ES2000606A6 - Procedimiento continuo para la preparacion de cloruro de dimetildialilamonio - Google Patents
Procedimiento continuo para la preparacion de cloruro de dimetildialilamonioInfo
- Publication number
- ES2000606A6 ES2000606A6 ES8600989A ES8600989A ES2000606A6 ES 2000606 A6 ES2000606 A6 ES 2000606A6 ES 8600989 A ES8600989 A ES 8600989A ES 8600989 A ES8600989 A ES 8600989A ES 2000606 A6 ES2000606 A6 ES 2000606A6
- Authority
- ES
- Spain
- Prior art keywords
- vessel
- mol
- stirred
- vessels
- dimethylamine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- GQOKIYDTHHZSCJ-UHFFFAOYSA-M dimethyl-bis(prop-2-enyl)azanium;chloride Chemical compound [Cl-].C=CC[N+](C)(C)CC=C GQOKIYDTHHZSCJ-UHFFFAOYSA-M 0.000 title abstract 3
- 238000010924 continuous production Methods 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 abstract 6
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 3
- OSDWBNJEKMUWAV-UHFFFAOYSA-N Allyl chloride Chemical compound ClCC=C OSDWBNJEKMUWAV-UHFFFAOYSA-N 0.000 abstract 2
- 150000001412 amines Chemical class 0.000 abstract 2
- 238000003756 stirring Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
- C07C209/06—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of halogen atoms
- C07C209/12—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of halogen atoms with formation of quaternary ammonium compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
EL PROCEDIMIENTO DESCRITO SE REALIZA EN AL MENOS DOS RECIPIENTES AGITADORES EN CASCADA ALIMENTANDO AL PRIMERO DIMETILAMINA Y CLORURO DE ALILO EN CANTIDAD ESTEQUIOMETRICA Y SOLAMENTE 70-95 POR CIENTO MOLAR DEL HIDROXIDO DE METAL ALCALINO ESTEQUIOMETRICAMENTE NECESARIO Y CONDUCIENDOLOS POR EL RECIPIENTE A 20-70JC CON UN TIEMPO DE PERMANENCIA TAL QUE EL PRODUCTO SALIENTE DEL RECIPIENTE Y ENVIADO A LOS DEMAS RECIPIENTES CONTENGA TODAVIA COMO MAXIMO 10 POR CIENTO MOLAR DE AMINA LIBRE. EL HIDROXIDO DE METAL ALCALINO RESTANTE SE APORTA CONTINUAMENTE A LOS DEMAS RECIPIENTES Y SE AJUSTA EN ESTOS; A 20-70JC, UN TIEMPO DE PERMANENCIA TAL QUE EL PRODUCTO SALIENTE DE LOS RECIPIENTES CONTENGA TODAVIA COMO MAXIMO 2 POR CIENTO MOLAR DE AMINA LIBRE, OBTENIENDOSE EL CLORURO DE DIMETIL-DIALILAMONIO A PARTIR DEL PRODUCTO SALIENTE DE LA CASCADA.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19853528985 DE3528985A1 (de) | 1985-08-13 | 1985-08-13 | Kontinuierliches verfahren zur herstellung von dimethyldiallylammoniumchlorid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2000606A6 true ES2000606A6 (es) | 1988-03-01 |
Family
ID=6278386
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES8600989A Expired ES2000606A6 (es) | 1985-08-13 | 1986-08-11 | Procedimiento continuo para la preparacion de cloruro de dimetildialilamonio |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4670594A (es) |
| EP (1) | EP0213403B1 (es) |
| JP (1) | JPH0825969B2 (es) |
| BR (1) | BR8603844A (es) |
| CA (1) | CA1260501A (es) |
| DE (2) | DE3528985A1 (es) |
| DK (1) | DK164104C (es) |
| ES (1) | ES2000606A6 (es) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4142541A1 (de) * | 1991-12-21 | 1993-06-24 | Hoechst Ag | Diallylammonium-verbindungen, verfahren zu ihrer herstellung sowie ihre verwendung |
| RU2155186C1 (ru) * | 1999-04-27 | 2000-08-27 | Иванова Елена Борисовна | Способ получения бромистого дидецилдиметиламмония |
| CN1323064C (zh) * | 2004-12-31 | 2007-06-27 | 南京理工大学 | 高纯度阳离子单体二甲基二烯丙基氯化铵的精制方法 |
| CN104262172B (zh) * | 2014-10-23 | 2016-02-10 | 山东宝莫生物化工股份有限公司 | 一种喷洒式提浓釜浓缩二甲基二烯丙基氯化铵的方法 |
| FR3125039B1 (fr) | 2021-07-09 | 2025-03-21 | Snf Sa | Procédé d’obtention d’halogénure de diallyldialkylammonium biosourcé |
| CN114539076A (zh) * | 2022-03-28 | 2022-05-27 | 苏州市晶协高新电子材料有限公司 | 一种二甲基二烯丙基氯化铵的连续化合成装置及工艺 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE136497C (es) * | ||||
| US2923701A (en) * | 1955-05-02 | 1960-02-02 | American Cyanamid Co | Composition comprising a linear copolymer of a quaternary ammonium compound and an ethylenically unsaturated copolymerizable compound |
| US3175008A (en) * | 1961-12-20 | 1965-03-23 | Armour & Co | Preparation of quaternary ammonium chlorides |
| US3461163A (en) * | 1967-03-16 | 1969-08-12 | Calgon Corp | Synthesis of dimethyl diallyl ammonium chloride |
| US3472740A (en) * | 1967-03-28 | 1969-10-14 | Calgon Corp | Process for purifying dialkyl diallyl ammonium chloride and dialkyl dimethallyl ammonium chloride |
| US4151202A (en) * | 1976-03-01 | 1979-04-24 | Nalco Chemical Company | Preparation of diallyl dimethyl ammonium chloride and polydiallyl dimethyl ammonium chloride |
| DD128392A1 (de) * | 1976-11-12 | 1977-11-16 | Detlef Ballschuh | Verfahren zur herstellung von dimethyl-diaethylenungesaettigtenammoniumhalogeniden,vorzugsweise von dimethyldiallylammoniumchlorid |
| JPS60184052A (ja) * | 1984-03-01 | 1985-09-19 | Dai Ichi Kogyo Seiyaku Co Ltd | ジメチルジアリルアンモニウムハライド単量体の製造方法 |
-
1985
- 1985-08-13 DE DE19853528985 patent/DE3528985A1/de not_active Withdrawn
-
1986
- 1986-07-30 DE DE8686110552T patent/DE3672539D1/de not_active Expired - Lifetime
- 1986-07-30 EP EP86110552A patent/EP0213403B1/de not_active Expired - Lifetime
- 1986-08-11 ES ES8600989A patent/ES2000606A6/es not_active Expired
- 1986-08-11 US US06/895,182 patent/US4670594A/en not_active Expired - Lifetime
- 1986-08-12 BR BR8603844A patent/BR8603844A/pt not_active IP Right Cessation
- 1986-08-12 CA CA000515740A patent/CA1260501A/en not_active Expired
- 1986-08-12 DK DK383686A patent/DK164104C/da not_active IP Right Cessation
- 1986-08-12 JP JP61187973A patent/JPH0825969B2/ja not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0213403A2 (de) | 1987-03-11 |
| EP0213403B1 (de) | 1990-07-11 |
| DE3672539D1 (de) | 1990-08-16 |
| DK383686A (da) | 1987-02-14 |
| DK164104B (da) | 1992-05-11 |
| JPS6239550A (ja) | 1987-02-20 |
| EP0213403A3 (en) | 1988-01-13 |
| DK164104C (da) | 1992-10-12 |
| BR8603844A (pt) | 1987-03-24 |
| CA1260501A (en) | 1989-09-26 |
| DE3528985A1 (de) | 1987-02-19 |
| JPH0825969B2 (ja) | 1996-03-13 |
| US4670594A (en) | 1987-06-02 |
| DK383686D0 (da) | 1986-08-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DZ1544A1 (fr) | Procédé pour la préparation de l'éthylène et mixtures contenant de l'éthylène. | |
| ES8406058A1 (es) | Procedimiento de fabricacion de clorosulfato basico de aluminio | |
| ES2000606A6 (es) | Procedimiento continuo para la preparacion de cloruro de dimetildialilamonio | |
| GB1527474A (en) | Production of dichloropinacolone | |
| GB1446538A (en) | Process for the preparation of a bisphenol bischlorocarbonic acid ester | |
| EP0364754A3 (en) | Process for the production of aluminium sulphate, starting from the residual slimes of plants for the anodic oxidation of aluminium, and pump to convey said slimes | |
| GB1419393A (en) | Treatment of potassium silico fluoride to produce metal fluorides | |
| UA8020A1 (uk) | Спосіб отримання 2,4-діхлор-5-фторбензойної кислоти | |
| US4693873A (en) | HCN and iron cyanide complex removal | |
| GB1479747A (en) | Process for the continuous production of monoalkylethanolamines and dialkylethanolamines | |
| ES2004803A6 (es) | Un procedimiento para preparar un liquido alcalino esencialmente exento de sulfuro | |
| GEP19960471B (en) | Method of producing n-sulfamine-3-(2-guanidinethiazol-4-ylmethylthio)-propioneamidine | |
| US4065492A (en) | Process for preparing aminonaphthalene derivatives in a titanium or titanium alloy reactor | |
| KR850008145A (ko) | 회전 오븐중에서 황산과 형석을 반응시켜 플루오르산을 제조하는 방법 | |
| JPS5617921A (en) | Manufacture of potassium sulfate | |
| ES8206372A1 (es) | Procedimiento para la preparacion de pentacloruro de fosforo | |
| GB1462010A (en) | Process for the preparation of bisphenol bischlorocarbonic acid esters | |
| JPS57200341A (en) | Manufacture of n-benzyl-n-isopropylpivaloylamide | |
| US3322820A (en) | Process for the continuous production of anthranilic acid | |
| GB1410420A (en) | Preparation of 1,2-dichloroethane | |
| GB1428542A (en) | Process for the production of sodium potassium or ammonium hexacyanoferrate-ii | |
| JPS5547224A (en) | Production of gypsum | |
| EP0148146A3 (en) | Hydrolysis of nitrilotriacetonitrile | |
| ES444512A1 (es) | Procedimiento para la preparacion de sales de metales alca- linos de las arilenbis-sulfonilureas. | |
| SU749832A1 (ru) | Способ получени амино- -оксифенантридонов |