EP2385148B1 - Alliage de zinc doté d'une résistance au fluage supérieure - Google Patents
Alliage de zinc doté d'une résistance au fluage supérieure Download PDFInfo
- Publication number
- EP2385148B1 EP2385148B1 EP10161783.5A EP10161783A EP2385148B1 EP 2385148 B1 EP2385148 B1 EP 2385148B1 EP 10161783 A EP10161783 A EP 10161783A EP 2385148 B1 EP2385148 B1 EP 2385148B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- content
- alloy
- zinc
- wire
- creep resistance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 229910001297 Zn alloy Inorganic materials 0.000 title description 5
- 229910045601 alloy Inorganic materials 0.000 claims description 24
- 239000000956 alloy Substances 0.000 claims description 24
- 229910000611 Zinc aluminium Inorganic materials 0.000 claims description 9
- HXFVOUUOTHJFPX-UHFFFAOYSA-N alumane;zinc Chemical compound [AlH3].[Zn] HXFVOUUOTHJFPX-UHFFFAOYSA-N 0.000 claims description 9
- 229910000679 solder Inorganic materials 0.000 claims description 6
- 239000011148 porous material Substances 0.000 claims description 5
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 238000012360 testing method Methods 0.000 description 7
- 229910052782 aluminium Inorganic materials 0.000 description 6
- 239000011777 magnesium Substances 0.000 description 6
- 239000011701 zinc Substances 0.000 description 6
- 239000010949 copper Substances 0.000 description 5
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 4
- 239000011572 manganese Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 238000005476 soldering Methods 0.000 description 3
- 229910052725 zinc Inorganic materials 0.000 description 3
- 238000005275 alloying Methods 0.000 description 2
- 238000005219 brazing Methods 0.000 description 2
- 230000004907 flux Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 230000035882 stress Effects 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910016344 CuSi Inorganic materials 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000001351 cycling effect Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000013011 mating Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 230000008646 thermal stress Effects 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C18/00—Alloys based on zinc
- C22C18/04—Alloys based on zinc with aluminium as the next major constituent
Definitions
- the present invention relates to a zinc aluminum alloy, a wire producible therefrom, and uses of the zinc aluminum alloy of the present invention.
- soldering of the aluminum components is done with the help of solder pastes (metal powder and flux) or by supplying a solid wire which is coated with flux or by means of a filler wire.
- solder pastes metal powder and flux
- a solid wire which is coated with flux or by means of a filler wire.
- the known brazing materials have a low creep resistance. Since the placement of the rings on the pipes and the soldering process takes place on different systems or partially in separate production facilities or separated in time, the attached rings lose their clamping voltage, move or even fall off the pipes.
- EP 1 462 207 A1 discloses a zinc alloy containing 1 to 25 wt .-% aluminum in addition to the usual impurities.
- This alloy may contain up to 500 ppm Mg, up to 500 ppm Cr, up to 2000 ppm Mn, up to 300 ppm Li, up to 4% Cu, up to 50 ppm B, up to 500 ppm Ti and / or up to 1000 ppm Si, in addition to the usual impurities. Rest zinc.
- the zinc alloy is suitable for use in wire form for inert gas welding or inert gas soldering.
- JP 1162740 discloses a zinc aluminum alloy with 10-25% aluminum, 0.05-0.3% copper, 0.005-3.0% each magnesium, silicon and manganese, balance zinc. This alloy is suitable for use in various devices and systems.
- the object of the present invention is to provide an alloy with improved creep resistance in order to provide greater production reliability in the preparation of parts to be soldered.
- the alloy to be created should also have significantly fewer pores (shrinkage porosity) than those of the prior art.
- a Zinc aluminum alloy which has an Al content of 12% - 22%; a Cu content of 0.5% - 1.0%; an Mg content of 0.001% -0.1%, an Mn content of 0.1% -0.5%; has an Si content of 0.1% -0.8% balanced with Zn to 100%.
- the newly developed alloy offers more than 20% better creep resistance compared to standard alloys and allows a secure hold of the rings on the pipe.
- the new alloy shows over that of the prior art ( FIG. 1 ) surprisingly also a very dense structure (see FIG. 2 ).
- a zinc aluminum alloy with an Al content of 18% has proven particularly useful; a Cu content of 0.8%; an Mg content of 0.03%; a Mn content of 0.18%; an Si content of 0.4% and a Zn content of 80.59%.
- the zinc aluminum alloy according to the invention can be converted into a wire in a manner known per se. This is usually done by a multi-stage rolling and drawing process.
- the wire according to the invention has an improved creep behavior and less relaxation under tension.
- DIN EN 10319-1 in the relaxation test under tensile stress at room temperature at a test voltage of 100 MPa, after a test time of 16 h, residual stresses of 40% -60% of the test voltage are determined.
- the wire according to the invention has only a small number of pores and good wettability.
- Example 1 Production of a Wire from the Inventive Alloy
- the alloy is produced by adding the individual alloying elements Al, Cu, Si, Mn, and Mg to a standard alloy with simultaneous stirring.
- master alloys such as for example CuSi for the production of the multicomponent alloy according to the invention is possible.
- Mg is added as the last alloying element.
- the wire is made from the cast strand in a multi-stage rolling and drawing process.
- the improved creep properties of the zinc alloy according to the invention are determined in the relaxation test.
- the samples are subjected to a force of 100 MPa (+/- 2 MPa) at room temperature in the testing machine and the voltage drop in the sample is recorded at a constant elongation over a period of up to 16 hours.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Conductive Materials (AREA)
- Manufacture And Refinement Of Metals (AREA)
Claims (5)
- Alliage de zinc-aluminium ayant une teneur en Al de 12% à 22% ; une teneur en Cu de 0,5% à 1,0% ; une teneur en Mg de 0,001% à 0,1% ; une teneur en Mn de 0,1% à 0,5% ; une teneur en Si de 0,1% à 0,8%, le reste étant du Zn en complément à 100%.
- Alliage de zinc-aluminium selon la revendication 1, ayant une teneur en Al de 18% ; une teneur en Cu de 0,8% ; une teneur en Mg de 0,03% ; une teneur en Mn de 0,18% ; une teneur en Si de 0,4% et une teneur en Zn de 80,59%.
- Fil en alliage selon la revendication 1 ou 2.
- Utilisation de l'alliage de zinc-aluminium selon la revendication 1 pour la fabrication d'un fil à fluage amélioré mesuré selon la norme DIN EN 10319-1.
- Utilisation du fil selon la revendication 3 comme fil à souder ayant une faible porosité et une bonne mouillabilité.
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PL10161783T PL2385148T3 (pl) | 2010-05-03 | 2010-05-03 | Stop cynku o wysokiej odporności na pełzanie |
EP10161783.5A EP2385148B1 (fr) | 2010-05-03 | 2010-05-03 | Alliage de zinc doté d'une résistance au fluage supérieure |
PT101617835T PT2385148T (pt) | 2010-05-03 | 2010-05-03 | Liga de zinco com elevada resistência ao deslizamento |
ES10161783.5T ES2610597T3 (es) | 2010-05-03 | 2010-05-03 | Aleación de cinc con alta resistencia a la fluencia |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP10161783.5A EP2385148B1 (fr) | 2010-05-03 | 2010-05-03 | Alliage de zinc doté d'une résistance au fluage supérieure |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2385148A1 EP2385148A1 (fr) | 2011-11-09 |
EP2385148B1 true EP2385148B1 (fr) | 2016-10-19 |
Family
ID=42610058
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP10161783.5A Active EP2385148B1 (fr) | 2010-05-03 | 2010-05-03 | Alliage de zinc doté d'une résistance au fluage supérieure |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP2385148B1 (fr) |
ES (1) | ES2610597T3 (fr) |
PL (1) | PL2385148T3 (fr) |
PT (1) | PT2385148T (fr) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103882262B (zh) * | 2014-02-26 | 2016-05-25 | 蚌埠市英路光电有限公司 | 一种角阀用锌基高铝合金材料及其制备方法 |
CN107496993B (zh) * | 2017-01-12 | 2022-10-11 | 乐普(北京)医疗器械股份有限公司 | 一种医用可降解植入性金属材料 |
US20210140014A1 (en) | 2017-07-04 | 2021-05-13 | Grillo-Werke Ag | Titanium-containing zinc wrought alloy |
WO2019007909A1 (fr) | 2017-07-04 | 2019-01-10 | Grillo-Werke Ag | Alliage de zinc corroyé présentant une aptitude au revêtement améliorée |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH01162740A (ja) * | 1984-02-14 | 1989-06-27 | Dowa Mining Co Ltd | 亜鉛−アルミニウム系高強度防振合金及びその製造法 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE9101303U1 (de) * | 1991-02-06 | 1991-04-25 | Müller, Ernst | Schweiß- und/oder Lötmaterial |
EP1462207A1 (fr) * | 2003-03-29 | 2004-09-29 | Grillo-Werke AG | Procédé de soudage ou de brasage sous atmosphère protectrice des pièces métalliques avec un matériau d'apport base Zn/Al |
EP1749616A1 (fr) * | 2005-08-05 | 2007-02-07 | Grillo-Werke AG | Procédé pour le soudage ou le brasage à l'arc ou à l'aide d'un faisceau à haute énergie de pièces en métaux identiques ou différents à l'aide d'un métal d'apport à base d'alliage d'étain; Fil à base d'alliage d'étain |
-
2010
- 2010-05-03 EP EP10161783.5A patent/EP2385148B1/fr active Active
- 2010-05-03 PT PT101617835T patent/PT2385148T/pt unknown
- 2010-05-03 PL PL10161783T patent/PL2385148T3/pl unknown
- 2010-05-03 ES ES10161783.5T patent/ES2610597T3/es active Active
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH01162740A (ja) * | 1984-02-14 | 1989-06-27 | Dowa Mining Co Ltd | 亜鉛−アルミニウム系高強度防振合金及びその製造法 |
Also Published As
Publication number | Publication date |
---|---|
EP2385148A1 (fr) | 2011-11-09 |
PT2385148T (pt) | 2017-01-12 |
PL2385148T3 (pl) | 2017-05-31 |
ES2610597T3 (es) | 2017-04-28 |
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