES 2164760 T3 ES2164760 T3 ES 2164760T3 ES 95907992 T ES95907992 T ES 95907992T ES 95907992 T ES95907992 T ES 95907992T ES 2164760 T3 ES2164760 T3 ES 2164760T3
Authority
ES
Spain
Prior art keywords
extruder
polyol
screw
mixture
conveyor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES95907992T
Other languages
English (en)
Inventor
James H Burgess
Sammie J Glorioso
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Apache Building Products Co
Original Assignee
Apache Building Products Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Apache Building Products Co filed Critical Apache Building Products Co
Application granted granted Critical
Publication of ES2164760T3 publication Critical patent/ES2164760T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/0066—Use of inorganic compounding ingredients
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
    • B29B7/58—Component parts, details or accessories; Auxiliary operations
    • B29B7/60—Component parts, details or accessories; Auxiliary operations for feeding, e.g. end guides for the incoming material
    • B29B7/603—Component parts, details or accessories; Auxiliary operations for feeding, e.g. end guides for the incoming material in measured doses, e.g. proportioning of several materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/74—Mixing; Kneading using other mixers or combinations of mixers, e.g. of dissimilar mixers ; Plant
    • B29B7/7476—Systems, i.e. flow charts or diagrams; Plants
    • B29B7/748—Plants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/80—Component parts, details or accessories; Auxiliary operations
    • B29B7/82—Heating or cooling
    • B29B7/823—Temperature control
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/80—Component parts, details or accessories; Auxiliary operations
    • B29B7/82—Heating or cooling
    • B29B7/826—Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/80—Component parts, details or accessories; Auxiliary operations
    • B29B7/88—Adding charges, i.e. additives
    • B29B7/90—Fillers or reinforcements, e.g. fibres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C44/00—Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles
    • B29C44/34—Auxiliary operations
    • B29C44/3442—Mixing, kneading or conveying the foamable material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C44/00—Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles
    • B29C44/34—Auxiliary operations
    • B29C44/36—Feeding the material to be shaped
    • B29C44/46—Feeding the material to be shaped into an open space or onto moving surfaces, i.e. to make articles of indefinite length
    • B29C44/50—Feeding the material to be shaped into an open space or onto moving surfaces, i.e. to make articles of indefinite length using pressure difference, e.g. by extrusion or by spraying
    • B29C44/505—Feeding the material to be shaped into an open space or onto moving surfaces, i.e. to make articles of indefinite length using pressure difference, e.g. by extrusion or by spraying extruding the compound through a flat die
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/04—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
    • C08J9/12—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a physical blowing agent
    • C08J9/14—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a physical blowing agent organic
    • C08J9/143—Halogen containing compounds
    • C08J9/144—Halogen containing compounds containing carbon, halogen and hydrogen only
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
    • B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
    • B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
    • B29B7/40—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with single shaft
    • B29B7/42—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with single shaft with screw or helix
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
    • B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
    • B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
    • B29B7/46—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft
    • B29B7/48—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/74—Mixing; Kneading using other mixers or combinations of mixers, e.g. of dissimilar mixers ; Plant
    • B29B7/7404—Mixing devices specially adapted for foamable substances
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2201/00—Foams characterised by the foaming process
    • C08J2201/02—Foams characterised by the foaming process characterised by mechanical pre- or post-treatments
    • C08J2201/03—Extrusion of the foamable blend
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2375/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
    • C08J2375/04—Polyurethanes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Medicinal Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Molding Of Porous Articles (AREA)
  • Extrusion Moulding Of Plastics Or The Like (AREA)

Abstract

PROCEDIMIENTO DE EXTRUSION EN UN EXTRUSOR DE TORNILLO (32) DE ELEVADOS NIVELES DE MATERIAL DE RELLENO CONTENIDO EN UN POLIOL Y UN ISOCIANATO, JUNTO CON UN CATALIZADOR, UN TENSIOACTIVO Y UN AGENTE SOPLANTE, QUE SE CARACTERIZA PORQUE LA MEZCLA SE EXTRUYE, PRODUCIENDO UN MATERIAL TERMOENDURECIDO SOBRE UNA BANDA TRANSPORTADORA (2) QUE, SEGUIDAMENTE, SE TRANSFORMA EN ESPUMA.
ES95907992T 1993-11-01 1995-01-06 Espuma de polimeros extruida con particulas de carga y procedimiento para producirla. Expired - Lifetime ES2164760T3 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/144,621 US5424014A (en) 1992-09-18 1993-11-01 Method for extruding foamable polymer material
PCT/US1995/000175 WO1996020966A1 (en) 1993-11-01 1995-01-06 Extruded polymer foam with filler particles and method

Publications (1)

Publication Number Publication Date
ES2164760T3 true ES2164760T3 (es) 2002-03-01

Family

ID=26789444

Family Applications (1)

Application Number Title Priority Date Filing Date
ES95907992T Expired - Lifetime ES2164760T3 (es) 1993-11-01 1995-01-06 Espuma de polimeros extruida con particulas de carga y procedimiento para producirla.

Country Status (10)

Country Link
US (1) US5424014A (es)
EP (1) EP0801660B1 (es)
JP (1) JP3226927B2 (es)
AT (1) ATE206443T1 (es)
AU (1) AU1598995A (es)
CA (1) CA2209563C (es)
DE (1) DE69523070T2 (es)
ES (1) ES2164760T3 (es)
MX (1) MX9704957A (es)
WO (1) WO1996020966A1 (es)

Families Citing this family (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
USRE37095E1 (en) * 1992-09-18 2001-03-13 Apache Products Company Extruded polymer foam with filler particles and method
US5723506A (en) * 1992-09-18 1998-03-03 Apache Products Company Extruded polymer foam with filler particles and method
US5846461A (en) * 1996-11-26 1998-12-08 National Foam Cushion Manufacturing, Inc. Method of manufacturing carpet pads from a polyurethane foam composition
US5981611A (en) * 1997-11-24 1999-11-09 Prince Corporation Thermoformable foam with infrared receptors
US6022912A (en) * 1998-09-22 2000-02-08 Bayer Corporation Expansion of polymeric microspheres insitu in a rigid PUR/PIR foam formulation using a twin screw extruder
US6403663B1 (en) 1999-09-20 2002-06-11 North Carolina State University Method of making foamed materials using surfactants and carbon dioxide
WO2001045941A2 (en) * 1999-12-20 2001-06-28 Advanced Plastics Technologies, Ltd. Laminates and coated materials comprising hydroxy-phenoxyether polymers
EP1268593A4 (en) * 2000-03-27 2004-09-01 Apache Prod Co FIRE RESISTANT FOAM AND FIRE RESISTANT FOAM PRODUCTS, METHOD AND DISPERSION FOR THE PRODUCTION THEREOF
DE10056251B4 (de) * 2000-11-14 2006-06-08 Basf Ag Verfahren zur Herstellung von Polyurethan-Schaumstoffen
US7435483B2 (en) 2001-04-04 2008-10-14 Advanced Plastics Technologies Luxembourg S.A. Process for coating paper, paperboard, and molded fiber with a water-dispersible polyester polymer
DE10123002C1 (de) * 2001-05-11 2002-08-08 Basf Ag Reaktionsapparat zur Herstellung von Reaktions-Kunststoffen
US7363244B2 (en) * 2002-11-08 2008-04-22 Palo Alto Research Center Incorporated Methods, apparatus, and program products for inferring service usage
US20040102830A1 (en) * 2002-11-22 2004-05-27 Williams Terrell M. System for coupling an implanatable medical device to an epicardial site
WO2004065092A1 (en) * 2003-01-22 2004-08-05 Wellstream International Limited Process for manufacturing a flexible tubular pipe having extruded layers made of crosslinked polyethylene
US7763341B2 (en) 2004-01-23 2010-07-27 Century-Board Usa, Llc Filled polymer composite and synthetic building material compositions
US7316559B2 (en) 2004-06-24 2008-01-08 Century-Board Usa, Llc Continuous forming apparatus for three-dimensional foam products
US7794224B2 (en) 2004-09-28 2010-09-14 Woodbridge Corporation Apparatus for the continuous production of plastic composites
US7329374B2 (en) * 2004-12-15 2008-02-12 Lung-Wen Chou Method for manufacturing resing films
JP4694191B2 (ja) * 2004-12-17 2011-06-08 住化バイエルウレタン株式会社 ポリウレタンフォーム成形品の製造法
US20070222106A1 (en) 2006-03-24 2007-09-27 Century-Board Usa, Llc Extrusion of polyurethane composite materials
EP2072564B1 (de) * 2007-12-19 2013-07-03 Sika Technology AG Einkomponentiger, feuchtigkeitshärtender Polymerschaum
MX2010007206A (es) * 2007-12-28 2010-09-30 Bostik Inc Proceso continuo para la producción de selladores y adhesivos de poliuretano de curado por humedad.
US9481759B2 (en) 2009-08-14 2016-11-01 Boral Ip Holdings Llc Polyurethanes derived from highly reactive reactants and coal ash
US8846776B2 (en) 2009-08-14 2014-09-30 Boral Ip Holdings Llc Filled polyurethane composites and methods of making same
JP2013072038A (ja) * 2011-09-28 2013-04-22 Nitto Denko Corp 熱可塑性樹脂発泡体の製造方法
AU2012318528A1 (en) 2011-10-07 2014-05-22 Boral Ip Holdings (Australia) Pty Limited Inorganic polymer/organic polymer composites and methods of making same
WO2014168633A1 (en) 2013-04-12 2014-10-16 Boral Ip Holdings (Australia) Pty Limited Composites formed from an absorptive filler and a polyurethane
TWI667285B (zh) 2013-10-18 2019-08-01 德商巴斯夫歐洲公司 膨脹熱塑性彈性體之製造
JP6321404B2 (ja) * 2014-02-26 2018-05-09 株式会社ジェイテクト 蓄電材料の製造装置および製造方法
WO2016018226A1 (en) 2014-07-28 2016-02-04 Crocco Guy The use of evaporative coolants to manufacture filled polyurethane composites
WO2016022103A1 (en) 2014-08-05 2016-02-11 Amitabha Kumar Filled polymeric composites including short length fibers
WO2016118141A1 (en) 2015-01-22 2016-07-28 Boral Ip Holdings (Australia) Pty Limited Highly filled polyurethane composites
US10030126B2 (en) 2015-06-05 2018-07-24 Boral Ip Holdings (Australia) Pty Limited Filled polyurethane composites with lightweight fillers
WO2017082914A1 (en) 2015-11-12 2017-05-18 Boral Ip Holdings (Australia) Pty Limited Filled polyurethane composites with size-graded fillers
KR102154867B1 (ko) * 2020-02-07 2020-09-10 최규술 폴리우레탄 발포폼 및 그 제조방법
EP4001335A1 (de) 2020-11-18 2022-05-25 Covestro Deutschland AG Verfahren zur herstellung von polyurethan-schaumstoffen
JP2022159929A (ja) * 2021-04-05 2022-10-18 積水化学工業株式会社 ポリオール組成物、ポリウレタン樹脂組成物、及びポリウレタンフォーム
CN113563555A (zh) * 2021-08-17 2021-10-29 长虹美菱股份有限公司 一种聚氨酯发泡料及其发泡工艺

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US3466705A (en) * 1966-03-07 1969-09-16 Owens Illinois Inc Apparatus for extruding foamable plastic materials in tubular form
DE2649996A1 (de) * 1976-10-30 1978-05-03 Bayer Ag Verfahren und vorrichtung zum herstellen eines fuellstoffhaltigen reaktionsgemisches aus mindestens zwei fliessfaehigen komponenten, insbesondere zum erzeugen von polyurethan
DE2707026A1 (de) * 1977-02-18 1978-08-24 Bayer Ag Verfahren und vorrichtung zum kontinuierlichen extrudieren von kunststoffprofilen aus polyurethan-rohstoffen
DE2828506C2 (de) * 1978-06-29 1980-04-17 Bayer Ag, 5090 Leverkusen Verfahren und Vorrichtung zum Herstellen eines schäumfähigen Gemisches aus mindestens zwei fließfähigen, schaumstoffbildenden Reaktionskomponenten und Zuschlagstoffen
DE2854406A1 (de) * 1978-12-16 1980-06-26 Bayer Ag Thermoplastische chemiewerkstoffe und verfahren zu ihrer herstellung
DE2854409A1 (de) * 1978-12-16 1980-06-26 Bayer Ag Verfahren zur herstellung von thermoplastischen chemiewerkstoffen
US4395214A (en) * 1981-08-27 1983-07-26 U.C. Industries Foam extrusion apparatus having downstream upper and lower hinged shaping means and side restraining means
DE3224324A1 (de) * 1982-06-30 1984-01-05 Basf Ag, 6700 Ludwigshafen Zweistufenverfahren zur herstellung von thermoplastischen polyurethan-elastomeren
DK157908C (da) * 1982-12-22 1990-09-03 John Schmidt Byggemateriale til byggeelementer samt fremgangsmaade og anlaeg til fremstilling heraf.
US4496625A (en) * 1983-10-12 1985-01-29 The Celotex Corporation Alkoxylated aromatic amine-aromatic polyester polyol blend and polyisocyanurate foam therefrom
US4795763A (en) * 1988-04-18 1989-01-03 The Celotex Corporation Carbon black-filled foam
US4948859A (en) * 1988-10-28 1990-08-14 Minnesota Mining And Manufacturing Company Extruder polymerization of polyurethanes
US5149722A (en) * 1991-08-28 1992-09-22 The Celotex Corporation Dispersant for carbon black-filled foam
US5137930A (en) * 1991-08-28 1992-08-11 The Celotex Corporation Dispersant for carbon black-filled foam
US5192607A (en) * 1991-08-28 1993-03-09 The Celotex Corporation Dispersant for carbon black-filled foam
US5373026A (en) * 1992-12-15 1994-12-13 The Dow Chemical Company Methods of insulating with plastic structures containing thermal grade carbon black

Also Published As

Publication number Publication date
EP0801660B1 (en) 2001-10-04
US5424014A (en) 1995-06-13
CA2209563C (en) 2002-06-25
AU1598995A (en) 1996-07-24
DE69523070D1 (de) 2001-11-08
ATE206443T1 (de) 2001-10-15
CA2209563A1 (en) 1996-07-11
DE69523070T2 (de) 2002-07-04
JPH10502415A (ja) 1998-03-03
MX9704957A (es) 1998-02-28
JP3226927B2 (ja) 2001-11-12
EP0801660A4 (en) 1998-04-08
EP0801660A1 (en) 1997-10-22
WO1996020966A1 (en) 1996-07-11

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