EP2274275A1 - Procédé continu de production d'amides d'acides hydroxycarbocyliques aliphatiques - Google Patents

Procédé continu de production d'amides d'acides hydroxycarbocyliques aliphatiques

Info

Publication number
EP2274275A1
EP2274275A1 EP09728707A EP09728707A EP2274275A1 EP 2274275 A1 EP2274275 A1 EP 2274275A1 EP 09728707 A EP09728707 A EP 09728707A EP 09728707 A EP09728707 A EP 09728707A EP 2274275 A1 EP2274275 A1 EP 2274275A1
Authority
EP
European Patent Office
Prior art keywords
microwave
reaction
acid
atoms
carbon atoms
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP09728707A
Other languages
German (de)
English (en)
Inventor
Matthias Krull
Roman MORSCHHÄUSER
Joachim Hess
Robert Milbradt
Franz-Xaver Scherl
Andreas Wacker
Michael Seebach
Jörg APPEL
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Clariant Finance BVI Ltd
Original Assignee
Clariant Finance BVI Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Clariant Finance BVI Ltd filed Critical Clariant Finance BVI Ltd
Priority to EP20140001820 priority Critical patent/EP2796445A1/fr
Publication of EP2274275A1 publication Critical patent/EP2274275A1/fr
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
    • B01J19/122—Incoherent waves
    • B01J19/126—Microwaves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00139—Controlling the temperature using electromagnetic heating
    • B01J2219/00141—Microwaves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12—Processes employing electromagnetic waves
    • B01J2219/1203—Incoherent waves
    • B01J2219/1206—Microwaves
    • B01J2219/1248—Features relating to the microwave cavity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

L'invention concerne un procédé continu de production d'amidesd'acide hydroxycarboxylique, selon lequel au moins un acide hydroxycarboxylique de formule (I) HO-R3-COOH (I), où R3 désigne un reste hydrocarbure aliphatique éventuellement substitué ayant entre 1 et 100 atomes de carbone est mis à réagir avec au moins une amine du formule (II) HNR1R2 (II) où R1 et R2 désignent indépendamment l'un de l'autre hydrogène ou un reste hydrocarbure ayant entre 1 et 100 atomes de C, pour former un sel d'ammonium. Ce sel d'ammonium est ensuite mis à réagir par exposition à des rayonnements de micro-ondes dans un tube de réaction dont l'axe longitudinal se situe dans le sens de propagation des micro-ones d'un applicateur de micro-ondes monomode, pour former de l'amide d'acide hydroxycarboxylique.
EP09728707A 2008-04-04 2009-03-18 Procédé continu de production d'amides d'acides hydroxycarbocyliques aliphatiques Withdrawn EP2274275A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP20140001820 EP2796445A1 (fr) 2008-04-04 2009-03-18 Procédé continu de production d'amides d'acides hydroxycarboxyliques aliphatiques

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102008017213A DE102008017213B4 (de) 2008-04-04 2008-04-04 Kontinuierliches Verfahren zur Herstellung von Amiden aliphatischer Hydroxycarbonsäuren
PCT/EP2009/001989 WO2009121489A1 (fr) 2008-04-04 2009-03-18 Procédé continu de production d'amides d'acides hydroxycarbocyliques aliphatiques

Related Child Applications (1)

Application Number Title Priority Date Filing Date
EP20140001820 Division EP2796445A1 (fr) 2008-04-04 2009-03-18 Procédé continu de production d'amides d'acides hydroxycarboxyliques aliphatiques

Publications (1)

Publication Number Publication Date
EP2274275A1 true EP2274275A1 (fr) 2011-01-19

Family

ID=40661046

Family Applications (2)

Application Number Title Priority Date Filing Date
EP20140001820 Withdrawn EP2796445A1 (fr) 2008-04-04 2009-03-18 Procédé continu de production d'amides d'acides hydroxycarboxyliques aliphatiques
EP09728707A Withdrawn EP2274275A1 (fr) 2008-04-04 2009-03-18 Procédé continu de production d'amides d'acides hydroxycarbocyliques aliphatiques

Family Applications Before (1)

Application Number Title Priority Date Filing Date
EP20140001820 Withdrawn EP2796445A1 (fr) 2008-04-04 2009-03-18 Procédé continu de production d'amides d'acides hydroxycarboxyliques aliphatiques

Country Status (11)

Country Link
US (1) US20110083957A1 (fr)
EP (2) EP2796445A1 (fr)
KR (1) KR20100135227A (fr)
CN (1) CN101910115B (fr)
AU (1) AU2009231124A1 (fr)
BR (1) BRPI0907149A2 (fr)
CA (1) CA2720347A1 (fr)
DE (1) DE102008017213B4 (fr)
EA (1) EA018156B9 (fr)
MX (1) MX2010010761A (fr)
WO (1) WO2009121489A1 (fr)

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DE102006047619B4 (de) * 2006-10-09 2008-11-13 Clariant International Limited Verfahren zur Herstellung basischer Fettsäureamide
DE102006047617B4 (de) 2006-10-09 2008-11-27 Clariant International Limited Verfahren zur Herstellung basischer (Meth)acrylamide
DE102008017216B4 (de) * 2008-04-04 2013-08-14 Clariant International Ltd. Kontinuierliches Verfahren zur Herstellung von Fettsäureamiden
DE102008017217A1 (de) * 2008-04-04 2009-10-08 Clariant International Ltd. Kontinuierliches Verfahren zur Herstellung von Amiden aromatischer Carbonsäuren
DE102008017218B4 (de) * 2008-04-04 2011-09-22 Clariant International Ltd. Kontinuierliches Verfahren zur Herstellung von Amiden niederer aliphatischer Carbonsäuren
DE102008017219A1 (de) * 2008-04-04 2009-10-08 Clariant International Ltd. Verfahren zur Herstellung von Amiden in Gegenwart von überhitztem Wasser
DE102008017214B4 (de) * 2008-04-04 2012-02-16 Clariant International Limited Kontinuierliches Verfahren zur Herstellung von Fettsäurealkanolamiden
DE102008017215B4 (de) * 2008-04-04 2012-08-09 Clariant International Ltd. Kontinuierliches Verfahren zur Herstellung von Amiden ethylenisch ungesättigter Carbonsäuren
WO2010108814A1 (fr) * 2009-03-26 2010-09-30 Basf Se Procédé de préparation de dialkylamide d'acide n,n'-lactique sous pression
WO2010108817A1 (fr) * 2009-03-26 2010-09-30 Basf Se Procédé de préparation de dialkylamide d'acide n,n'-lactique au moyen de liquides ioniques
DE102009031059A1 (de) 2009-06-30 2011-01-05 Clariant International Ltd. Vorrichtung zur kontinuierlichen Durchführung chemischer Reaktionen bei hohen Temperaturen
DE102009042523B4 (de) 2009-09-22 2012-02-16 Clariant International Ltd. Vorrichtung und Verfahren zur kontinuierlichen Durchführung heterogen katalysierter chemischer Reaktionen bei hohen Temperaturen
DE102009042522A1 (de) 2009-09-22 2011-04-07 Clariant International Ltd. Kontinuierliches Umesterungsverfahren
KR101292329B1 (ko) 2010-05-18 2013-08-01 주식회사 엘지화학 알킬락테이트의 제조방법 및 이를 이용한 락타미드의 제조방법
DE102010056564A1 (de) 2010-12-30 2012-07-05 Clariant International Limited Hydroxylgruppen und Estergruppen tragende Polymere und Verfahren zu ihrer Herstellung
DE102010056565A1 (de) 2010-12-30 2012-07-05 Clariant International Ltd. Verfahren zur Modifizierung Hydroxylgruppen tragender Polymere
DE102010056579A1 (de) * 2010-12-30 2012-07-05 Clariant International Limited Kontinuierliches Verfahren zur Umsetzung Säuregruppen tragender Polymere mit Aminen
CN103435511A (zh) * 2013-04-11 2013-12-11 浙江江山化工股份有限公司 一种n,n-二取代-2-羟基脂肪族酰胺类化合物的合成方法
CN112608244B (zh) * 2020-12-22 2022-11-11 山东华鲁恒升化工股份有限公司 一种新型制备一乙醇胺的方法
CN112495434B (zh) * 2020-12-22 2021-09-28 山东华鲁恒升化工股份有限公司 一种制备乙醇酰胺的新方法及其催化剂的制备

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Also Published As

Publication number Publication date
AU2009231124A1 (en) 2009-10-08
BRPI0907149A2 (pt) 2015-07-07
DE102008017213B4 (de) 2012-08-09
CA2720347A1 (fr) 2009-10-08
CN101910115B (zh) 2014-12-24
MX2010010761A (es) 2010-11-05
CN101910115A (zh) 2010-12-08
EA018156B1 (ru) 2013-05-30
US20110083957A1 (en) 2011-04-14
DE102008017213A1 (de) 2009-10-08
EA201001110A1 (ru) 2010-12-30
KR20100135227A (ko) 2010-12-24
EP2796445A1 (fr) 2014-10-29
EA018156B9 (ru) 2013-11-29
WO2009121489A1 (fr) 2009-10-08

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