EP2718028A2 - Séparateur dynamique pour matériaux pulvérulents - Google Patents
Séparateur dynamique pour matériaux pulvérulentsInfo
- Publication number
- EP2718028A2 EP2718028A2 EP12731079.5A EP12731079A EP2718028A2 EP 2718028 A2 EP2718028 A2 EP 2718028A2 EP 12731079 A EP12731079 A EP 12731079A EP 2718028 A2 EP2718028 A2 EP 2718028A2
- Authority
- EP
- European Patent Office
- Prior art keywords
- selection
- primary
- rotor
- blades
- chamber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
- B07B—SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
- B07B7/00—Selective separation of solid materials carried by, or dispersed in, gas currents
- B07B7/08—Selective separation of solid materials carried by, or dispersed in, gas currents using centrifugal force
- B07B7/083—Selective separation of solid materials carried by, or dispersed in, gas currents using centrifugal force generated by rotating vanes, discs, drums, or brushes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
- B07B—SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
- B07B4/00—Separating solids from solids by subjecting their mixture to gas currents
- B07B4/02—Separating solids from solids by subjecting their mixture to gas currents while the mixtures fall
- B07B4/06—Separating solids from solids by subjecting their mixture to gas currents while the mixtures fall using revolving drums
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
- B07B—SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
- B07B7/00—Selective separation of solid materials carried by, or dispersed in, gas currents
- B07B7/08—Selective separation of solid materials carried by, or dispersed in, gas currents using centrifugal force
Definitions
- the present invention relates to the classification of powders of various grain sizes, in a dynamic separator traversed by a gas flow, generally air.
- the classification of powders or grains into two granulometric fractions can be suspended in air by means of dynamic separators. These separators use to separate the particles according to their size, the forces created by the movement of the air and by the rotary separation members.
- the most recent separator generation is commonly referred to as the "third generation". From a raw product of the same particle size, these separators make it possible to extract more fines, in a selected particle size range, than the apparatuses of previous generations.
- the materials to be separated are powders, often of mineral origin, such as cement, lime or limestone, whose granulometric spectrum can range from a few microns to several millimeters.
- the separation of the particles takes place in a restricted annular volume, called the "selection chamber" 3, delimited on the external side by the fixed louvers 5 of FIG. guiding the selection air 4, and, on the internal side, by the blades of the selection rotor 6.
- the rotor 6 is integral with a vertical shaft 8 which rotates it.
- the material to be selected is generally fed by gravity, through several material inlet chutes 1, distributed at the upper part of the selection chamber 3.
- the material leaving the chutes then falls on an annular distribution plate 2, which centrifugally, in order to distribute it uniformly in the selection chamber 3.
- There are also separators where the material to be selected is brought into the selection chamber, suspended in the air 4, through the guide plates 5.
- Each particle entering the selection chamber 3 is subjected to the resultant of the force of gravity, the centrifugal force initiated by the rotation of the turbine 6 and the resistance force of the selection air 4 introduced through the lamellae 5.
- the lighter particles, called fines penetrate inside the selection chamber 7 where they are entrained by the air towards the outlet duct 9.
- the heavier particles, called rejects fall by gravity into the refusal chamber 10 where they are discharged, by gravity, through the outlet port 1 1.
- the quality of the separation is quantified by parameters derived from a so-called Tromp curve, which makes it possible to know, for a given particle size range, the quantities of fines trapped in the refusals.
- the cutoff point is the dimension for which any particle smaller than this dimension is classified in fines and any particle larger than this dimension is classified in rejections.
- the desired cutoff point is obtained by varying the rotational speed of the selection rotor. Indeed, an increase in this rotation speed increases the component of the centrifugal force, and thus allows smaller particles to compensate for the force of the air flow by the centrifugal force, and thus to have the time to fall by gravity in the refusal chamber 1 0. This therefore reduces the cutoff diameter.
- the separation quality evolves in a non-linear manner, in the opposite direction of the selection chamber concentration criterion, a criterion measuring the ratio between the quantity of material supplying the chamber and the flow of air passing through it.
- concentration criterion measuring the ratio between the quantity of material supplying the chamber and the flow of air passing through it.
- this reduction requires increasing the amount of air passing through the separator and therefore the volume of the selection chamber, which increases the size of the separator and its energy consumption, often reducing the profitability of the separator. investment, with regard to the commercial value of the product to be selected.
- a third-generation separator has only two adjustment parameters which are the rotational speed of the rotor and, in a range generally restricted to +/- 10% of its nominal value, the air flow of ventilation.
- the document ⁇ 0,250,747 discloses a separator having a first separation volume, from which the fines go directly to the outlet. Discharges are conducted to a second separation volume below, which improves the separation quality of coarse rejects by removing more fines.
- this solution does not reduce the necessary air flow, but instead requires to increase to supply the two separation volumes. It does not therefore make it possible to significantly improve the cutoff quality for a given ratio of the mass flow rate of particles to the volume of air.
- EPO 492,062 discloses a separator with two concentric separation volumes, designed to allow the production of at least three material streams of different sizes, with an improved separation quality, but nevertheless insufficient. Such a solution does not reduce the amount of air.
- DD 241 869 discloses a separator with two concentric separation volumes, with rotors rotating in opposite directions to cause a greater difference in speed, and to increase the flow rate of constant size treated material. Such a solution does not, however, improve the quality of separation.
- the present invention proposes a solution making it possible to avoid at least some of the aforementioned drawbacks, and relates to a separator whose internal arrangement of the classification organs makes it possible to split the selection, which leads to a substantial reduction in the final concentration rates, without any increase. the volume of air required.
- a dynamic separator for pulverulent materials such as cement, lime or raw materials, comprising a primary rotor, mobile in rotation about a vertical axis, provided with primary selection blades arranged at its periphery so as to sweep, during the rotation of the primary rotor, a hollow circular cylinder, a secondary rotor provided with secondary selection blades disposed at its periphery, a part of said secondary selection blades being located inside said cylinder, so as to form a secondary selection chamber between said primary selection blades and said secondary selection blades, and guide vanes located outside said cylinder so as to form a primary selection chamber between said guide vanes and said vanes primary selection.
- a primary rotor mobile in rotation about a vertical axis, provided with primary selection blades arranged at its periphery so as to sweep, during the rotation of the primary rotor, a hollow circular cylinder, a secondary rotor provided with secondary selection blades disposed at its periphery, a part of said secondary selection blades being located inside said
- This dynamic separator is particular in that said secondary selection blades and said guide vanes protrude under said cylinder, so as to form, under said cylinder between said guide vanes and said secondary selection blades, a refusal selection chamber, intended to carry out a complementary separation operation against refusals from the primary and secondary selection chambers.
- the secondary selection chamber recovers an air discharged from a part of the refusals, and therefore with a lower concentration of material. For a given airflow, this provides improved performance in terms of separation quality.
- the refusal selection chamber makes it possible to create a second flow of fines, and to improve the overall rate of production of fines. According to other characteristics:
- the secondary rotor may comprise a diaphragm disposed substantially at the lower end of the selection blades of said primary rotor so as to limit the movements of air between a lower part situated under said diaphragm and an upper part situated above said diaphragm of the secondary rotor; this arrangement makes it possible to regulate the relative flow of air between the one which passes through the two primary and secondary selection chambers, and that which passes through the refusal selection chamber; this prevents a majority of air passes through the refusal selection chamber, which would reduce the overall performance by reducing the selection operation of the primary and secondary selection rooms,
- said guide vanes may be inclined by rotation about their vertical axis, so as to orient the flow of incoming air and give it a tangential velocity; this makes it possible to reduce the load on the drive shafts of the primary and secondary rotors,
- the height of the primary rotor selection blades can be between half and three quarters of the height of the secondary rotor selection blades; such a proportion makes it possible to obtain particularly advantageous results,
- At least one of the rotors may be equipped with a means capable of making its speed of rotation adjustable, which makes it possible to adjust the cut-off points of each selection chamber, until an optimum result is obtained,
- said separator may comprise a distribution plate disposed above the primary and secondary rotors adapted to distribute the material input stream under the effect of the centrifugal force,
- said separator may comprise an outlet for the fines situated above the secondary rotor
- said separator may comprise an outlet for the fines situated below the secondary rotor
- the invention also relates to a method of dynamic separation by means of a separator according to the invention fed by a selection gas, for example selection air.
- a selection gas for example selection air. This method is particular in that the angular velocity of the primary rotor is lower than that of the secondary rotor.
- the supply of fresh material can be made by gravity and dispersed, under the effect of centrifugal force, by a distribution plate located above the selection rotors,
- the supply of pulverulent material may be suspended in the selection gas, through the guide plates at the primary and secondary selection chambers, a gas free of pulverulent material being introduced via a conduit of distribution enveloping the guide plates at the level of the refusal selection chamber,
- said selection gas may be a hot gas, so that the pulverulent materials dry during their passage through said separator.
- FIG. 1 represents, in section, a third-generation separator of the state of the art
- FIG. 2 represents, in section, a separator according to a first embodiment of the invention
- FIG. 3 represents, in section, a separator according to a second embodiment of the invention
- FIG. 4 represents one of the possible provisions of the air classification scheme, for a separator supplied with material by gravity, according to FIG. 2.
- FIG. 5 represents one of the possible provisions of the air classification scheme, for a separator supplied with material pneumatically, according to FIG.
- the separator according to the invention is illustrated, in one of the possible configurations, in FIG. 2. It comprises a primary rotor 6 driven by a primary shaft 19 and a secondary rotor 14 coaxial with the primary rotor 6 and driven by a secondary shaft 8.
- the selection blades of the primary rotor 6 define a cylinder which they sweep during the rotation of the rotor.
- the annular volume formed by the space between the guiding lamellae 5 and the selection blades of the primary rotor 6 form the primary selection chamber 3.
- the contiguous annular space delimited by the selection blades of the primary rotor 6 and the rotor secondary 14, constitutes the secondary selection chamber 7, the secondary selection blades being arranged at least partly inside the cylinder described above.
- the primary rotor 6 rotates at a lower speed than the secondary rotor 14, and this speed can, depending on the application, be fixed or variable for an optimization adjustment.
- the selection air 4 enters the separator through the guide vanes 5 with a radial velocity towards the rotation axis of the rotors. Due to the rotation of the primary rotor 6, the selection air 4 takes a tangential speed in addition to its radial velocity. An appropriate inclination of the guide vanes 5 makes it possible to initiate this tangential velocity. As a result, the particles suspended in the selection air 4 are driven by the air flow, towards the inside of the primary rotor 6, and in a rotational movement inducing a centrifugal force.
- the centrifugal force exerted on a particle increases proportionally to its volume, so substantially like the cube of its dimension, while its resistance to the air flow increases proportionally to its area, so substantially like the square of its dimension.
- the smaller particles will move more towards the inside of the rotor, and the larger particles, more sensitive to the centrifugal force, will stay longer in the annular space formed by the selection chamber, and will more often fall down. in the refusal room 1 0.
- the selection air 4 arrives in the secondary selection chamber 7 with a lower amount of material, and the selection work is therefore done on a more weakly concentrated product. Since the speed of rotation of the secondary rotor 14 is higher, the centrifugal force increases, and the cut-off dimension is smaller, making it possible to drive towards the outlet duct 9 a stream of fines that is sufficiently fine because of the lower cutoff. and of very good quality because of the lower concentration of particles in the secondary selection chamber 7.
- the height of the selection blades of the primary rotor 6 are between half and three quarters of the height of the selection blades of the secondary rotor 14.
- the discharges arriving in this chamber are at selected again, at an even lower concentration, resulting from the respective elimination of the fines fractions in the primary and secondary selector chambers 7.
- This refusal selection chamber 12 operates with the speed of rotation of the secondary rotor 14, and so with a cutoff point identical to that of the secondary selection chamber 7.
- the cutoff quality is here also very good, because of the low concentration of material.
- the refusal selection chamber 12 thus makes it possible to drive towards the outlet duct 9 a second stream of fines, which joins the first stream of fines described above.
- the secondary rotor 14 is partitioned, in its lower part, by a diaphragm 1 5 compensating for the least pressure drop experienced by the fraction of the air passing through the rejection selection chamber 12, with respect to the fraction that passes through both primary and secondary rotors. Without this diaphragm 15, most of the incoming air would pass through the refusal selection room 12 where the separation would be extremely well done, but little air would pass through the primary and secondary screening chambers, where there would be would therefore have a much less good separation.
- the diaphragm 15 thus makes it possible to adjust the distribution of the selection air flow 4 between the upper part and the lower part of the secondary rotor 14.
- This diaphragm 15 cuts in two parts, in the direction of the height, the secondary rotor 14
- the upper part 1 3 receives the fines coming from the primary and secondary selections chambers 7, while the lower part 16 receives the residual fines picked up in the rejection selection chamber 1 2.
- the selection air 4 loaded with fines leaves the upper part of the secondary rotor 14, through the outlet duct 9.
- a circular seal 17 prevents the suction of particles fed by the ducts 1, by the air exiting through the duct 9.
- this air exits through a duct placed at the base of the secondary rotor 14.
- Example 1 Class 32.5 cement at 85% passers at 32 ⁇ .
- the separator is fed at 100 t / h of material to be separated at a rate of 2.5 kg / m 3 of air.
- the secondary rejections represent 27.4 t / h, and come s add to 48.5 t / h of primary refusals to give a flow rate of 75.9 t / h which enters the refusal selection chamber 12, with a concentration of 1, 9 kg / m3.
- This concentration makes it possible to recover 13 t / h of fines cut at 28 ⁇ , which adds up to 24.1 t / h, which makes it possible to reach a production of 37.1 t / h, which comes out as a product. finished by the conduit 9.
- Example 2 cement class 52.5 at 93% passers to 32 ⁇
- the separator is supplied with 100 t / h of material to be separated at a rate of 2.5 kg / m 3 of air.
- the secondary refusals represent 31.6 t / h, and come s' add to 48.5 t / h of primary refusals to give a flow of 80.1 t / h which enters the refusal selection chamber 12, with a concentration of 2.0 kg / m3. This concentration makes it possible to recover 1 1, 6 t / h of fine cut at 22 ⁇ , which is added to the 19.9 t / h, which makes it possible to reach a production of 31.5 t / h, which comes out in as a finished product by conduit 9.
- the material to be selected is fed by gravity through the material inlet chutes 1, distributed around the periphery of the primary selection chamber 3.
- the number of these chutes depends on the size of the separator and the flow rate to be treated; it is generally greater than or equal to two, to ensure a distribution as homogeneous as possible.
- the material thus dispersed falls in the primary selection chamber 3 where each grain is subjected to the triple effect of the centrifugal force, generated by the rotation of the primary rotor 6, the thrust of the air selection 4 and gravity.
- a large proportion of grains larger than the primary cut-off point defined by the rotational speed of the primary rotor 6 thus falls in the rejection selection chamber 1 2, whereas the largest proportion of grains of size less than or equal to the point primary cutoff is driven into the secondary selection chamber 7. It follows, according to the invention, a significant decrease in the concentration of material in this chamber, induced by the withdrawal of a fraction of the coarsest elements, during the primary selection.
- the secondary rotor 14 rotating at a higher speed than that of the primary rotor 6, by increasing the centrifugal force, induces a cutoff point of smaller dimension than that created by the primary rotor 6. This results in the elimination of a second quantity of refusals, which in turn fall into the rejection selection chamber 1 2.
- the secondary rotor 14 is provided with a speed variation device which makes it possible to adjust the final cut-off point as a function of the granulometric curve. searched for the finished product.
- all the refusals are subjected to a third selection, in order to extract the residual fines that have been trapped in the rejects during the two previous selections.
- the blades of the secondary rotor 14 extend into the rejection selection chamber 12, and are active in cooperation with the lamellae.
- the blades can be rectilinear, and move with the rotation of the secondary rotor 14 in the same diameter in this area as at the level of the secondary selection chamber 7. But they can also be located further from the axis of the rotors, or closer, according to the needs of the design of the separator, these blades can also be blades independent of those which are active at the secondary selection chamber 7, but fixed on the same secondary rotor 14.
- the concentration levels in the two selection chambers 7 and 1 2 being substantially lower than the initial concentration in the chamber 3, the recovery rates of fines are higher than those of a third generation separator having an equivalent selection air flow 4 and a rotor rotating at the same speed as the secondary rotor 14 of the separator according to the invention (see examples above).
- the separator may not comprise a rejection selection chamber 12. This has the advantage of the lowest concentration in the secondary selection chamber 7. Nevertheless, the results obtained for a concentration of given material are generally worse, because it does not take advantage of the third chamber to recover a complementary flow of fines.
- FIG. 4 shows an example of a ventilation diagram. wherein the fines-laden air is introduced into a filter allowing the separation of these fines, and their recovery 25, under the filter hopper, while the purified air 21 is extracted by a fan
- the invention discloses another variant, illustrated by FIGS. 3 and 5.
- the material 1 to be selected is brought into suspension in the primary fraction 4a of the selection air 4, a fraction which exclusively feeds the selection chambers. 3 and 7.
- the balance of the selection air 4, constituting the secondary fraction 4b entering the rejection selection chamber 1 2, is free of suspended matter, thus avoiding increasing, in this zone, the rate of concentration.
- the separation of the airs at the level of the rotors is done according to the principle illustrated in FIG. 5, where the secondary fraction 4b of the air arrives through an air distribution duct 24, which distributes it through the part 5.
- the secondary fraction 4b of the air comes from the recirculation 22 of a fraction of the purified air 21.
- An introduction point 23 makes it possible to control, if necessary, the temperature of the secondary fraction 4b of the air by introducing an air or a gas at a fixed temperature through the point of introduction 23.
- the separator according to the invention makes it possible to adjust the ratio of the speeds of the primary and secondary rotors, so as to minimize the concentration levels in the selector chambers with a constant air flow rate.
- the selection air 4 can be replaced by a hot combustion gas, allowing the material to be dried during the classification phases.
- the separator according to the invention proposes a single feed point fresh material 1, preferably arranged axially, and is responsible for optimizing this distribution by the plate of split 2, seamlessly for the installer.
- the latter can be oriented in a standard manner, in a vertical plane, of 1 5 degrees in 1 5 degrees, between 45 and 90 degrees, depending on the needs of the installer.
- the installer can choose between an annular inlet, from below, where a cyclonic side entry. This flexibility greatly facilitates the implementation of the separator, especially in existing workshops where there may be strong installation constraints.
- the present invention is particularly intended for the classification of powders, such as those produced in industrial grinding plants of any capacity, and over a wide range of fineness, ranging from a few microns to several mm.
Landscapes
- Combined Means For Separation Of Solids (AREA)
- Cyclones (AREA)
Abstract
Description
Claims
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR1155000A FR2976194B1 (fr) | 2011-06-08 | 2011-06-08 | Separateur dynamique pour materiaux pulverulents |
PCT/FR2012/051194 WO2012168625A2 (fr) | 2011-06-08 | 2012-05-29 | Séparateur dynamique pour matériaux pulvérulents |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2718028A2 true EP2718028A2 (fr) | 2014-04-16 |
EP2718028B1 EP2718028B1 (fr) | 2015-03-11 |
Family
ID=46420395
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP12731079.5A Not-in-force EP2718028B1 (fr) | 2011-06-08 | 2012-05-29 | Séparateur dynamique pour matériaux pulvérulents et méthode de séparation correspondante |
Country Status (5)
Country | Link |
---|---|
US (1) | US9527112B2 (fr) |
EP (1) | EP2718028B1 (fr) |
DK (1) | DK2718028T3 (fr) |
FR (1) | FR2976194B1 (fr) |
WO (1) | WO2012168625A2 (fr) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102013101517A1 (de) * | 2013-02-15 | 2014-08-21 | Thyssenkrupp Resource Technologies Gmbh | Sichter und Verfahren zum Betreiben eines Sichters |
JP6415298B2 (ja) * | 2014-12-16 | 2018-10-31 | 三菱日立パワーシステムズ株式会社 | 回転式分級機および竪型ミル |
FR3085867A1 (fr) * | 2018-09-17 | 2020-03-20 | Bigarren Bizi | Procede et installation de separation aeraulique |
FR3101791B1 (fr) * | 2019-10-15 | 2021-09-17 | Broyeurs Poittemill Ingenierie | Procédé et installation de séparation aéraulique en continu de matériaux particulaires constitués d’un mélange de particules hétérogène à la fois en granulométrie et en densité |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4296864A (en) | 1979-07-17 | 1981-10-27 | Onoda Cement Co., Ltd. | Air classifier |
US4551241A (en) | 1984-02-08 | 1985-11-05 | Sturtevant, Inc. | Particle classifier |
DD241869A1 (de) * | 1985-10-21 | 1987-01-07 | Dessau Zementanlagenbau Veb | Vorrichtung zum sichten feinster koernungen |
DE3545691C1 (de) * | 1985-12-21 | 1987-01-29 | Orenstein & Koppel Ag | Vorrichtung zum Klassieren von staubfoermigen Schuettguetern |
DE3621221A1 (de) | 1986-06-25 | 1988-01-14 | Pfeiffer Fa Christian | Verfahren zur windsichtung und windsichter |
DE3808022A1 (de) * | 1988-03-10 | 1989-09-21 | Krupp Polysius Ag | Sichter |
DE4112018A1 (de) * | 1990-06-08 | 1991-12-12 | Kloeckner Humboldt Deutz Ag | Sichter |
DE4040890C2 (de) * | 1990-12-20 | 1995-03-23 | Krupp Foerdertechnik Gmbh | Windsichter |
US8353408B2 (en) * | 2006-02-24 | 2013-01-15 | Taiheiyo Cement Corporation | Centrifugal air classifier |
DE102008038776B4 (de) * | 2008-08-12 | 2016-07-07 | Loesche Gmbh | Verfahren zur Sichtung eines Mahlgut-Fluid-Gemisches und Mühlensichter |
US8960027B2 (en) * | 2010-04-23 | 2015-02-24 | Nisshin Engineering Inc. | Method for classifying powder |
-
2011
- 2011-06-08 FR FR1155000A patent/FR2976194B1/fr not_active Expired - Fee Related
-
2012
- 2012-05-29 WO PCT/FR2012/051194 patent/WO2012168625A2/fr active Application Filing
- 2012-05-29 DK DK12731079.5T patent/DK2718028T3/en active
- 2012-05-29 US US14/124,917 patent/US9527112B2/en not_active Expired - Fee Related
- 2012-05-29 EP EP12731079.5A patent/EP2718028B1/fr not_active Not-in-force
Non-Patent Citations (1)
Title |
---|
See references of WO2012168625A2 * |
Also Published As
Publication number | Publication date |
---|---|
US9527112B2 (en) | 2016-12-27 |
US20140166554A1 (en) | 2014-06-19 |
WO2012168625A3 (fr) | 2013-02-07 |
FR2976194A1 (fr) | 2012-12-14 |
EP2718028B1 (fr) | 2015-03-11 |
DK2718028T3 (en) | 2015-06-15 |
FR2976194B1 (fr) | 2014-01-10 |
WO2012168625A2 (fr) | 2012-12-13 |
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