EP3236756A1 - System zur schnellen umwandlung von rohen maiskörnern in eine masse und fertigprodukte - Google Patents
System zur schnellen umwandlung von rohen maiskörnern in eine masse und fertigprodukteInfo
- Publication number
- EP3236756A1 EP3236756A1 EP15873824.5A EP15873824A EP3236756A1 EP 3236756 A1 EP3236756 A1 EP 3236756A1 EP 15873824 A EP15873824 A EP 15873824A EP 3236756 A1 EP3236756 A1 EP 3236756A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- masa
- corn
- flour
- kernels
- dough
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000002017 Zea mays subsp mays Nutrition 0.000 title claims abstract description 74
- 240000008042 Zea mays Species 0.000 title claims abstract description 73
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 title claims abstract description 70
- 235000005822 corn Nutrition 0.000 title claims abstract description 70
- 241000718541 Tetragastris balsamifera Species 0.000 title claims abstract description 42
- 235000013312 flour Nutrition 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims abstract description 12
- 235000011941 Tilia x europaea Nutrition 0.000 claims abstract description 12
- 239000004571 lime Substances 0.000 claims abstract description 12
- 239000002245 particle Substances 0.000 claims abstract description 7
- 238000012545 processing Methods 0.000 claims abstract description 3
- 235000012184 tortilla Nutrition 0.000 claims description 19
- 238000003801 milling Methods 0.000 claims description 8
- 238000005520 cutting process Methods 0.000 claims description 6
- 235000008371 tortilla/corn chips Nutrition 0.000 claims description 6
- 238000011282 treatment Methods 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 3
- 238000005096 rolling process Methods 0.000 claims description 2
- 238000013467 fragmentation Methods 0.000 claims 2
- 238000006062 fragmentation reaction Methods 0.000 claims 2
- 244000241257 Cucumis melo Species 0.000 claims 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 claims 1
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 claims 1
- 238000000151 deposition Methods 0.000 claims 1
- 230000003020 moisturizing effect Effects 0.000 claims 1
- 239000012634 fragment Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 18
- 239000000047 product Substances 0.000 description 17
- 230000008569 process Effects 0.000 description 16
- 235000013339 cereals Nutrition 0.000 description 10
- 238000010411 cooking Methods 0.000 description 9
- 238000004519 manufacturing process Methods 0.000 description 6
- 238000002791 soaking Methods 0.000 description 6
- 235000013305 food Nutrition 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 4
- 239000002585 base Substances 0.000 description 4
- 239000011575 calcium Substances 0.000 description 4
- 229910052791 calcium Inorganic materials 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 3
- 239000000920 calcium hydroxide Substances 0.000 description 3
- 235000011116 calcium hydroxide Nutrition 0.000 description 3
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 235000009973 maize Nutrition 0.000 description 3
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 3
- 235000011888 snacks Nutrition 0.000 description 3
- 238000012546 transfer Methods 0.000 description 3
- PVNIIMVLHYAWGP-UHFFFAOYSA-N Niacin Chemical compound OC(=O)C1=CC=CN=C1 PVNIIMVLHYAWGP-UHFFFAOYSA-N 0.000 description 2
- 208000002141 Pellagra Diseases 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 235000012054 meals Nutrition 0.000 description 2
- 229960003512 nicotinic acid Drugs 0.000 description 2
- 235000001968 nicotinic acid Nutrition 0.000 description 2
- 239000011664 nicotinic acid Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 241000580063 Ipomopsis rubra Species 0.000 description 1
- 206010029400 Nicotinic acid deficiency Diseases 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 241000482268 Zea mays subsp. mays Species 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000009837 dry grinding Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- PHTXVQQRWJXYPP-UHFFFAOYSA-N ethyltrifluoromethylaminoindane Chemical compound C1=C(C(F)(F)F)C=C2CC(NCC)CC2=C1 PHTXVQQRWJXYPP-UHFFFAOYSA-N 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000008570 general process Effects 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000004572 hydraulic lime Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000010808 liquid waste Substances 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 235000011181 potassium carbonates Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 239000008400 supply water Substances 0.000 description 1
- 235000012789 taco shells Nutrition 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/10—Cereal-derived products
- A23L7/117—Flakes or other shapes of ready-to-eat type; Semi-finished or partly-finished products therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Definitions
- This invention concerns making corn based products from a starting material of raw, uncooked, whole corn kernels, manipulating those kernels into a masa, sheeting the masa and forming cooked products therefrom. Nixtamalization of the corn is occasioned without added external heat or cooking in the presence of lime. Finished products include tortilla, tortilla chips, corn chips, taco shells and snack products of various configurations.
- This invention derives from the ancient process of converting corn, maize, etc. into an edible and digestible food. It was known to the native living in Central America prior to the coming of the European explorers.
- Nixtamalization is the Nahuatl word for the cooking and steeping of corn in alkaline water. The steeping liquor in an earlier era was simply dumped into the local sewer system but in our modern era this is unacceptable environmentally.
- nejayote this liquid was drained off after the process was complete and the remaining corn was washed to remove a portion of its skin and the excess alkali.
- the batch of corn is known as nixtama which can be ground to produce the dough known as masa -from which there was made tortillas, tamales, tiacoyos, etc; or it can be left whole and boiled again to
- Nixtamalization was invented in ancient Mesoamerica, now Mexico and Central America, over 3500 years ago.
- the alkalai of choice in this region is calcium hydroxide (slaked lime).
- Nixtamalization eased the workload of women charged with performing the back-breaking labor of grinding corn. Untreated corn is extremely difficult to grind by hand -especially using the traditional Mesoamerican metate e mano: a stone table and rolling pin.
- nixtamalization does much more.
- Nixtamalized corn has an amazing aroma and flavor, which is why a tortilla doesn't taste like plain cornmeal.
- Nixtamalized corn makes a fantastic masa -ideal for tortillas, tamales, tlacoyos, etc. Untreated corn doesn't - we'll see why later.
- niacin as opposed to green and sweet corn, is deficient in available niacin. It contains plenty of bound niacin (as glycosides associated with proteins) and alkali processing releases it. European explorers did not realize this crucial fact when they appropriated corn as a staple grain.
- Nixtamalized corn is the primary source of calcium for many people who consume tortillas as a staple food.
- “Nixtamalization” is the process of cooking maize grains in a lime solution, soaking and washing them, to obtain "nixtamal”. This nixtamal is then stone-ground to obtain nixtamal dough or masa.
- a variety of products e.g. tortilla and corn chips, tamales, tostadas, tacos, enchiladas, atoles, etc.
- masa and tortilla is the most popular one.
- Whole corn kernels are used in the manufacture of corn tortillas in which the masa flour used to make the tortillas is prepared by a traditional method called nixtamalization.
- the calcium content of corn kernels increases notably depending on the time of soaking of the corn kernels. Simultaneous processes of water and calcium diffusion occur during the nixtamalization process, affecting the final product's physicochemical characteristics.
- nixtamalization refers to the alkaline cooking process of converting corn into foods such as tortillas and snack foods (corn chips, tortillas chips, and tacos).
- This alkaline cooking technique softens the pericarp and allows the endosperm to absorb water, thus facilitating its milling.
- the nixtamal is washed several times to remove excess lime, the maize seed coat, and other solids. This material is then ground into dough (masa) from which tortillas and other food products are made. The nixtamal is also ground and dehydrated to obtain flour used to make tortillas (Sahai etai, 2001).
- traditional nixtamalization processes generate effluents on a large scale, require long soaking time (12-16 hr), and high liquid-waste discharges (3-10 L of contaminating effluents/kg of corn).
- Vaquiero (1986) developed a process (US Patent #4,594,260) by using whole corn kernels in a selective nixtamalization process which comprises separating the hull from the kernels for forming a hull fraction and an endosperm-germ fraction, subjecting only the hull fraction to nixtamalization such as by heating in an alkaline solution and then mixing the nixtamalized hull fraction with the untreated endosperm-germ fraction. This mixture is suitable for producing a good quality corn flour suitable for producing tortillas.
- the present invention discloses a system for producing masa and other corn based products using as starting materials raw, whole kernel corn, the system being operative to convert the raw starting materials into the finished product within a short period of time on the order of 20 minutes.
- Functional components of the system are its controls including the corn weigher, kernel pre-milling treatment means serving to remove kernel pericarp and other kernel factions. Further kernel per-cutting means serve to sever the kernel into smaller pieces prior to milling thus enabling a faster milling operation to produces a flour of a preferred particle distribution.
- Another weighing means in the system serves to measure out proportionate quanta of flour, lime and water for deposit into mixer apparatus means operatively controlled as to rotational speeds, duration and temperature of the constituents being mixed to realize nixtamalization thus creating a masa dough.
- Means serving to transfer the masa dough into a dough fragmenter so as to reduce the dough mass into small pieces so as to facilitate sheeting or other treatments for producing the desired product.
- a general object of the present invention is to produce a system operative on a large commercial scale to produce corn masa using raw corn kernels and not a specialize prepared corn flour as it starting product thus realizing economies in raw material usage and overall quickness in production.
- Another object of this invention is to enable in a continuous system adjustments to achieve better taste profiles in the finished products.
- a further object of the present invention is to enable a commercial producer of corn bases products to be self-sufficient in the realm of corn kernel starting materials.
- Another object of this invention is to enable the production of a consistent masa irrespective of the quality of the starting corn kernel materials.
- Still another object of the present invention is to achieve thorough gelatinization and nixtamalization in producing masa without the need of kernel soaking and cooking time.
- Yet a further object of this invention is to enable masa production that is compatible with community environmental standards in so far as avoiding any effluent discharges into the community waste disposal system.
- Fig. 1 is a elevation view of the discharge side of the masa maker system made in accordance with the principles of the present invention
- Fig. 2 is a view like Fig. 1 but showing the feed side of the masa maker system
- Fig. 3 is a group of 10 views illustrating a mixer apparatus especially adapted for use in the system of the present invention
- Fig. 4 is a group of 4 perspective views illustrating the masa dough breaker or disintegrator especially adapted for use in that system of the present invention.
- Fig. 5 is a group of 9 views, 2 in perspective of the masa dough preacher- disintegrator shown in Fig. 4.
- FIG. 1 There is shown in the drawings, particularly Figs. 1 and 2, a system 10 for making masa starting from raw corn kernels and related corn bases products, the system 10 being configured in accordance with the principles of the present invention.
- a control center station 11 is shown in the drawings embraces as soft ware and firm ware the several controls facilitating the steps for operating the system.
- this system 10 is a unified set of component equipment its automatic controls serve to blend the functions of the individual components without the constant intervention of a human being. There follows a control plan that enables the system operation and overall function to produce masa from raw kernel corn.
- Control 1 Selection of resultant end product from the group tortillas, tortilla chip, corn chip or taco and similar products.
- Control 2 Selection of the corn type. See Tables 1-3 below from which a choice may be made and evaluate the corn's characteristics.
- Control 3 Weigh the corn quantum loaded into the system.
- Control 4 Treatment of the corn kernels, pre-milling, by soaking, abrading to remove pericarp, pre-cutting the kernels to enable removal of the additional pericarp, heart, stem or other corn factions.
- Control 5 Evaluation of the amount of pericarp removal and the amount of residual corn factions.
- Control 6 Mill/grind the residual corn faction into a flour with a desired particle distribution, i.e., control the particle size to the most desirable range.
- Control 7 Load a multi tine mixer 12, as shown in Fig. 3, with a selected quantum of flour and lime in a proper ratio.
- Control 8 Supply water to the dry ingredients in the mixer 12 in a selected volume of water at a preferred water temperature.
- Control 9 Mix for a selected period of time the dry ingredients of flour, lime with water until a preselected temperature of the mixture is attained and nixtamalization occurs developing a body of masa dough formed with a desired degree of gelatization and moisture content.
- Control 10 After removing the body of masa dough from the mixer 12 transfer the dough into a masa disintegrator 13, Figs. 4 and 5, to reduce its size into portions in a size range comparison to that of a soccer ball to that of a baseball, thereby permitting the masa to cool and nixtamalization to cease.
- Control 11 Sheeting the masa portions into the preselected thickness and shaped pieces.
- Control 12 Cooking the shaped pieces in either an oven, an oil bath or the like to attain the selected end product.
- Control 13 Test the end product for taste, crunch and appearance via a taste panel and, if needed, make the necessary adjustment in the above Controls to achieve a perfect product.
- the thirteen Controls listed above could be added to, expanded upon or deleted from as matter dictate and are determined. However all of the Controls will connect to a Master/Prime Control, with a touch screen. The Master Control will be programed to enable quick changes from product to product, from corn type to corn type.
- Suitable apparatus to achieve pre-cutting the corn kernels is available from Urschek Laboratories Incorporated of Valpariso, Indiana, 48384. Comitrol processor models 1700 and 3600 are suitable to perform this function.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201462124605P | 2014-12-26 | 2014-12-26 | |
PCT/US2015/000443 WO2016105557A1 (en) | 2014-12-26 | 2015-12-24 | System for quickly converting raw corn kernels into a masa and finished products |
Publications (3)
Publication Number | Publication Date |
---|---|
EP3236756A1 true EP3236756A1 (de) | 2017-11-01 |
EP3236756A4 EP3236756A4 (de) | 2018-06-20 |
EP3236756B1 EP3236756B1 (de) | 2020-02-26 |
Family
ID=56151280
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP15873824.5A Active EP3236756B1 (de) | 2014-12-26 | 2015-12-24 | System und prozess zur schnellen umwandlung von rohen maiskörnern in eine masse und fertigprodukte |
Country Status (13)
Country | Link |
---|---|
US (1) | US11324240B2 (de) |
EP (1) | EP3236756B1 (de) |
JP (1) | JP6728184B2 (de) |
CN (1) | CN107249337B (de) |
AU (1) | AU2015371280B2 (de) |
BR (2) | BR122020002846B1 (de) |
CA (1) | CA2972241C (de) |
CL (1) | CL2017001702A1 (de) |
CO (1) | CO2017007333A2 (de) |
ES (1) | ES2781250T3 (de) |
MX (1) | MX2017008385A (de) |
PE (1) | PE20171151A1 (de) |
WO (1) | WO2016105557A1 (de) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
MX364082B (es) * | 2017-06-05 | 2019-04-11 | Heat Control Inc | Dispositivo de navaja de desprendimiento de figura de masa y sistema del mismo. |
MX2017007061A (es) * | 2017-06-05 | 2019-02-08 | Heat Control Inc | Proceso y sistema de fabricación de masa vegetal. |
KR20240019477A (ko) | 2022-08-04 | 2024-02-14 | 고려대학교 산학협력단 | 바제독시펜을 유효성분으로 포함하는 염증성 피부질환의 예방 또는 치료용 조성물 |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4778690A (en) * | 1986-08-15 | 1988-10-18 | Mapam, Inc. | Process containing a cooking extrusion step for forming a food product from a cereal |
US5100686A (en) * | 1989-10-19 | 1992-03-31 | Miles J. Willard | Corn rings and method of manufacture |
US4985269A (en) * | 1990-06-12 | 1991-01-15 | Borden, Inc. | Continuous extrusion for tortilla chip production |
DE4137161C2 (de) * | 1991-11-12 | 1994-02-24 | Stephan & Soehne | Verfahren zur Teigbereitung |
US5558886A (en) * | 1993-10-21 | 1996-09-24 | Centro De Investigacion Y De Estudios Avanzados Del I.P.N. | Extrusion apparatus for the preparation of instant fresh corn dough or masa |
JP2750843B2 (ja) | 1996-01-09 | 1998-05-13 | レオン自動機株式会社 | 分割されたパン生地の連結供給方法および装置 |
US6025011A (en) | 1997-06-09 | 2000-02-15 | J. R. Short Milling Company | Process for producing nixtamal and masa flour |
MXPA03009248A (es) * | 2001-04-09 | 2004-01-29 | Cargill Inc | PROCESO PARA LA PRODUCCIoN DE HARINA Y MASA DE NIXTAMAL. |
US20030198725A1 (en) * | 2001-11-28 | 2003-10-23 | Cardenas Juan De Dios Figueroa | Nixtamalized corn and products thereof |
US20120263854A1 (en) * | 2002-06-07 | 2012-10-18 | Innophos, Inc. | Flat bread dough composition and method for making flat breads |
US7955634B2 (en) * | 2006-04-10 | 2011-06-07 | The Quaker Oats Company | Method and system of preventing rancidity in whole grain corn products |
-
2015
- 2015-12-24 US US15/538,962 patent/US11324240B2/en active Active
- 2015-12-24 BR BR122020002846-7A patent/BR122020002846B1/pt active IP Right Grant
- 2015-12-24 ES ES15873824T patent/ES2781250T3/es active Active
- 2015-12-24 CA CA2972241A patent/CA2972241C/en active Active
- 2015-12-24 EP EP15873824.5A patent/EP3236756B1/de active Active
- 2015-12-24 JP JP2017534562A patent/JP6728184B2/ja active Active
- 2015-12-24 MX MX2017008385A patent/MX2017008385A/es unknown
- 2015-12-24 PE PE2017001150A patent/PE20171151A1/es unknown
- 2015-12-24 WO PCT/US2015/000443 patent/WO2016105557A1/en active Application Filing
- 2015-12-24 CN CN201580076957.7A patent/CN107249337B/zh active Active
- 2015-12-24 BR BR112017013819-0A patent/BR112017013819B1/pt active IP Right Grant
- 2015-12-24 AU AU2015371280A patent/AU2015371280B2/en active Active
-
2017
- 2017-06-23 CL CL2017001702A patent/CL2017001702A1/es unknown
- 2017-07-24 CO CONC2017/0007333A patent/CO2017007333A2/es unknown
Also Published As
Publication number | Publication date |
---|---|
AU2015371280B2 (en) | 2019-11-07 |
CA2972241A1 (en) | 2016-06-30 |
BR122020002846B1 (pt) | 2022-02-08 |
MX2017008385A (es) | 2018-05-04 |
CN107249337A (zh) | 2017-10-13 |
CA2972241C (en) | 2022-07-26 |
JP2018500036A (ja) | 2018-01-11 |
BR112017013819A2 (pt) | 2018-02-27 |
JP6728184B2 (ja) | 2020-07-22 |
EP3236756A4 (de) | 2018-06-20 |
PE20171151A1 (es) | 2017-08-15 |
AU2015371280A1 (en) | 2017-07-13 |
ES2781250T3 (es) | 2020-08-31 |
BR112017013819B1 (pt) | 2022-02-15 |
CL2017001702A1 (es) | 2018-03-16 |
US20190124961A1 (en) | 2019-05-02 |
CN107249337B (zh) | 2021-05-28 |
EP3236756B1 (de) | 2020-02-26 |
CO2017007333A2 (es) | 2017-10-20 |
US11324240B2 (en) | 2022-05-10 |
WO2016105557A1 (en) | 2016-06-30 |
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Legal Events
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Free format text: STATUS: THE INTERNATIONAL PUBLICATION HAS BEEN MADE |
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