EP2734652B1 - Procédé de production d'un élément structural par formage à chaud d'un produit primaire en acier - Google Patents
Procédé de production d'un élément structural par formage à chaud d'un produit primaire en acier Download PDFInfo
- Publication number
- EP2734652B1 EP2734652B1 EP12750986.7A EP12750986A EP2734652B1 EP 2734652 B1 EP2734652 B1 EP 2734652B1 EP 12750986 A EP12750986 A EP 12750986A EP 2734652 B1 EP2734652 B1 EP 2734652B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- forming
- component
- mill bar
- hot
- strength
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 229910000831 Steel Inorganic materials 0.000 title claims description 18
- 239000010959 steel Substances 0.000 title claims description 18
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- 239000002243 precursor Substances 0.000 title description 15
- 238000000034 method Methods 0.000 claims description 27
- 239000011248 coating agent Substances 0.000 claims description 12
- 238000000576 coating method Methods 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 10
- 239000002184 metal Substances 0.000 claims description 6
- 229910052751 metal Inorganic materials 0.000 claims description 6
- 238000005482 strain hardening Methods 0.000 claims description 5
- 230000005855 radiation Effects 0.000 claims description 3
- 230000006698 induction Effects 0.000 claims 1
- 230000009466 transformation Effects 0.000 claims 1
- 239000000463 material Substances 0.000 description 8
- 238000003303 reheating Methods 0.000 description 5
- 238000001816 cooling Methods 0.000 description 3
- 238000005260 corrosion Methods 0.000 description 3
- 230000007797 corrosion Effects 0.000 description 3
- 239000011701 zinc Substances 0.000 description 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- 238000005275 alloying Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000005097 cold rolling Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000005242 forging Methods 0.000 description 2
- 239000010410 layer Substances 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000011241 protective layer Substances 0.000 description 2
- 238000010791 quenching Methods 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 229910000712 Boron steel Inorganic materials 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 238000000137 annealing Methods 0.000 description 1
- 229910001566 austenite Inorganic materials 0.000 description 1
- 230000008033 biological extinction Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- PALQHNLJJQMCIQ-UHFFFAOYSA-N boron;manganese Chemical compound [Mn]#B PALQHNLJJQMCIQ-UHFFFAOYSA-N 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000003618 dip coating Methods 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 230000029142 excretion Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000005246 galvanizing Methods 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 230000001050 lubricating effect Effects 0.000 description 1
- 229910000734 martensite Inorganic materials 0.000 description 1
- 238000011089 mechanical engineering Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
- 229910000859 α-Fe Inorganic materials 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B1/00—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
- B21B1/02—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling heavy work, e.g. ingots, slabs, blooms, or billets, in which the cross-sectional form is unimportant ; Rolling combined with forging or pressing
- B21B1/024—Forging or pressing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B1/00—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
- B21B1/38—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling sheets of limited length, e.g. folded sheets, superimposed sheets, pack rolling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21C—MANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
- B21C1/00—Manufacture of metal sheets, metal wire, metal rods, metal tubes by drawing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D—WORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D22/00—Shaping without cutting, by stamping, spinning, or deep-drawing
- B21D22/20—Deep-drawing
- B21D22/208—Deep-drawing by heating the blank or deep-drawing associated with heat treatment
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D7/00—Modifying the physical properties of iron or steel by deformation
- C21D7/02—Modifying the physical properties of iron or steel by deformation by cold working
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D7/00—Modifying the physical properties of iron or steel by deformation
- C21D7/13—Modifying the physical properties of iron or steel by deformation by hot working
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
- C21D9/08—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for tubular bodies or pipes
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
- C21D9/46—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for sheet metals
- C21D9/48—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for sheet metals deep-drawing sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B1/00—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
- B21B1/38—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling sheets of limited length, e.g. folded sheets, superimposed sheets, pack rolling
- B21B2001/383—Cladded or coated products
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/62—Quenching devices
- C21D1/673—Quenching devices for die quenching
Definitions
- the invention relates to a method for producing a component by hot forming a precursor of steel according to the preamble of claim 1.
- precursors sheet metal plates are understood.
- Such components are mainly used in the automotive industry, but also in mechanical engineering or construction can be used.
- the primary suppliers are trying to meet this need by reducing the wall thickness by providing high-strength and ultra-high-strength steels, while at the same time improving component behavior during production and operation.
- the board is cut to fit the hot forming forming tool. It is also possible to provide the respective workpiece to be formed, or the blank, with a hot-dip coating.
- the application of a metallic coating on the preform to be formed prior to hot forming is advantageous in this method because the coating effectively prevents scaling of the base material and, due to an additional lubricating effect, excessive tool wear.
- thermoformable steels for this application are z. B. the manganese-boron steel "22MnB5" and recently also air hardenable steels according to a still unpublished patent application of the applicant.
- this process requires a great deal of energy by heating the precursor to austenitizing temperature and converting ferrite into austenite, which makes the process expensive and produces significant amounts of CO 2 .
- an additional metallic protective layer or a protective layer Lacquer base required or a considerable rework of the scale-hardened by heating and reshaping.
- a further disadvantage is that to obtain appropriate component strengths after press hardening only convertible steels can be used with a sufficient conversion inertia, which must have correspondingly expensive alloying additions for the structure to be achieved and hardness after forming.
- the object of the invention is to provide a method for producing a component by hot working, which is inexpensive and can be achieved with the comparable or improved properties of the formed component as in the known hot forming by press hardening.
- this object is achieved by a method in which in the course of the process, the heating of the precursor takes place at a temperature below the Ac 1 conversion temperature and the precursor undergoes an increase in strength by cold forming prior to heating.
- the inventive method has opposite to that of DE 601 19 826 T2 known method for producing a component on the advantage that at significantly lower energy consumption for heating the component strength after forming in the Substantially achieved by the previously introduced into the precursor Kaltverfestist. This saves energy and alloying costs.
- the introduced dislocations lead to a considerable increase in strength, which is only insignificantly reduced by the heating process, so that the strength of the component can be adjusted in a targeted manner.
- Experiments have also shown that the ductility of the finished component compared to a component produced by press-hardening could be significantly increased.
- the degree of cold work not less than 3% should not be less than 5% advantageous depending on the material used in the precursor.
- Forming degrees which have been found to be advantageous in the case of hot-rolled strip are between about 3% and about 50% to 80% between conventional temper rolling.
- the invention is easily applicable even at the high degrees of cold rolling.
- cold work grades in the range of 5 to 35% have proven excellent.
- the invention is applicable to precursors of soft to high strength steels, eg. B. with yield strengths of 140 MPa to 1200 MPa, which may be provided with a scale or corrosion inhibiting layer as a metallic coating.
- the metallic coating may contain Zn and / or Mg and / or Al and / or Si.
- surface-finished hot strip can already be used for forming following heating, since the adhesion and the ductility endure half-hot forming with low degrees of deformation.
- the metallic coating is resistant to short-term reheating of the substrate / coating combination (steel strip / coating) below the Ac 1 temperature of the substrate to survive reheating prior to semi-hot forming and actual semi-hot forming.
- the reheating takes place before the half-warm forms by means of radiation, since the efficiency is significantly higher than when heated in an oven or conductive heating and the energy input into the material takes place faster and more effective depending on the surface condition.
- the cold-formed intermediate product is advantageously heated to a temperature of below 720 ° C. in a temperature range of 400-700 ° C. and then shaped into a component.
- the optimum forming temperature depends on the required strength of the component and is preferably between about 540 ° C and 700 ° C.
- a further increase in strength is achieved during the pressing process and the subsequent cooling by the so-called “bake-hardening effect" or by an additional excretion formation, eg. B. VC, allows.
- the increase in strength can be achieved by controlled cooling or subsequent heat treatment (eg paint baking or stress relief annealing).
- a local exceeding of the temperature range of the Semi-warm forming in the austenitizing made in order to make specific local property changes (eg local hardening), which are adapted to the subsequent stresses of the component in combination with the increase in strength of the remaining material.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Thermal Sciences (AREA)
- Physics & Mathematics (AREA)
- Heat Treatment Of Articles (AREA)
- Shaping Metal By Deep-Drawing, Or The Like (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Coating With Molten Metal (AREA)
Claims (10)
- Procédé de production d'un élément structurel par formage à chaud d'une platine d'acier découpée dans un feuillard à chaud, dans lequel la platine est chauffée à la température de formage et est ensuite façonnée,
caractérisé en ce que,
le chauffage se fait à une température en dessous de la température de conversion de Ac1 et la platine subit avant le chauffage une augmentation de résistance par laminage à froid, dans lequel elle est façonnée avec un degré de formage lors du laminage à froid d'au moins 3 %. - Procédé selon la revendication 1,
caractérisé en ce que
la platine est façonnée avec un degré de formage à froid d'au moins 5 %. - Procédé selon la revendication 2,
caractérisé en ce que
la platine est façonnée avec un degré de formage à froid d'au moins 5 à 35 %. - Procédé selon au moins l'une quelconque des revendications 1 à 3,
caractérisé en ce que
le chauffage de la platine se fait à une température inférieure à 720 °C. - Procédé selon la revendication 4,
caractérisé en ce que
le chauffage de la platine se fait dans une plage de températures de 400 à 700 °C. - Procédé selon la revendication 5,
caractérisé en ce que
le chauffage de la platine se fait dans une plage de températures de 540 à 700 °C. - Procédé selon l'une quelconque des revendications 1 à 6,
caractérisé en ce que
la platine est pourvue avant le chauffage d'un revêtement métallique ou de type vernis. - Procédé selon la revendication 7,
caractérisé en ce que
la platine est pourvue avant le formage à froid d'un revêtement métallique ou de type vernis. - Procédé selon la revendication 7 ou 8,
caractérisé en ce que
le revêtement métallique contient du Zn et/ou du Mg et/ou de l'Al et/ou du Si, - Procédé selon au moins l'une quelconque des revendications 1 à 9,
caractérisé en ce que
le chauffage se fait à la température de formage par voie inductive, conductrice ou au moyen d'un rayonnement.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102011108162A DE102011108162B4 (de) | 2011-07-20 | 2011-07-20 | Verfahren zur Herstellung eines Bauteils durch Warmumformen eines Vorproduktes aus Stahl |
PCT/DE2012/000685 WO2013010524A1 (fr) | 2011-07-20 | 2012-07-04 | Procédé de production d'un élément structural par formage à chaud d'un produit primaire en acier |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2734652A1 EP2734652A1 (fr) | 2014-05-28 |
EP2734652B1 true EP2734652B1 (fr) | 2018-12-12 |
Family
ID=46750134
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP12750986.7A Active EP2734652B1 (fr) | 2011-07-20 | 2012-07-04 | Procédé de production d'un élément structural par formage à chaud d'un produit primaire en acier |
Country Status (6)
Country | Link |
---|---|
US (1) | US9943894B2 (fr) |
EP (1) | EP2734652B1 (fr) |
KR (1) | KR102006963B1 (fr) |
DE (1) | DE102011108162B4 (fr) |
RU (1) | RU2581948C2 (fr) |
WO (1) | WO2013010524A1 (fr) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102012006941B4 (de) * | 2012-03-30 | 2013-10-17 | Salzgitter Flachstahl Gmbh | Verfahren zur Herstellung eines Bauteils aus Stahl durch Warmumformen |
US10260124B2 (en) | 2013-05-14 | 2019-04-16 | Nippon Steel & Sumitomo Metal Corporation | Hot-rolled steel sheet and manufacturing method thereof |
DE102013009232A1 (de) | 2013-05-28 | 2014-12-04 | Salzgitter Flachstahl Gmbh | Verfahren zur Herstellung eines Bauteils durch Warmumformen eines Vorproduktes aus Stahl |
AT514422B1 (de) * | 2013-11-05 | 2015-01-15 | Böhler Profil Gmbh | Verfahren zur Herstellung von Schneidmessern |
JP6582892B2 (ja) * | 2015-11-04 | 2019-10-02 | 日本製鉄株式会社 | 鋼材の熱間圧延方法 |
DE102016104800A1 (de) | 2016-03-15 | 2017-09-21 | Salzgitter Flachstahl Gmbh | Verfahren zur Herstellung eines warmumgeformten Stahlbauteils und ein warmumgeformtes Stahlbauteil |
DE102017124724B4 (de) | 2016-10-25 | 2022-01-05 | Koki Technik Transmission Systems Gmbh | Verfahren zur Herstellung einer Schaltgabel |
DE102016222961A1 (de) | 2016-11-22 | 2018-05-24 | Volkswagen Aktiengesellschaft | Verfahren zur Warmumformung von Stahlbauteilen und Fahrzeug |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SU1027240A1 (ru) * | 1982-01-28 | 1983-07-07 | Уфимский авиационный институт им.Орджоникидзе | Способ обработки низколегированной стали |
US4462238A (en) * | 1982-12-20 | 1984-07-31 | Uti Corporation | Method for controlling properties of metals and alloys |
US5454888A (en) * | 1990-10-24 | 1995-10-03 | Consolidated Metal Products, Inc. | Warm forming high-strength steel structural members |
DE4318931C1 (de) * | 1993-06-03 | 1994-12-01 | Mannesmann Ag | Verfahren zur Herstellung von geschweißten Rohren |
FR2807447B1 (fr) * | 2000-04-07 | 2002-10-11 | Usinor | Procede de realisation d'une piece a tres hautes caracteristiques mecaniques, mise en forme par emboutissage, a partir d'une bande de tole d'acier laminee et notamment laminee a chaud et revetue |
PT1660693E (pt) * | 2003-07-29 | 2015-01-05 | Voestalpine Krems Gmbh | Processo de produção de um elemento de perfil temperado |
DE102004028236B3 (de) * | 2004-06-11 | 2005-11-17 | Rolf-Josef Schwartz | Verfahren und Vorrichtung zum Erwärmen von Werkstücken vor der Warm- oder Halbwarmumformung |
US20060169368A1 (en) * | 2004-10-05 | 2006-08-03 | Tenaris Conncections A.G. (A Liechtenstein Corporation) | Low carbon alloy steel tube having ultra high strength and excellent toughness at low temperature and method of manufacturing the same |
ATE434672T1 (de) * | 2005-06-30 | 2009-07-15 | Outokumpu Oy | Martensitischer rostfreier stahl |
RU2389803C2 (ru) * | 2005-10-05 | 2010-05-20 | Ниппон Стил Корпорейшн | Холоднокатаный стальной лист с прекрасной способностью к термическому упрочнению стали при отверждении краски и свойством нестарения при нормальной температуре и способ его производства |
TW200827460A (en) * | 2006-08-11 | 2008-07-01 | Nippon Steel Corp | DR steel sheet and manufacturing method thereof |
DE102008020757A1 (de) * | 2007-04-30 | 2008-11-06 | Volkswagen Ag | Verfahren zur Umformung von Blechwerkstücken aus Eisen-Mangan-Stahl |
WO2009090443A1 (fr) * | 2008-01-15 | 2009-07-23 | Arcelormittal France | Procédé pour fabriquer des produits estampés, et produits estampés préparés à l'aide de celui-ci |
DE102008050315A1 (de) * | 2008-10-02 | 2009-05-20 | Daimler Ag | Umformen von Martensit-haltigen Stahlblechen |
DE102010020373A1 (de) * | 2010-05-12 | 2011-11-17 | Voestalpine Stahl Gmbh | Verfahren zur Herstellung eines Bauteils aus einem Eisen-Mangan-Stahlblech |
DE102011118491A1 (de) * | 2010-11-26 | 2012-05-31 | Salzgitter Flachstahl Gmbh | Verfahren zur Herstellung von Bauteilen durch Warmumformung von Platinen |
-
2011
- 2011-07-20 DE DE102011108162A patent/DE102011108162B4/de not_active Expired - Fee Related
-
2012
- 2012-07-04 EP EP12750986.7A patent/EP2734652B1/fr active Active
- 2012-07-04 RU RU2014106307/02A patent/RU2581948C2/ru active
- 2012-07-04 US US14/234,020 patent/US9943894B2/en active Active
- 2012-07-04 KR KR1020147003144A patent/KR102006963B1/ko active IP Right Grant
- 2012-07-04 WO PCT/DE2012/000685 patent/WO2013010524A1/fr active Application Filing
Also Published As
Publication number | Publication date |
---|---|
KR102006963B1 (ko) | 2019-08-02 |
EP2734652A1 (fr) | 2014-05-28 |
KR20140050041A (ko) | 2014-04-28 |
US9943894B2 (en) | 2018-04-17 |
DE102011108162A1 (de) | 2013-01-24 |
DE102011108162B4 (de) | 2013-02-21 |
RU2581948C2 (ru) | 2016-04-20 |
RU2014106307A (ru) | 2015-08-27 |
US20140290322A1 (en) | 2014-10-02 |
WO2013010524A1 (fr) | 2013-01-24 |
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