ES2127600T3 - Procedimiento para la purificacion de n-vinilpirrolidona mediante cristalizacion. - Google Patents
Procedimiento para la purificacion de n-vinilpirrolidona mediante cristalizacion.Info
- Publication number
- ES2127600T3 ES2127600T3 ES96115818T ES96115818T ES2127600T3 ES 2127600 T3 ES2127600 T3 ES 2127600T3 ES 96115818 T ES96115818 T ES 96115818T ES 96115818 T ES96115818 T ES 96115818T ES 2127600 T3 ES2127600 T3 ES 2127600T3
- Authority
- ES
- Spain
- Prior art keywords
- vinylpyrolidone
- crystallization
- purification
- procedure
- crystallizer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000002425 crystallisation Methods 0.000 title abstract 2
- 230000008025 crystallization Effects 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 238000000746 purification Methods 0.000 title abstract 2
- 239000013078 crystal Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D207/00—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
- C07D207/02—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D207/18—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
- C07D207/22—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D207/24—Oxygen or sulfur atoms
- C07D207/26—2-Pyrrolidones
- C07D207/263—2-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms
- C07D207/267—2-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to the ring nitrogen atom
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyrrole Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
EN UN PROCEDIMIENTO PARA LA PURIFICACION DE N-VINIL-PIRROLIDONA POR CRISTALIZACION EN UN CRISTALIZADOR, SE CUBRE LA SUPERFICIE DE CRISTALIZACION DEL CRISTALIZADOR CON UNA CAPA DE N-VINILPIRROLIDONA ANTES DE QUE CREZCAN LOS CRISTALES.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19536859A DE19536859A1 (de) | 1995-10-02 | 1995-10-02 | Verfahren zur Reinigung von N-Vinylpyrrolidon durch Kristallisation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2127600T3 true ES2127600T3 (es) | 1999-04-16 |
Family
ID=7773933
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES96115818T Expired - Lifetime ES2127600T3 (es) | 1995-10-02 | 1996-10-02 | Procedimiento para la purificacion de n-vinilpirrolidona mediante cristalizacion. |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US5710284A (es) |
| EP (1) | EP0767169B1 (es) |
| JP (1) | JP4059304B2 (es) |
| CN (1) | CN1069898C (es) |
| DE (2) | DE19536859A1 (es) |
| ES (1) | ES2127600T3 (es) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19536859A1 (de) * | 1995-10-02 | 1997-04-03 | Basf Ag | Verfahren zur Reinigung von N-Vinylpyrrolidon durch Kristallisation |
| DE10026233A1 (de) * | 2000-05-26 | 2001-11-29 | Basf Ag | Verfahren zur Gewinnung von reinem N-Vinylpyrrolidon |
| JP2004345994A (ja) * | 2003-05-21 | 2004-12-09 | Nippon Shokubai Co Ltd | N−ビニル−2−ピロリドンの精製方法 |
| DE102004058071A1 (de) * | 2004-12-01 | 2006-06-08 | Basf Ag | Verfahren zur Reinigung von polaren Vinylverbindungen |
| DE102004058907A1 (de) | 2004-12-07 | 2006-06-08 | Basf Ag | Reinigung von ionischen Flüssigkeiten |
| US7138528B2 (en) * | 2005-02-01 | 2006-11-21 | Lyondell Chemical Technology, L.P. | Method for crystallizing N-vinyl-2-pyrrolidone |
| EP2336106B1 (en) * | 2005-04-11 | 2014-07-16 | Nippon Shokubai Co., Ltd. | Production method of N-vinyl-2-pyrrolidone |
| DE102008023833B4 (de) * | 2008-05-14 | 2013-03-21 | Hapila Gmbh | Anordnung und Verfahren zur Herstellung von hochreinen Kristallen |
| JP2012072277A (ja) * | 2010-09-29 | 2012-04-12 | Nippon Shokubai Co Ltd | 環状n−ビニルラクタム系架橋体およびその製造方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1555614A (es) * | 1967-09-05 | 1969-01-31 | ||
| US3591764A (en) * | 1969-02-24 | 1971-07-06 | Jury Matveevich Taran | Method of checking metal expulsion in resistance welding |
| SU582247A1 (ru) * | 1976-07-12 | 1977-11-30 | Всесоюзный научно-исследовательский институт технологии кровезаменителей и гормональных препаратов | Способ очистки -винилпирролидона |
| DE3736603A1 (de) * | 1987-10-29 | 1989-05-11 | Basf Ag | Verfahren zur reindarstellung von n-vinylpyrrolid-2-on |
| US4873336A (en) * | 1988-03-28 | 1989-10-10 | Gaf Corporation | Process for the preparation of N-vinyl lactams |
| US5329021A (en) * | 1993-02-04 | 1994-07-12 | Isp Investments Inc. | Process for the production of pure vinyl pyrrolidone |
| DE19536859A1 (de) * | 1995-10-02 | 1997-04-03 | Basf Ag | Verfahren zur Reinigung von N-Vinylpyrrolidon durch Kristallisation |
-
1995
- 1995-10-02 DE DE19536859A patent/DE19536859A1/de not_active Withdrawn
-
1996
- 1996-09-09 US US08/708,820 patent/US5710284A/en not_active Expired - Lifetime
- 1996-09-27 CN CN96113099A patent/CN1069898C/zh not_active Expired - Fee Related
- 1996-09-27 JP JP25636096A patent/JP4059304B2/ja not_active Expired - Fee Related
- 1996-10-02 DE DE59601070T patent/DE59601070D1/de not_active Expired - Lifetime
- 1996-10-02 ES ES96115818T patent/ES2127600T3/es not_active Expired - Lifetime
- 1996-10-02 EP EP96115818A patent/EP0767169B1/de not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE59601070D1 (de) | 1999-02-11 |
| US5710284A (en) | 1998-01-20 |
| JP4059304B2 (ja) | 2008-03-12 |
| DE19536859A1 (de) | 1997-04-03 |
| EP0767169A1 (de) | 1997-04-09 |
| EP0767169B1 (de) | 1998-12-30 |
| CN1069898C (zh) | 2001-08-22 |
| CN1150148A (zh) | 1997-05-21 |
| JPH09169724A (ja) | 1997-06-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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