EP2172119B1 - Wrapping materials for smoking articles - Google Patents
Wrapping materials for smoking articles Download PDFInfo
- Publication number
- EP2172119B1 EP2172119B1 EP10150360A EP10150360A EP2172119B1 EP 2172119 B1 EP2172119 B1 EP 2172119B1 EP 10150360 A EP10150360 A EP 10150360A EP 10150360 A EP10150360 A EP 10150360A EP 2172119 B1 EP2172119 B1 EP 2172119B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- layer
- wrapping material
- bands
- printed
- layers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000463 material Substances 0.000 title claims description 1000
- 230000000391 smoking effect Effects 0.000 title claims description 30
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 283
- 235000019504 cigarettes Nutrition 0.000 claims description 247
- 239000001856 Ethyl cellulose Substances 0.000 claims description 156
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 claims description 156
- 229920001249 ethyl cellulose Polymers 0.000 claims description 156
- 235000019325 ethyl cellulose Nutrition 0.000 claims description 156
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 138
- 239000000796 flavoring agent Substances 0.000 claims description 38
- 239000000853 adhesive Substances 0.000 claims description 31
- 230000001070 adhesive effect Effects 0.000 claims description 31
- 235000013355 food flavoring agent Nutrition 0.000 claims description 29
- 239000000654 additive Substances 0.000 claims description 24
- CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Chemical group CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 claims description 16
- -1 sodium silicate pentahydrate Chemical class 0.000 claims description 14
- 230000000996 additive effect Effects 0.000 claims description 12
- NVEQFIOZRFFVFW-RGCMKSIDSA-N caryophyllene oxide Chemical compound C=C1CC[C@H]2O[C@]2(C)CC[C@H]2C(C)(C)C[C@@H]21 NVEQFIOZRFFVFW-RGCMKSIDSA-N 0.000 claims description 12
- 229940073505 ethyl vanillin Drugs 0.000 claims description 8
- 229910052751 metal Inorganic materials 0.000 claims description 7
- 239000002184 metal Substances 0.000 claims description 7
- NVEQFIOZRFFVFW-UHFFFAOYSA-N 9-epi-beta-caryophyllene oxide Natural products C=C1CCC2OC2(C)CCC2C(C)(C)CC21 NVEQFIOZRFFVFW-UHFFFAOYSA-N 0.000 claims description 6
- RSYBQKUNBFFNDO-UHFFFAOYSA-N caryophyllene oxide Natural products CC1(C)CC2C(=C)CCC3OC3(C)CCC12C RSYBQKUNBFFNDO-UHFFFAOYSA-N 0.000 claims description 6
- PETRWTHZSKVLRE-UHFFFAOYSA-N 2-Methoxy-4-methylphenol Chemical compound COC1=CC(C)=CC=C1O PETRWTHZSKVLRE-UHFFFAOYSA-N 0.000 claims description 4
- CFAKWWQIUFSQFU-UHFFFAOYSA-N 2-hydroxy-3-methylcyclopent-2-en-1-one Chemical compound CC1=C(O)C(=O)CC1 CFAKWWQIUFSQFU-UHFFFAOYSA-N 0.000 claims description 4
- IUFQZPBIRYFPFD-UHFFFAOYSA-N 5-ethyl-3-hydroxy-4-methyl-2(5H)-furanone Chemical compound CCC1OC(=O)C(O)=C1C IUFQZPBIRYFPFD-UHFFFAOYSA-N 0.000 claims description 4
- 229920001202 Inulin Polymers 0.000 claims description 4
- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 claims description 4
- 229940029339 inulin Drugs 0.000 claims description 4
- XPJSGGHNJMXYKR-UHFFFAOYSA-L magnesium;sulfate;decahydrate Chemical compound O.O.O.O.O.O.O.O.O.O.[Mg+2].[O-]S([O-])(=O)=O XPJSGGHNJMXYKR-UHFFFAOYSA-L 0.000 claims description 4
- OSWPMRLSEDHDFF-UHFFFAOYSA-N methyl salicylate Chemical compound COC(=O)C1=CC=CC=C1O OSWPMRLSEDHDFF-UHFFFAOYSA-N 0.000 claims description 4
- PHXATPHONSXBIL-UHFFFAOYSA-N xi-gamma-Undecalactone Chemical compound CCCCCCCC1CCC(=O)O1 PHXATPHONSXBIL-UHFFFAOYSA-N 0.000 claims description 4
- SATCULPHIDQDRE-UHFFFAOYSA-N piperonal Chemical compound O=CC1=CC=C2OCOC2=C1 SATCULPHIDQDRE-UHFFFAOYSA-N 0.000 claims description 3
- YOMSJEATGXXYPX-UHFFFAOYSA-N 2-methoxy-4-vinylphenol Chemical compound COC1=CC(C=C)=CC=C1O YOMSJEATGXXYPX-UHFFFAOYSA-N 0.000 claims description 2
- 239000004115 Sodium Silicate Substances 0.000 claims description 2
- 229910021538 borax Inorganic materials 0.000 claims description 2
- 239000010633 clary sage oil Substances 0.000 claims description 2
- PHXATPHONSXBIL-JTQLQIEISA-N gamma-Undecalactone Natural products CCCCCCC[C@H]1CCC(=O)O1 PHXATPHONSXBIL-JTQLQIEISA-N 0.000 claims description 2
- 229940020436 gamma-undecalactone Drugs 0.000 claims description 2
- WRUGWIBCXHJTDG-UHFFFAOYSA-L magnesium sulfate heptahydrate Chemical compound O.O.O.O.O.O.O.[Mg+2].[O-]S([O-])(=O)=O WRUGWIBCXHJTDG-UHFFFAOYSA-L 0.000 claims description 2
- 229940061634 magnesium sulfate heptahydrate Drugs 0.000 claims description 2
- 229960001047 methyl salicylate Drugs 0.000 claims description 2
- 239000010671 sandalwood oil Substances 0.000 claims description 2
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 2
- RSIJVJUOQBWMIM-UHFFFAOYSA-L sodium sulfate decahydrate Chemical compound O.O.O.O.O.O.O.O.O.O.[Na+].[Na+].[O-]S([O-])(=O)=O RSIJVJUOQBWMIM-UHFFFAOYSA-L 0.000 claims description 2
- 239000004328 sodium tetraborate Substances 0.000 claims description 2
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 2
- PARHMNZPOUVEIQ-UHFFFAOYSA-N 1-(4-hydroxyphenyl)butan-2-one Chemical compound CCC(=O)CC1=CC=C(O)C=C1 PARHMNZPOUVEIQ-UHFFFAOYSA-N 0.000 claims 1
- 239000010410 layer Substances 0.000 description 1113
- 239000000203 mixture Substances 0.000 description 543
- 238000009472 formulation Methods 0.000 description 460
- 238000007639 printing Methods 0.000 description 358
- 239000002585 base Substances 0.000 description 172
- 239000008199 coating composition Substances 0.000 description 156
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 112
- 238000000576 coating method Methods 0.000 description 111
- 241000208125 Nicotiana Species 0.000 description 102
- 239000011248 coating agent Substances 0.000 description 84
- 239000000945 filler Substances 0.000 description 78
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 67
- 239000002904 solvent Substances 0.000 description 65
- 238000004519 manufacturing process Methods 0.000 description 64
- 230000003287 optical effect Effects 0.000 description 50
- 239000000020 Nitrocellulose Substances 0.000 description 48
- 229920001220 nitrocellulos Polymers 0.000 description 48
- 239000000126 substance Substances 0.000 description 46
- 238000000034 method Methods 0.000 description 45
- 230000008033 biological extinction Effects 0.000 description 43
- 229920002472 Starch Polymers 0.000 description 37
- 235000019698 starch Nutrition 0.000 description 37
- 239000003795 chemical substances by application Substances 0.000 description 35
- 239000002245 particle Substances 0.000 description 35
- 238000012360 testing method Methods 0.000 description 32
- 239000008107 starch Substances 0.000 description 31
- 239000007788 liquid Substances 0.000 description 30
- 235000002639 sodium chloride Nutrition 0.000 description 30
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical compound CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 description 30
- JMMWKPVZQRWMSS-UHFFFAOYSA-N isopropanol acetate Natural products CC(C)OC(C)=O JMMWKPVZQRWMSS-UHFFFAOYSA-N 0.000 description 28
- 229940011051 isopropyl acetate Drugs 0.000 description 28
- GWYFCOCPABKNJV-UHFFFAOYSA-M isovalerate Chemical compound CC(C)CC([O-])=O GWYFCOCPABKNJV-UHFFFAOYSA-M 0.000 description 28
- 239000004372 Polyvinyl alcohol Substances 0.000 description 26
- 229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 description 26
- 229920002451 polyvinyl alcohol Polymers 0.000 description 26
- 235000019422 polyvinyl alcohol Nutrition 0.000 description 26
- AIXZBGVLNVRQSS-UHFFFAOYSA-N 5-tert-butyl-2-[5-(5-tert-butyl-1,3-benzoxazol-2-yl)thiophen-2-yl]-1,3-benzoxazole Chemical compound CC(C)(C)C1=CC=C2OC(C3=CC=C(S3)C=3OC4=CC=C(C=C4N=3)C(C)(C)C)=NC2=C1 AIXZBGVLNVRQSS-UHFFFAOYSA-N 0.000 description 23
- 239000000976 ink Substances 0.000 description 23
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 22
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 21
- 239000003125 aqueous solvent Substances 0.000 description 21
- 239000005038 ethylene vinyl acetate Substances 0.000 description 21
- 239000000080 wetting agent Substances 0.000 description 20
- 241000282836 Camelus dromedarius Species 0.000 description 19
- 239000000835 fiber Substances 0.000 description 18
- 150000003839 salts Chemical class 0.000 description 17
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 16
- 239000000758 substrate Substances 0.000 description 16
- 239000001087 glyceryl triacetate Substances 0.000 description 15
- 235000013773 glyceryl triacetate Nutrition 0.000 description 15
- 229960002622 triacetin Drugs 0.000 description 15
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 14
- 235000010445 lecithin Nutrition 0.000 description 14
- 239000000787 lecithin Substances 0.000 description 14
- 229940067606 lecithin Drugs 0.000 description 14
- 239000000779 smoke Substances 0.000 description 14
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 12
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 12
- 239000001509 sodium citrate Substances 0.000 description 12
- 235000011083 sodium citrates Nutrition 0.000 description 12
- 235000010493 xanthan gum Nutrition 0.000 description 12
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- 229940082509 xanthan gum Drugs 0.000 description 12
- DQXBYHZEEUGOBF-UHFFFAOYSA-N but-3-enoic acid;ethene Chemical compound C=C.OC(=O)CC=C DQXBYHZEEUGOBF-UHFFFAOYSA-N 0.000 description 11
- 239000000284 extract Substances 0.000 description 11
- 239000002657 fibrous material Substances 0.000 description 11
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 11
- 239000000347 magnesium hydroxide Substances 0.000 description 11
- 229910001862 magnesium hydroxide Inorganic materials 0.000 description 11
- 230000008569 process Effects 0.000 description 11
- 239000011780 sodium chloride Substances 0.000 description 11
- 244000061176 Nicotiana tabacum Species 0.000 description 10
- 239000011247 coating layer Substances 0.000 description 10
- 238000001514 detection method Methods 0.000 description 10
- 235000019634 flavors Nutrition 0.000 description 10
- 239000004615 ingredient Substances 0.000 description 10
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 10
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- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 description 2
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Images
Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/02—Cigars; Cigarettes with special covers
- A24D1/025—Cigars; Cigarettes with special covers the covers having material applied to defined areas, e.g. bands for reducing the ignition propensity
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/66—Coatings characterised by a special visual effect, e.g. patterned, textured
- D21H19/68—Coatings characterised by a special visual effect, e.g. patterned, textured uneven, broken, discontinuous
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H11/00—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
- D21H11/12—Pulp from non-woody plants or crops, e.g. cotton, flax, straw, bagasse
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/303,639 US6976493B2 (en) | 2002-11-25 | 2002-11-25 | Wrapping materials for smoking articles |
US10/303,646 US6929013B2 (en) | 2001-08-14 | 2002-11-25 | Wrapping materials for smoking articles |
US10/303,648 US6997190B2 (en) | 2002-11-25 | 2002-11-25 | Wrapping materials for smoking articles |
US10/686,558 US7237559B2 (en) | 2001-08-14 | 2003-10-15 | Wrapping materials for smoking articles |
EP03783753A EP1569531B1 (en) | 2002-11-25 | 2003-11-25 | Wrapping materials for smoking articles |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP03783753.1 Division | 2003-11-25 |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2172119A1 EP2172119A1 (en) | 2010-04-07 |
EP2172119B1 true EP2172119B1 (en) | 2011-09-28 |
Family
ID=32398249
Family Applications (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP10150360A Expired - Lifetime EP2172119B1 (en) | 2002-11-25 | 2003-11-25 | Wrapping materials for smoking articles |
EP03783753A Expired - Lifetime EP1569531B1 (en) | 2002-11-25 | 2003-11-25 | Wrapping materials for smoking articles |
EP09179763A Expired - Lifetime EP2160951B1 (en) | 2002-11-25 | 2003-11-25 | Wrapping materials for smoking articles |
Family Applications After (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP03783753A Expired - Lifetime EP1569531B1 (en) | 2002-11-25 | 2003-11-25 | Wrapping materials for smoking articles |
EP09179763A Expired - Lifetime EP2160951B1 (en) | 2002-11-25 | 2003-11-25 | Wrapping materials for smoking articles |
Country Status (5)
Country | Link |
---|---|
EP (3) | EP2172119B1 (ja) |
JP (1) | JP4606170B2 (ja) |
AU (1) | AU2003291158A1 (ja) |
CA (1) | CA2506302A1 (ja) |
WO (1) | WO2004047572A1 (ja) |
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- 2003-11-25 EP EP03783753A patent/EP1569531B1/en not_active Expired - Lifetime
- 2003-11-25 WO PCT/US2003/037462 patent/WO2004047572A1/en active Application Filing
- 2003-11-25 AU AU2003291158A patent/AU2003291158A1/en not_active Abandoned
- 2003-11-25 EP EP09179763A patent/EP2160951B1/en not_active Expired - Lifetime
- 2003-11-25 JP JP2004555636A patent/JP4606170B2/ja not_active Expired - Lifetime
- 2003-11-25 CA CA002506302A patent/CA2506302A1/en not_active Abandoned
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EP2172119A1 (en) | 2010-04-07 |
WO2004047572A1 (en) | 2004-06-10 |
EP1569531A1 (en) | 2005-09-07 |
JP2006517391A (ja) | 2006-07-27 |
EP1569531B1 (en) | 2010-07-21 |
EP2160951A1 (en) | 2010-03-10 |
AU2003291158A1 (en) | 2004-06-18 |
EP1569531A4 (en) | 2009-07-15 |
CA2506302A1 (en) | 2004-06-10 |
EP2160951B1 (en) | 2012-03-07 |
JP4606170B2 (ja) | 2011-01-05 |
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