ES2077433T3 - Procedimiento para preparar cristales de zeolita de tipo mfi uniformes. - Google Patents

Procedimiento para preparar cristales de zeolita de tipo mfi uniformes.

Info

Publication number
ES2077433T3
ES2077433T3 ES92920944T ES92920944T ES2077433T3 ES 2077433 T3 ES2077433 T3 ES 2077433T3 ES 92920944 T ES92920944 T ES 92920944T ES 92920944 T ES92920944 T ES 92920944T ES 2077433 T3 ES2077433 T3 ES 2077433T3
Authority
ES
Spain
Prior art keywords
zeolite crystals
procedure
type zeolite
synthesis mixture
uniform type
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES92920944T
Other languages
English (en)
Spanish (es)
Inventor
Johannes Petrus Verduijn
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ExxonMobil Chemical Patents Inc
Original Assignee
Exxon Chemical Patents Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Exxon Chemical Patents Inc filed Critical Exxon Chemical Patents Inc
Application granted granted Critical
Publication of ES2077433T3 publication Critical patent/ES2077433T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B01J20/18—Synthetic zeolitic molecular sieves
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/02—Crystalline silica-polymorphs, e.g. silicalites dealuminated aluminosilicate zeolites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C01B39/38—Type ZSM-5
    • C01B39/40—Type ZSM-5 using at least one organic template directing agent
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00—Chemistry of inorganic compounds
    • Y10S423/22—MFI, e.g. ZSM-5. silicalite, LZ-241

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Catalysts (AREA)
ES92920944T 1991-10-23 1992-10-08 Procedimiento para preparar cristales de zeolita de tipo mfi uniformes. Expired - Lifetime ES2077433T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB919122498A GB9122498D0 (en) 1991-10-23 1991-10-23 Process for preparing uniform mfitype zeolite crystals

Publications (1)

Publication Number Publication Date
ES2077433T3 true ES2077433T3 (es) 1995-11-16

Family

ID=10703410

Family Applications (1)

Application Number Title Priority Date Filing Date
ES92920944T Expired - Lifetime ES2077433T3 (es) 1991-10-23 1992-10-08 Procedimiento para preparar cristales de zeolita de tipo mfi uniformes.

Country Status (11)

Country Link
US (1) US5672331A (OSRAM)
EP (1) EP0609270B1 (OSRAM)
JP (1) JPH07500561A (OSRAM)
KR (1) KR100245940B1 (OSRAM)
CA (1) CA2122049A1 (OSRAM)
DE (1) DE69204850T2 (OSRAM)
ES (1) ES2077433T3 (OSRAM)
GB (1) GB9122498D0 (OSRAM)
MX (1) MX9206080A (OSRAM)
TW (1) TW250441B (OSRAM)
WO (1) WO1993008124A1 (OSRAM)

Families Citing this family (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SG49056A1 (en) * 1991-10-23 1998-05-18 Exxon Chemical Patents Inc Nanometer-sized molecular sieve crystals or agglomerates and processes for their production
US5863516A (en) * 1992-09-02 1999-01-26 Exxon Chemical Patent Inc. Micro particles
EP0758626A1 (en) 1995-08-04 1997-02-19 Unilever Plc Aluminosilicates
EP0753483A1 (en) 1995-07-10 1997-01-15 Exxon Chemical Patents Inc. Zeolites and processes for their manufacture
EP0753485A1 (en) 1995-07-10 1997-01-15 Exxon Chemical Patents Inc. Zeolites and processes for their manufacture
EP0753482A1 (en) 1995-07-10 1997-01-15 Exxon Chemical Patents Inc. Zeolites and processes for their manufacture
GB9600082D0 (en) * 1996-01-04 1996-03-06 Exxon Chemical Patents Inc Molecular sieves and processes for their manufacture
ZA979264B (en) * 1996-10-17 1998-12-29 Exxon Chemical Patents Inc Synthesis of large crystal zeolites
KR100484081B1 (ko) * 1996-10-17 2005-04-20 엑손모빌 케미칼 패턴츠 인코포레이티드 대결정 제올라이트 함유 제올라이트 촉매를 사용한 탄화수소의 전환 방법
DE19707994A1 (de) † 1997-02-27 1998-09-03 Sued Chemie Ag Verfahren zur Herstellung von Zeolithen mit einem hohen Si/Al-Atomverhältnis
CN1116111C (zh) 1997-12-03 2003-07-30 埃克森美孚化学专利公司 由mfi结构类型的沸石粘合的沸石的制备方法及其用途
GB9816508D0 (en) * 1998-07-29 1998-09-23 Exxon Chemical Patents Inc Molecular sieves and processes for their manufacture
JP4693239B2 (ja) 1998-07-29 2011-06-01 エクソン ケミカル パテンツ インコーポレイテッド 結晶性分子ふるい
WO2000017105A1 (en) 1998-09-22 2000-03-30 Exxon Chemical Patents Inc. Preparation of high silica zeolites bound by zeolite and use thereof
DE19951781A1 (de) * 1999-10-27 2001-05-03 Sued Chemie Ag Verfahren zur Herstellung von synthetischen Zeolithen mit MFI-Struktur
US6521198B2 (en) 2000-05-17 2003-02-18 The Regents Of The University Of California Metal surfaces coated with molecular sieve for corrosion resistance
DE10036953A1 (de) 2000-07-28 2002-02-07 Bayer Ag Verfahren zur Herstellung von Hydroxyaromaten
EP1532076B1 (en) * 2002-08-28 2019-05-15 Albemarle Netherlands B.V. Process for the preparation of doped pentasil-type zeolites using doped seeds
US20070059238A1 (en) * 2004-01-16 2007-03-15 Thakur Ram M Process for enhancing yield of sodium aluminosilicate molecular sieves during synthesis
US7112316B1 (en) * 2005-08-08 2006-09-26 Uop Llc Process for preparing molecular sieves via continuous addition of nutrients
US8048402B2 (en) * 2005-08-18 2011-11-01 Exxonmobil Chemical Patents Inc. Synthesis of molecular sieves having the chabazite framework type and their use in the conversion of oxygenates to olefins
DE102005049362A1 (de) * 2005-10-12 2007-04-19 Basf Ag Verfahren zur Herstellung eines Silikates
US20110009680A1 (en) * 2008-03-31 2011-01-13 Sebastien Kremer Molecular Sieve Composition and Method of Making and Using the Same
FR2936791B1 (fr) * 2008-10-07 2011-05-06 Inst Francais Du Petrole Procede de preparation d'une zeolithe de type structural mfi
US7846994B2 (en) * 2008-12-23 2010-12-07 Potters Industries, Inc. Inorganic microspheres
CZ201091A3 (cs) 2010-02-05 2010-08-04 Výzkumný ústav anorganické chemie, a. s. Zpusob výroby zeolitu pentasilové struktury s rízenou distribucí hliníkových atomu ve skeletu
KR101248880B1 (ko) * 2010-07-06 2013-03-29 한국에너지기술연구원 열균열이 방지된 제올라이트 분리막 및 그 제조 방법
US20120157741A1 (en) * 2010-12-17 2012-06-21 Guang Cao Synthesis of Silicoaluminophosphate Having Lev Framework-Type
EP2676728A1 (en) * 2012-06-18 2013-12-25 ExxonMobil Chemical Patents Inc. Synthesis of crystalline molecular sieves having the EUO framework type
SG11201502434YA (en) * 2012-12-07 2015-04-29 Exxonmobil Res & Eng Co Synthesis of zsm-5 crystals with improved morphology
SG11201503973UA (en) * 2012-12-21 2015-06-29 Exxonmobil Chem Patents Inc Small crystal zsm-5, its synthesis and use
US9932240B2 (en) 2013-03-14 2018-04-03 Jonas Hedlund Method for producing zeolite crystals and/or zeolite-like crystals
CN103708497A (zh) * 2013-12-27 2014-04-09 复旦大学 用于甲醇制烯烃的纳米颗粒堆积的B-Al-ZSM-5沸石催化剂及其制备方法和应用
CN107427820B (zh) 2015-04-09 2021-06-29 巴斯夫公司 Zsm-5催化剂
CN112619685B (zh) * 2020-12-18 2021-11-12 复旦大学 具有mfi结构的纳米雏晶催化剂及其制备方法和应用

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3702886A (en) * 1969-10-10 1972-11-14 Mobil Oil Corp Crystalline zeolite zsm-5 and method of preparing the same
US3808326A (en) * 1971-03-19 1974-04-30 Grace W R & Co Preparation of zeolites
US3781226A (en) * 1972-04-17 1973-12-25 Mobil Oil Corp Treatment of colloidal zeolites
US4002697A (en) * 1973-12-03 1977-01-11 Mobil Oil Corporation Selective production of para-xylene
US4166099A (en) * 1974-04-20 1979-08-28 W. R. Grace & Co. Preparation of zeolites
US4061724A (en) * 1975-09-22 1977-12-06 Union Carbide Corporation Crystalline silica
US4100262A (en) * 1977-08-15 1978-07-11 Mobil Oil Corporation Synthesis of zeolite ZSM-5
US4526879A (en) * 1978-11-13 1985-07-02 Mobil Oil Corporation Synthesis of zeolite ZSM-5
US4205053A (en) * 1979-02-01 1980-05-27 Mobil Oil Corporation Manufacture of nitrogenous zeolites
NL182469C (nl) * 1979-08-02 1988-03-16 Shell Int Research Werkwijze voor de bereiding van kristallijne ijzersilicaten; werkwijze voor het uitvoeren van katalytische processen.
NZ206295A (en) * 1982-11-22 1986-09-10 Mobil Oil Corp Preparation of zeolites
US4908342A (en) * 1985-09-04 1990-03-13 Mobil Oil Corporation ZSM-5 zeolites having uniformly large crystals
FR2608068B1 (fr) * 1986-12-16 1989-03-24 Inst Francais Du Petrole Nouveau procede de synthese de zeolithes du type ferrisilicate, produits ainsi obtenus et leurs utilisations
US5240892A (en) * 1987-09-02 1993-08-31 Mobil Oil Corporation Small crystal ZSM-5, as a catalyst
US4797267A (en) * 1987-12-23 1989-01-10 Mobil Oil Corporation Method of producing rod-shaped ZSM-5 zeolite
FR2631327B1 (fr) * 1988-05-11 1990-09-07 Inst Francais Du Petrole Synthese de nouveaux gallosilicates de structure mfi
EP0514715B1 (en) * 1991-05-17 1997-12-29 Asahi Kasei Kogyo Kabushiki Kaisha Method for producing a particulate zeolite

Also Published As

Publication number Publication date
DE69204850T2 (de) 1996-02-22
EP0609270B1 (en) 1995-09-13
MX9206080A (es) 1993-05-01
KR100245940B1 (ko) 2000-03-02
GB9122498D0 (en) 1991-12-04
CA2122049A1 (en) 1993-04-29
TW250441B (OSRAM) 1995-07-01
JPH07500561A (ja) 1995-01-19
US5672331A (en) 1997-09-30
DE69204850D1 (de) 1995-10-19
WO1993008124A1 (en) 1993-04-29
EP0609270A1 (en) 1994-08-10

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