EP3018220B1 - Procédé de fabrication de tuyau en acier à forte teneur en carbone, soudé par résistance électrique, et pièce automobile - Google Patents

Procédé de fabrication de tuyau en acier à forte teneur en carbone, soudé par résistance électrique, et pièce automobile Download PDF

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Publication number
EP3018220B1
EP3018220B1 EP14846979.4A EP14846979A EP3018220B1 EP 3018220 B1 EP3018220 B1 EP 3018220B1 EP 14846979 A EP14846979 A EP 14846979A EP 3018220 B1 EP3018220 B1 EP 3018220B1
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Prior art keywords
electric resistance
less
resistance welded
steel pipe
reducing
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German (de)
English (en)
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EP3018220A4 (fr
EP3018220A1 (fr
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Yoshikazu Kawabata
Kenichi Iwazaki
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JFE Steel Corp
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JFE Steel Corp
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/58Ferrous alloys, e.g. steel alloys containing chromium with nickel with more than 1.5% by weight of manganese
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C37/00Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape
    • B21C37/06Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of tubes or metal hoses; Combined procedures for making tubes, e.g. for making multi-wall tubes
    • B21C37/08Making tubes with welded or soldered seams
    • B21C37/0807Tube treating or manipulating combined with, or specially adapted for use in connection with tube making machines, e.g. drawing-off devices, cutting-off
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C37/00Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape
    • B21C37/06Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of tubes or metal hoses; Combined procedures for making tubes, e.g. for making multi-wall tubes
    • B21C37/30Finishing tubes, e.g. sizing, burnishing
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/10Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of tubular bodies
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/08Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for tubular bodies or pipes
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/06Ferrous alloys, e.g. steel alloys containing aluminium
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/50Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for welded joints

Definitions

  • the present invention relates to a method for producing high carbon electric resistance welded steel pipes or tubes and automotive parts preferable as hollow mechanical parts for automobiles and the like.
  • the present invention especially relates to improvement in reliability in electric resistance welded parts.
  • the present invention relates to a method for producing high carbon electric resistance welded steel pipes or tubes preferable as hollow mechanical parts for automobiles and the like.
  • the present invention especially relates to improvement in reliability in electric resistance welded parts.
  • hollow raw materials have been used as raw materials for automobile parts instead of conventionally used solid materials.
  • the use of electric resistance welded steel pipe or tube of high carbon steel, which is high carbon steel for mechanical structural use, has been considered as the hollow raw materials for parts used for automobiles and the like on which a heat treatment is required.
  • the high carbon steel for mechanical structural becomes to have more carbon content
  • the high carbon steel exhibits tendencies of increasing the strength, degrading the elongation, and developing the segregation.
  • the segregated portion where C, Mn, P, or the like are strongly segregated has hot workability at high temperatures which considerably degraded. This makes the electric resistance welding itself difficult, or a defect such as hot cracking frequently occurs in the electric resistance welded part originated from the segregated portion. This leaves a problem in workability as a steel pipe or tube.
  • Patent Literature 1 discloses an electric resistance welded steel pipe or tube of mechanical structural high carbon steel.
  • the mechanical structural high carbon steel contains, by mass%, C: 0.4 to 0.8%, Si: 0.15 to 0.35%, Mn: 0.3 to 2.0%, P: 0.030% or less, S: 0.035% or less, and Al: 0.035% or less, and further Mo: 0.05 to 0.15% is added.
  • the balance is Fe and incidental impurities.
  • the technique disclosed in Patent Literature 1 involves adding Mo to ensure substantially improving hot workability at 1000°C or more. This completes the steel electric resistance welded steel pipe or tube of mechanical structural high carbon steel excellent in hot workability.
  • Patent Literature 2 discloses a method for producing an electric resistance welded steel pipe or tube of high carbon steel with high workability.
  • the method produces the electric resistance welded steel pipe or tube using a hot-rolled coil of high carbon steel as the raw material.
  • the hot-rolled coil is obtained by hot-rolling a high-carbon steel slab.
  • the high-carbon steel slab contains, by mass%, C: 0.3 to 0.6%, Si: 0.15 to 0.35%, Mn: 0.3 to 1.5%, P: 0.012% or less, S: 0.035% or less, and Al: 0.035% or less.
  • the P concentration at the center segregation part of the high-carbon steel slab on which the continuous cast is performed is adjusted to the low level while satisfying the specific relationship with the C concentration.
  • the hot cracking during the electric resistance welding is restrained, and the yield is improved. According to the technique disclosed in Patent Literature 2, even if a severe treatment such as bulge forming is performed, a possibility of embrittlement crack of the segregated portion is low.
  • the technique improves the workability of the electric resistance welded steel pipe or tube of high carbon steel.
  • Patent Literature 3 discloses the method for producing an electric resistance welded steel pipe or tube of mechanical structural high carbon steel with high workability.
  • the method involves performing continuous cast on the high carbon steel that contains, by mass%, C: 0.30 to 0.60% and P: 0.012% or less, to form high-carbon steel slab whose P concentration at the center segregation part is adjusted to the low level while satisfying the specific relationship with the C concentration.
  • This high-carbon steel slab is hot-rolled to obtain a hot-rolled coil of high carbon steel as the raw material.
  • the hot-rolled coil is formed into a cylindrically-shaped open pipe by the forming roll group. After the forming, preferably, both edges of the open pipe are preheated at the heating width of 2 to 4 mm, which is wider than usual, and at 800 to 1000°C.
  • the electric resistance welding is performed on both edges of the open pipe, and subsequently the electric resistance welded part is air-cooled.
  • the hot cracking during the electric resistance welding is restrained, the yield is improved, and further reduces the hardness of the electric resistance welded part. Accordingly, even if a severe treatment such as the bulge forming is performed, the method can prevent a crack of the welded part, improving the workability of the electric resistance welded steel pipe or tube of high carbon steel.
  • Patent Literature 4 discloses a method for heat treatment of an electric resistance welded part. The method involves performing the electric resistance welding on the electric resistance welded steel pipe or tube with the composition containing C: 0.03 to 0.30%, Si: 0.50 to 3.00%, and Mn: 0.30 to 3.00%. After the welding, the welded part is heated to 800 to 1000°C and then is rapidly cooled from the Ar 3 transformation point or more at 20 to 200°C/s. Thus, the method causes the retained austenite to remain in the electric resistance welded part to enhance the workability of the electric resistance welded part. The technique disclosed in Patent Literature 4 improves the ductility of the electric resistance welded part and produces the electric resistance welded steel pipe or tube that can endure the severe treatment such as hydro forming.
  • EP2578712 discloses a method for manufacturing electric resistance welded steel pipes by cold drawing, normalizing (950°C x 10 min), subsequently forming into a shape of hollow drive shaft, and thereafter hardening by high-frequency heating.
  • the electric resistance welded steel pipe or tube As the raw material for parts, the electric resistance welded steel pipe or tube has been requested to include an electric resistance welded part having reliability higher than the conventional ones.
  • the techniques disclosed in Patent Literatures 1 to 4 have a problem that there is a case occurs which fails to fully satisfy requisite performance for reliability, which is represented by fatigue strength of the electric resistance welded parts.
  • the object of the present invention is to provide a method for producing an electric resistance welded steel pipe or tube of high carbon steel that includes an electric resistance welded part excellent in reliability by solving the problems.
  • excellent in reliability means the case where a defect that affects a fatigue strength is absent from the electric resistance welded part.
  • excellent in reliability means the following situation. Assume that an ultrasonic flaw detection test is conducted under the following conditions. The notch at depth: 0.2 mm ⁇ length: 12.5 mm is employed as a criterion. Section UA in JIS G 0582 "Automated ultrasonic examination of steel pipes and tubes" is applied to the ultrasonic flaw detection method.
  • sensitivity enhancement of 6 decibels is conducted. As the result, the number of defects is 0. Further, a crack does not occur in the torsion fatigue test.
  • the torsion fatigue test is conducted on the outer surface at the torsional stress ⁇ of 350 MPa and the number of repeats of up to two millions.
  • the following treatments are considered for the electric resistance welded steel pipe or tube of high carbon steel. After terminating the electric resistance welding, only the electric resistance welded part is normalized. Afterwards, treatments such as the sizing and the straightening are performed in cold. However, even this method fails to obtain the improvement in sufficient reliability. Although the cause is not apparent at the moment, it is guessed that defects such as shrinkage cavities are more likely to relate to the cause.
  • the ground is considered as follows.
  • the electric resistance welding on the low-carbon steel usually squeezes the welded part with a squeeze roll to prevent the defects such as shrinkage cavities. However, since the electric resistance welding on the high carbon steel is performed at a low melting point, this causes a melting section to remain even after the high carbon steel passes through the squeeze roll. Accordingly, the defects such as shrinkage cavities are likely to occur in some cases.
  • the inventors have concluded that, to further improve the reliability in the electric resistance welded steel pipe or tube of high carbon steel, performing a treatment (reducing) to squash the defects such as shrinkage cavities occurring in the electric resistance welded part is necessary in addition to simply performing a heat treatment on the electric resistance welded part to improve the ductility.
  • the inventors have found the following as effective.
  • the treatment in cold, such as a correction, immediately after the electric resistance welding is minimized as much as possible.
  • the electric resistance welded steel pipe or tube is reheated and hot-reducing rolling is performed in a temperature range of 850°C or more and at a reducing rate of diameter of 10% or more.
  • the use of induction heating for reheating ensures shortening the heating time and ensures restraining decarburization.
  • a high carbon steel sheet (sheet thickness: 7.9 mm) with a composition of containing, by mass%, C: 0.37%, Si: 0.25%, Mn: 1.50%, Al: 0.025%, N: 0.004%, Ti: 0.02%, and B: 0.002% was used as a raw material steel sheet.
  • the high carbon steel sheet was cold-formed into an approximately cylindrical shape.
  • the mutually opposed end surfaces were butted and the electric resistance welding was performed, thereby forming electric resistance welded steel pipes or tubes (outer diameter: 89.1 mm ⁇ ).
  • the electric resistance welded steel pipe or tube was cold-reduced by a sizer rolling mill in cold at the reducing rate of 0 to 1.2%.
  • FIG. 1 illustrates the obtained results.
  • the cold-reducing was performed at the reducing rate of cold-reducing: 0.1%, and after the cold-reducing, the electric resistance welded steel pipe or tube was immediately reheated to 980°C to change the reducing rate of diameter in the temperature range of 850°C or more up to 0 to 35%, thereby performing the hot-reducing rolling.
  • the ultrasonic inspection was conducted on the electric resistance welded parts of the obtained electric resistance welded steel pipes or tubes, and the numbers of defected portions (the number of defects) were measured.
  • the conditions on the ultrasonic inspection were similar to the conditions after the electric resistance welding.
  • FIG. 2 illustrates the obtained results. The following has been found from FIG. 2 .
  • the hot-reducing rolling at the reducing rate of diameter of less than 10% exhibited defects remarkably in the electric resistance welded part.
  • the excess of the reducing rate of diameter of 10% remarkably reduces the defects.
  • the present invention has been completed by adding further examinations based on the knowledge. That is, the gist of the present invention is as follows.
  • the present invention allows obtaining an electric resistance welded steel pipe or tube of high carbon steel that includes an electric resistance welded part where a defect is restrained and that features excellent reliability. As a result, the present invention remarkably improves the reliability in the electric resistance welded steel pipe or tube of high carbon steel.
  • the present invention also improves the reliability in hollow parts formed by using the electric resistance welded steel pipe or tube of high carbon steel as a raw material, for example, various automotive parts, such as front forks, rack bars, drive shafts, tie rods, stator shafts, and cam shafts or the like.
  • the present invention is a method for producing an electric resistance welded steel pipe or tube of high carbon steel.
  • the present invention produces the electric resistance welded steel pipe or tube of high carbon steel employing a high carbon steel sheet as a raw material steel sheet and applying a commonly used method for producing the electric resistance welded steel pipe or tube.
  • the "steel sheet” includes a steel strip.
  • the steel sheet used as the raw material steel sheet in the present invention contains C: 0.30 to 0.60%, Si: 0.05 to 0.50%, Mn: 0.30 to 2.0%, Al: 0.50% or less, and N: 0.0100% or less.
  • the steel sheet used as the raw material steel sheet in the present invention may contain one element or two or more elements selected from the group consisting of Cu: 1.0% or less, Ni: 1.0% or less, Cr: 1.2% or less, Mo: 1.0% or less, and W: 1.5% or less.
  • the steel sheet used as the raw material steel sheet in the present invention may contain one element or, two or more elements selected from the group consisting of Ti: 0.04% or less, Nb: 0.2% or less, and V: 0.2% or less.
  • the steel sheet used as the raw material steel sheet in the present invention may contain B: 0.0005 to 0.0050%.
  • the balance other than the required components and the optional components is Fe and incidental impurities.
  • the sheet thickness of the raw material steel sheet is preferably 8 mm or less.
  • the C is an element which becomes in solid solution state or which is precipitated as carbide or carbonitride to contribute to the increase in strength.
  • the C content is designed to be 0.30% or more.
  • the "desired steel pipe strength” is defined as tensile strength TS: 1200 MPa or more.
  • the excess of the C content of 0.60% degrades the toughness after the heat treatment. For this reason, the C content is limited to the range of 0.30 to 0.60%.
  • Si is an element that serves as a deoxidizing agent.
  • the Si content is designed to be 0.05% or more.
  • the excess of Si content of 0.50% saturates the effect and is economically disadvantageous. Additionally, the excess promotes the generation of inclusions during the electric resistance welding, adversely affecting the soundness of the electric resistance welded part. For this reason, the Si content is limited to the range of 0.05 to 0.50% and is preferably 0.10 to 0.30%.
  • Mn is an element which becomes in solid solution state to increase the strength, contributing to improvement in hardenability.
  • the Mn content is designed to be 0.30% or more. Meanwhile, the excess of the Mn content of 2.0% forms retained austenite, degrading the toughness after tempering. For this reason, the Mn content is limited to the range of 0.30 to 2.0% and is preferably 0.8 to 1.6%.
  • Al is an element that serves as a deoxidizing agent.
  • the Al content is preferably designed to be 0.01% or more.
  • the excess of the Al content of 0.50% saturates the effect. Accordingly, the effect matching the content cannot be expected, resulting in economically disadvantageous. Additionally, this promotes the generation of inclusions during the electric resistance welding, adversely affecting the soundness of the electric resistance welded part.
  • the Al content is limited to the range of 0.50% or less and is preferably 0.02 to 0.04%.
  • N is an effective element to form nitride or carbonitride to ensure the strength after heat treatment (tempering).
  • the N content is preferably designed to be 0.0005% or more.
  • the excess of the N content of 0.0100% forms a coarse nitride, possibly degrading the toughness and a fatigue resistance life. Accordingly, the N content is limited to 0.0100% or less.
  • N containing Ti from the relationship with the Ti content, adjusting N so as to meet the following expression is preferable.
  • N / 14 ⁇ Ti / 47.9 (Here, N and Ti are the contents (mass%) of the respective elements.)
  • the components described above are basic components of the steel sheet, which will be the raw material steel sheet.
  • the electric resistance welded steel pipes or tubes of the invention may as necessary further contain one element or two or more elements selected from the group consisting of Cu: 1.0% or less, Ni: 1.0% or less, Cr: 1.2% or less, Mo: 1.0% or less, and W: 1.5% or less; and/or one element or two or more elements selected from the group consisting of Ti: 0.04% or less, Nb: 0.20% or less, and V: 0.20% or less; and/or B: 0.0005 to 0.0050%.
  • the steel sheet which will be the raw material steel sheet, can contain one element or two or more elements selected from the group consisting of Cu, Ni, Cr, Mo, and W as necessary.
  • Cu is an element which becomes in solid solution state to contribute to the increase in strength and the improvement in hardenability. Furthermore, Cu also improves toughness, delayed fracture resistance, and corrosion fatigue resistance. To obtain such effect, the Cu content is preferably designed to be 0.05% or more. Meanwhile, the excess of the Cu content of 1.0% saturates the effect. Accordingly, the effect matching the content cannot be expected, resulting in economically disadvantageous and deterioration of workability. Accordingly, in the case of containing Cu, Cu is preferably limited to 1.0% or less and is more preferably 0.05 to 0.25%.
  • Ni is an element which becomes in solid solution state to contribute to the increase in strength and the improvement in hardenability. Furthermore, Ni also contributes to the improvements in toughness, delayed fracture resistance, and corrosion fatigue resistance. To obtain such effect, the Ni content is preferably designed to be 0.05% or more. The excess of the Ni content of 1.0% saturates the effect. Accordingly, the effect matching the content cannot be expected, resulting in economically disadvantageous and deterioration of workability. Accordingly, in the case of containing Ni, the Ni content is preferably limited to 1.0% or less and is more preferably 0.05 to 0.25%.
  • the Cr content is preferably designed to be 0.1% or more. Meanwhile, the excess of the Cr content of 1.2% saturates the effect. Accordingly, the effect matching the content cannot be expected, resulting in economically disadvantageous. Additionally, the excess is likely to generate inclusions during the electric resistance welding, adversely affecting the soundness of the electric resistance welded part. Accordingly, in the case of containing Cr, the Cr content is preferably limited to 1.2% or less and is more preferably 0.1 to 0.5%.
  • Mo becomes in solid solution state to contribute to the increase in strength and the improvement in hardenability. Furthermore, Mo generates fine carbides, and by performing precipitation strengthening on Mo, Mo contributes to the increase in strength. To obtain such effect, the Mo content is preferably contained to be 0.01% or more. Meanwhile, the excess of the Mo content of 1.0% saturates the effect. Accordingly, the effect matching the content cannot be expected, resulting in economically disadvantageous. This forms coarse carbides, possibly resulting in deterioration of toughness. Accordingly, in the case of containing Mo, the Mo content is preferably limited to 1.0% or less and is more preferably 0.10 to 0.30%.
  • W also becomes in solid solution state to contribute to the increase in strength and improvement in hardenability.
  • W has an effect of properly balancing the hardness and toughness after the heat treatment.
  • the W content is preferably designed to be 0.01% or more.
  • the excess of the W content of 1.5% saturates the effect. Accordingly, the effect matching the content cannot be expected, resulting in economically disadvantageous.
  • W is preferably limited to 1.5% or less and is more preferably 0.10 to 0.30%.
  • Ti, Nb, and V are all the elements that form fine carbides to contribute to the increase in strength.
  • One element or two or more elements of Ti, Nb, and V can be selected and contained as necessary.
  • Ti is an element that has an effect of ensuring a solid solution B, which is effective to improve the hardenability, by coupling with N and fixing N, in addition to the above-described effects.
  • Ti forms fine nitrides and has an effect of restraining grain coarsening during the heat treatment and the electric resistance welding, contributing to the improvement in toughness.
  • the Ti content is preferably designed to be 0.001% or more. Meanwhile, the excess of the Ti content of 0.04% increases the inclusions, possibly resulting in deterioration of toughness. Accordingly, in the case of containing Ti, the Ti content is preferably limited to 0.04% or less. In the case of containing Ti, it is preferable to contain Ti so as to satisfy the following expression in the relationship with the N content. Ti is more preferable to be 0.01 to 0.03%. N / 14 ⁇ Ti / 47.9
  • Nb has an effect of forming fine carbides during tempering to contribute to the increase in strength. Nb also has an effect of refining a structure after the heat treatment to improve the toughness and delayed fracture resistance. To obtain such effect, the Nb content is preferably designed to be 0.001% or more. Meanwhile, the excess of the Nb content of 0.20% saturates the effect. Accordingly, the effect matching the content cannot be expected, resulting in economically disadvantageous. Accordingly, in the case of containing Nb, Nb is preferably limited to 0.20% or less and is more preferably 0.01 to 0.02%.
  • V forms fine carbides during tempering to contribute to the increase in strength.
  • the V content is preferably designed to be 0.001% or more. Meanwhile, the excess of the V content of 0.20% saturates the effect. Accordingly, the effect matching the content cannot be expected, resulting in economically disadvantageous. Accordingly, in the case of containing V, the V content is preferably limited to 0.20% or less and is more preferably 0.01 to 0.08%.
  • Containing a trace of B improves the hardenability, properly balancing the hardness and toughness after the heat treatment.
  • B strengthens the grain boundary, improving the quenching crack resistance.
  • B can be contained as necessary.
  • the B content is designed to be 0.0005% or more.
  • the excess of the B content of 0.0050% saturates the effect. Accordingly, the effect matching the content cannot be expected, resulting in economically disadvantageous. Additionally, the excess generates coarse B-containing precipitates, resulting in deterioration of the toughness. Accordingly, in the case of containing B, the B content is preferably limited in the range of 0.0005 to 0.0050%.
  • the B content is more preferably 0.002 to 0.003%.
  • the balance other than the above-described components is Fe and incidental impurities.
  • incidental impurities P: 0.020% or less, S: 0.010% or less, and O: 0.005% or less are allowable.
  • the P content is an element that adversely affects the weld crack resistance and the toughness.
  • the P content is preferably reduced within the range of 0.020% or less as much as possible. However, since the excessive reduction of the P content increases the refining cost, the P content is preferably 0.0005% or more and is more preferably 0.010% or less.
  • S is an element present as sulfide inclusions in steel. S adversely affects the workability, the toughness, and the fatigue life; and increases the reheat cracking sensitivity.
  • the S content is preferably reduced as much as possible in the range of 0.010% or less. However, since the excessive reduction increases the refining cost, the S content is preferably designed to be 0.0005% or more. The S content is more preferably 0.001% or less.
  • the O (oxygen) content is preferably reduced as much as possible within the range of 0.005% or less.
  • the O content is more preferably 0.002% or less.
  • the present invention employs the high carbon steel sheet with the above-described composition as the raw material steel sheet.
  • the method for producing the raw material steel sheet is not necessary to be especially limited. All the ordinary methods for producing a hot-rolled steel sheet are applicable. Slitting is performed on the raw material steel sheet so as to provide a predetermined width.
  • the raw material steel sheet is continuously formed into an approximately cylindrical shape in cold preferably using a plurality of forming rolls. After forming, the opposed end surfaces are butted and the electric resistance welding is performed, thereby forming the electric resistance welded steel pipe or tube.
  • the present invention performs the electric resistance welding to form the electric resistance welded steel pipe or tube. After forming, this electric resistance welded steel pipe or tube is cold-reduced to prevent a defect of shape.
  • the use of the sizer rolling mill is preferable for this rolling.
  • the present invention limits the reducing rate of the cold-reducing to 0.8% or less. If the reducing rate exceeds 0.8%, a defect such as a crack occurs in the electric resistance welded part, resulting in degrading the reliability in the electric resistance welded part. In view of this, the reducing rate of the cold-reducing, which is performed after the electric resistance welding, was limited to 0.8% or less.
  • the reducing rate is preferably 0.01 to 0.1%.
  • the cold-reducing be not performed (the reducing rate: 0%) if a defect occurs in the electric resistance welded part. If not performing the cold-reducing, a probability of a failure occurring into a tube geometry is high.
  • the reducing rate is defined as: (perimeter before sizing - perimeter after sizing)/perimeter before sizing ⁇ 100 (%).
  • the electric resistance welded steel pipe or tube on which the cold-reducing has been performed at the reducing rate: 0.8% or less is immediately reheated or is cooled up to a room temperature and then is reheated.
  • the temperature for reheating is not especially limited. In the present invention, the temperature for reheating is preferably a temperature in the temperature range of 850°C or more and at which the hot-reducing rolling can be performed with the reducing rate of diameter of 10% or more, namely, 900 to 1050°C.
  • the hot-reducing rolling is performed to ensure high toughness of the electric resistance welded part with reheating up to an austenite region and squash the defect generated at the electric resistance welded part. This ensures the defect to be harmless, thereby improving the reliability in the electric resistance welded part. If the finish rolling temperature of the hot-reducing rolling is less than 850°C, compression bonding of defects such as shrinkage cavities becomes insufficient. This fails to make the desired defect harmless.
  • the finish rolling temperature of the hot-reducing rolling is preferably 900°C or more.
  • the upper limit of the finish rolling temperature of the hot-reducing rolling is 1000°C at which coarsening of the structure can be prevented.
  • the reducing rate of diameter of the hot-reducing rolling is less than 10% in the temperature range of 850°C or more, the reducing rate of diameter is insufficient, failing to make the desired defect harmless. Accordingly, the reducing rate of diameter of the hot-reducing rolling was limited to 10% or more.
  • the reducing rate of diameter is preferably 30% or more.
  • the upper limit of the reducing rate of diameter of the hot-reducing rolling is determined according to the desired dimensional shape. The reducing rate of diameter is defines as (outer diameter before rolling - outer diameter after rolling)/outer diameter before rolling ⁇ 100 (%).
  • the hot-rolled steel sheets (sheet thickness: 7.8 mm) of high carbon steel with the compositions shown in Table 1 were used as the raw material steel sheets. Slitting was performed on these raw material steel sheets so as to have the predetermined width.
  • the raw material steel sheets were formed into approximately cylindrical-shaped open pipes in cold with a plurality of rolls. Afterwards, the opposed end surfaces were butted and the electric resistance welding was performed to form electric resistance welded steel pipes or tubes (headers) with outer diameter: 89.1 mm ⁇ wall thickness: 7.9 mm. After the electric resistance welding, the cold-reducing at the reducing rate shown in Table 2 was performed on the electric resistance welded steel pipes or tubes using the sizer rolling mill to adjust the electric resistance welded steel pipes or tubes to be a predetermined dimensional shape.
  • the electric resistance welded steel pipes or tubes were immediately heated up to the temperature shown in Table 2 by induction heating means.
  • the hot-reducing rolling was performed under the conditions shown in Table 2 with hot-reducing rolling mill, and after the hot-reducing rolling, air cooling was performed.
  • the electric resistance welded steel pipes or tubes at the outer diameter of 42.7 mm ⁇ wall thickness of 8.0 mm were formed.
  • the ultrasonic flaw detection was performed across the overall length (about 10000 m) of the electric resistance welded parts of the obtained electric resistance welded steel pipes or tubes to examine the presentence/absence of detected defect and the number of defects (counted per the length of 10000 m) .
  • the ultrasonic flaw detection was performed employing the notch at a depth: 0.2 mm ⁇ length: 12.5 mm as a criterion.
  • the sensitivity enhancement of 6 decibels was performed.
  • Test materials were extracted from the obtained electric resistance welded steel pipes or tubes, and a cold-drawing was performed until the outer diameter: 36.7 mm ⁇ wall thickness: 7.2 mm were obtained. After the cold-drawing, a normalizing treatment (air cooling after heated to 945°C) and a quenching treatment (water-cooling and quenching after heated to 950°C) were performed. Torsion fatigue specimens (length: 500 mm) were extracted to conduct a torsion fatigue test.
  • the torsion fatigue test was conducted on ten pieces of specimens as follows.
  • the torsional stress ⁇ applied on the outer surface was set to 350 MPa.
  • the test was conducted up to the number of repeats: two million times. Then, an incidence (%) of crack at the electric resistance welded part was measured. From these results (the results of the ultrasonic flaw detection and the torsion fatigue test), the reliability in the electric resistance welded part was evaluated.
  • the number of defects after the ultrasonic flaw detection was 0 and a crack was not generated by the torsion fatigue test, the result was determined as "Good.”

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Heat Treatment Of Steel (AREA)
  • Heat Treatment Of Articles (AREA)

Claims (4)

  1. Procédé de fabrication d'un tube ou tuyau en acier soudé par résistance électrique constitué d'acier à haute teneur en carbone, comprenant les étapes consistant à :
    former une tôle d'acier de matière première dans une forme approximativement cylindrique par un travail à froid ; et
    ensuite, effectuer un soudage bout à bout par résistance électrique sur des surfaces d'extrémité opposées pour former un tube ou tuyau en acier soudé par résistance électrique,
    dans lequel la tôle d'acier de matière première est une tôle d'acier à haute teneur en carbone qui a une composition constituée de, en % en masse, C : 0,30 à 0,60 %, Si : 0,05 à 0,50 %, Mn : 0,30 à 2,0 %, Al : 0,50 % ou moins et N : 0,0100 % ou moins, optionnellement un élément ou deux éléments ou plus choisis dans le groupe constitué de Cu : 1,0 % ou moins, Ni : 1,0 % ou moins, Cr : 1,2 % ou moins, Mo : 1,0 % ou moins et W : 1,5 % ou moins, optionnellement un élément ou deux éléments ou plus choisis dans le groupe constitué de Ti : 0,04 % ou moins, Nb : 0,2 % ou moins et V : 0,2 % ou moins et optionnellement B : 0,0005 à 0,0050 %, et le reste est Fe et les impuretés accidentelles, et le procédé comprenant en outre les étapes suivantes :
    après le soudage bout à bout par résistance électrique, la réalisation d'une réduction à froid à un taux de réduction de 0,8 % ou moins ;
    ensuite, immédiatement après la réduction à froid, un réchauffage ou un refroidissement et un réchauffage ; et
    la réalisation d'un laminage de réduction à chaud dans une plage de température de 850 °C ou plus à un taux de réduction de diamètre de 10 % ou plus.
  2. Procédé selon la revendication 1, dans lequel le réchauffage est un chauffage par des moyens de chauffage par induction haute fréquence.
  3. Pièce automobile, dans laquelle la pièce automobile est fabriquée en utilisant un tube ou tuyau en acier soudé à haute résistance électrique à haute teneur en carbone en tant que matière première, et le tube ou tuyau en acier soudé par résistance électrique à haute teneur en carbone est fabriqué selon la revendication 1 ou 2.
  4. Pièce automobile selon la revendication 3, dans laquelle la pièce automobile est l'une quelconque parmi une fourche avant, une barre de crémaillère, un arbre d'entraînement, une barre d'accouplement, un arbre de stator et un arbre à cames.
EP14846979.4A 2013-09-25 2014-09-24 Procédé de fabrication de tuyau en acier à forte teneur en carbone, soudé par résistance électrique, et pièce automobile Active EP3018220B1 (fr)

Applications Claiming Priority (2)

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JP2013197819A JP5867474B2 (ja) 2013-09-25 2013-09-25 電縫溶接部の信頼性に優れた高炭素電縫溶接鋼管の製造方法
PCT/JP2014/004882 WO2015045373A1 (fr) 2013-09-25 2014-09-24 Procédé de fabrication de tuyau en acier à forte teneur en carbone, soudé par résistance électrique, et pièce automobile

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101676244B1 (ko) 2015-04-14 2016-11-29 현대자동차주식회사 열변형 저감 스티어링 랙바용 탄소강 조성물 및 이의 제조방법
MX2020013761A (es) * 2018-06-27 2021-03-02 Jfe Steel Corp Tubo de acero soldado por resistencia electrica para la produccion de estabilizador hueco, estabilizador hueco, y metodo para la produccion de los mismos.
CN109252096A (zh) * 2018-10-10 2019-01-22 江阴兴澄特种钢铁有限公司 经济型重载卡车转向器齿条用43MnCrMoB钢及其生产方法
CN113528939A (zh) * 2021-06-10 2021-10-22 江苏利淮钢铁有限公司 一种高性能汽车转向系统中横拉杆接头用钢

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6013024A (ja) * 1983-07-05 1985-01-23 Nippon Steel Corp 高炭素、高マンガン電縫鋼管の製造方法
JPH01108314A (ja) * 1987-10-20 1989-04-25 Nkk Corp 冷間加工性に優れた電縫鋼管用帯鋼の製造方法
JP2596860B2 (ja) * 1991-02-04 1997-04-02 新日本製鐵株式会社 鋼管の円周方向ヤング率が高く圧潰特性に優れた電縫油井管の製造方法
JPH0776409B2 (ja) 1991-02-16 1995-08-16 新日本製鐵株式会社 熱間加工性の優れた機械構造用高炭素鋼および高炭素鋼電縫鋼管
JPH0688129A (ja) * 1992-09-10 1994-03-29 Kawasaki Steel Corp 低残留応力の溶接まま高強度鋼管の製造方法
JPH06179945A (ja) * 1992-12-15 1994-06-28 Nippon Steel Corp 延性の優れたCr−Mo系超高張力電縫鋼管
JPH06256845A (ja) * 1993-03-04 1994-09-13 Nippon Steel Corp 高強度電縫鋼管の製造方法
JPH09279250A (ja) * 1996-04-16 1997-10-28 Sumitomo Metal Ind Ltd 溶接部高靭性高強度電縫鋼管の製造方法
JPH11156433A (ja) 1997-11-27 1999-06-15 Sumitomo Metal Ind Ltd 高加工性高炭素鋼電縫鋼管
JP3232040B2 (ja) 1998-02-10 2001-11-26 住友鋼管株式会社 高加工性機械構造用高炭素鋼電縫鋼管の製造方法
JP4105796B2 (ja) 1998-05-08 2008-06-25 新日本製鐵株式会社 電縫溶接部の加工性を高める電縫溶接部熱処理方法
JP4474729B2 (ja) * 2000-04-27 2010-06-09 Jfeスチール株式会社 ハイドロフォーミング性に優れ、溶接部の軟化が少ない構造用電縫鋼管
JP2004027368A (ja) * 2000-09-20 2004-01-29 Sumitomo Metal Ind Ltd 電縫鋼管およびその製造方法
JP3699394B2 (ja) * 2001-12-26 2005-09-28 住友鋼管株式会社 機械構造用電縫鋼管の熱処理方法
CN101248202A (zh) * 2005-08-22 2008-08-20 新日本制铁株式会社 淬透性、热加工性及疲劳强度优异的高强度厚壁电焊钢管及其制造方法
JP4837601B2 (ja) * 2006-03-09 2011-12-14 新日本製鐵株式会社 中空部品用鋼管及びその製造方法
JP2007262469A (ja) * 2006-03-28 2007-10-11 Jfe Steel Kk 鋼管およびその製造方法
JP5303842B2 (ja) * 2007-02-26 2013-10-02 Jfeスチール株式会社 偏平性に優れた熱処理用電縫溶接鋼管の製造方法
JP5540646B2 (ja) * 2009-10-20 2014-07-02 Jfeスチール株式会社 低降伏比高強度電縫鋼管およびその製造方法
JP5845623B2 (ja) * 2010-05-27 2016-01-20 Jfeスチール株式会社 耐ねじり疲労特性に優れた電縫鋼管及びその製造方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
None *

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Publication number Publication date
EP3018220A4 (fr) 2016-09-14
JP5867474B2 (ja) 2016-02-24
WO2015045373A1 (fr) 2015-04-02
JP2015062920A (ja) 2015-04-09
CN105555976B (zh) 2017-10-10
KR20160055193A (ko) 2016-05-17
EP3018220A1 (fr) 2016-05-11
KR101766293B1 (ko) 2017-08-08
CN105555976A (zh) 2016-05-04

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