EP1554421B1 - Verfahren und vorrichtung zur herstellung von vliesstoffen unter verminderung der bewegungsgeschwindigkeit der verdichteten faserbahn - Google Patents
Verfahren und vorrichtung zur herstellung von vliesstoffen unter verminderung der bewegungsgeschwindigkeit der verdichteten faserbahn Download PDFInfo
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- EP1554421B1 EP1554421B1 EP03775475A EP03775475A EP1554421B1 EP 1554421 B1 EP1554421 B1 EP 1554421B1 EP 03775475 A EP03775475 A EP 03775475A EP 03775475 A EP03775475 A EP 03775475A EP 1554421 B1 EP1554421 B1 EP 1554421B1
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- Prior art keywords
- web
- speed
- compacting
- conveyor
- machine
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- 238000000034 method Methods 0.000 title claims abstract description 18
- 239000004745 nonwoven fabric Substances 0.000 title claims abstract description 12
- 238000006073 displacement reaction Methods 0.000 title claims description 7
- 238000007596 consolidation process Methods 0.000 claims abstract description 25
- 239000000126 substance Substances 0.000 claims abstract description 4
- 239000000835 fiber Substances 0.000 claims description 25
- 238000009736 wetting Methods 0.000 claims description 9
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 239000012943 hotmelt Substances 0.000 claims description 2
- 239000011368 organic material Substances 0.000 claims description 2
- 238000005056 compaction Methods 0.000 abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 21
- 239000000463 material Substances 0.000 abstract description 4
- 238000009950 felting Methods 0.000 abstract 1
- 229920000728 polyester Polymers 0.000 description 9
- 239000004744 fabric Substances 0.000 description 4
- 238000009434 installation Methods 0.000 description 4
- 238000009960 carding Methods 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 230000035699 permeability Effects 0.000 description 3
- 230000001360 synchronised effect Effects 0.000 description 3
- 230000001143 conditioned effect Effects 0.000 description 2
- 230000001788 irregular Effects 0.000 description 2
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 2
- -1 polypropylene Polymers 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 238000004804 winding Methods 0.000 description 2
- 241001644893 Entandrophragma utile Species 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 229920000297 Rayon Polymers 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000032798 delamination Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000004746 geotextile Substances 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 239000000700 radioactive tracer Substances 0.000 description 1
- 230000000284 resting effect Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
Images
Classifications
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H18/00—Needling machines
- D04H18/04—Needling machines with water jets
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/44—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
- D04H1/46—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
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- D—TEXTILES; PAPER
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- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/44—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
- D04H1/46—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
- D04H1/492—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres by fluid jet
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/54—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by welding together the fibres, e.g. by partially melting or dissolving
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/58—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives
- D04H1/64—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives the bonding agent being applied in wet state, e.g. chemical agents in dispersions or solutions
- D04H1/655—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives the bonding agent being applied in wet state, e.g. chemical agents in dispersions or solutions characterised by the apparatus for applying bonding agents
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/70—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres
- D04H1/72—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged
- D04H1/732—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged by fluid current, e.g. air-lay
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/70—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres
- D04H1/74—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being orientated, e.g. in parallel (anisotropic fleeces)
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/08—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating
- D04H3/10—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between yarns or filaments made mechanically
- D04H3/105—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between yarns or filaments made mechanically by needling
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/08—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating
- D04H3/10—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between yarns or filaments made mechanically
- D04H3/11—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between yarns or filaments made mechanically by fluid jet
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/08—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating
- D04H3/12—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with filaments or yarns secured together by chemical or thermo-activatable bonding agents, e.g. adhesives, applied or incorporated in liquid or solid form
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/08—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating
- D04H3/14—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between thermoplastic yarns or filaments produced by welding
Definitions
- the present invention relates to processes and machines for the production of nonwovens, consisting of fibers or filaments made of an organic material, in particular fibers or natural, synthetic or artificial textile filaments.
- the fibers or filaments may be in particular polypropylene, polyester, or another plastic material and mixtures thereof.
- a process for producing a nonwoven is already known in which a web in displacement of filaments or fibers at a compaction station is compacted in the direction of thickness.
- the compaction is obtained by passing the web moving in the nip between two moving elements moving in the same direction.
- One of the movable elements may be a conveyor or a cylinder and the other may also be a conveyor or a cylinder.
- Downstream of the compaction station the compacted tablecloth is consolidated into a consolidated sheet at a consolidation station.
- the consolidation can be carried out by mechanical needling, by chemical or thermal bonding. Hydraulic binding is preferably used by jets of water.
- the nonwovens obtained have a ratio of a property in the long direction, and in particular of the tensile strength, to the same property in the cross direction, which is much greater than one.
- the long direction is defined by the direction in which the web moves when it is sent to the compaction station, while the cross direction is the direction perpendicular to this direction in the plane of the web.
- it would be desirable to reduce the ratio of a non-woven property. in the long direction to this property in the transverse direction whereas the production processes of veils, sheets and webs preferentially orient the fibers or filaments in the long direction, while having a high speed of displacement and synonymous with great productivity.
- the invention provides for this by a process for producing a nonwoven in which a web of filaments or fibers is compacted in the direction of thickness at a point on its path of travel. a compacting station, and then consolidates the compacted web into a consolidated web at a consolidation station downstream, in the direction of travel of the web, the compaction station. According to the invention, the speed of movement of the web is reduced at the very point of its travel path where it is compacted.
- the document GB 891143 discloses a method and a production machine according to the preambles of claims 1 and 8.
- the property whose ratio is changed in the process according to the invention is preferably tensile strength, maximum at break, but it is also the tensile elongation or other tensile property. It has also been found that the process according to the invention makes it possible to improve the resistance of nonwovens to delamination.
- the web is wetted at the compaction station or just downstream from this station.
- wetting the deformation of the fibers of the web and thus retains the relationship between the property of the nonwoven in the long direction and the property of the nonwoven in the cross direction, is obtained at the compaction station, at the exit thereof while, without the fixation by wetting, the fibers tend, after they are no longer compacted to resume, at least in part, their initial orientation.
- anchorage takes place before the arrival of the sheet at the consolidation station.
- the sheet may be wetted by means of a hydraulic injector arranged in such a way that the jets extend substantially over the entire width of the sheet and by sending jets whose pressure is between 1 and 50 bars. .
- this attachment may already have a certain consolidation effect, that is to say entanglement of the fibers. In some cases, it is wetted with a liquid other than pure water.
- the compacted sheet is then consolidated into a consolidated sheet at the consolidation station, which is downstream in the direction of movement of the sheet of the compaction station and downstream from the point where the wetting of the sheet is carried out, if necessary.
- the consolidation can be carried out by any known means, in particular by mechanical needling using metal needles, by chemical bonding, by thermal bonding using hot-melt fibers and by means of impregnation means such as scarf or spray or foam spray with a binder. But it is much preferred to carry out the consolidation by a hydraulic linkage by jets of water, if necessary also combined with other means of binding. Hydraulic binding can be carried out by jets of water of a diameter of between 50 and 250 microns at pressures of between 10 and 1000 bar.
- the web is preferably a web of filaments from a machine operating in the melt or a web of fibers from a nonwoven card; it can also come from a machine operating aeraulic way called "air ugly” or a lapper-stretcher.
- the invention applies in particular for surface masses of 0 to 500 g / m 2 and preferably 20 to 300 g / m 2 of the web.
- the invention makes it possible in particular to produce filtration products, geotextiles, agrotextiles in civil engineering and construction, in the automobile, furniture, clothing, in medical applications, in roof seals, products soundproofing and thermal insulation, wiping products that are dry or impregnated for cleaning and hygiene.
- the invention also relates to a machine for producing a nonwoven comprising a first element for sending a sheet to means intended to compress it in the direction of the thickness, characterized in that said means are also means for reducing the speed of movement of the web to the point where it is compacted by the compacting means.
- the first element is preferably a conveyor, but it can also be a cylinder fed by a conveyor.
- the compacting means are formed by the formation of a pinch point between the first element and another mobile element and the reduction in the speed of movement of the web is achieved by giving the other moving element a linear velocity less than that of the first element.
- the other movable element may be a second conveyor or a second cylinder.
- the nip preferably extends over the entire width of the web, relating to a whole generatrix of the pinch cylinder.
- the machine comprises means for wetting the web while it is compacted or has just been compacted and before it arrives at consolidation means.
- the consolidation means are arranged so as to consolidate the sheet while it passes over the other mobile element, since the consolidation is better as the speed of passage of the sheet to the consolidation station is smaller .
- the invention relates to the use of a method or a machine according to the invention for reducing the ratio of a property of a nonwoven in the long direction to this property in the transverse direction and more particularly for to decrease the ratio of the tensile strength at break of a nonwoven in the long direction to this tensile strength at break in the cross direction.
- the machine represented in figure 1 comprises a conveyor comprising a frame 1 resting by four feet 2 on the ground S.
- This frame carries three return rollers 3, a tensioning roller 4 and a guide roller 5 of a conveyor belt 6 permeable to water.
- Above the upper strand 7 of the conveyor is mounted a cylinder 8 of horizontal axis perpendicular to the direction of movement of the strand 7, while at the vertical of the cylinder 8 and below the strand 7 is mounted an injector 9 anchorage.
- the distance between the strand 7 and the lowest point of the cylinder 8 is so small that when a sheet is conveyed and passes on the strand 7, it comes into the nip between the strand 7 and the cylinder 8 and is compacted.
- the sheet then passes along the cylinder 8 to arrive in front of two jets consolidation 10 by water jets.
- the cylinder 8 is a hollow cylinder which rotates counterclockwise while the web passing on the strand 7 goes from left to right in the drawing.
- the cylinder 8 comprises a quadrant 8a between 4 o'clock and 6 o'clock, subjected to a depression so that the ply is pressed against the cylinder 8 from the exit of the nip to the injectors 10.
- the machine shown is preferred when the thickness of the web is greater than 50 mm. It has the same elements as the machine of the figure 1 but, in addition, an additional conveyor carried by four feet 11 and brackets 12.
- the conveyor has a guide roller 13, a tensioner roller 14, a return roller 15 and the conveyor belt 15 permeable passes around of the cylinder 8 and in the nip between the cylinder 8 and the belt 7.
- a conveyor 18 having return rollers 19, a tensioner roll and a guide roll 21.
- the conveyor further has a return roller 22 which is in contact with the upper strand 7 of the conveyor belt of the first conveyor and which is arranged on this strand upstream of an injector 23 for wetting a mat that reaches the mat 7 going from left to right in the figure.
- the roller 17 is just downstream of the injector 23 and is arranged in such a way with respect to the roller 22 that it holds the strand 7 in close contact with the lower strand of the belt 24 which passes on the upper conveyor by turning counterclockwise.
- the web is thus compressed between the upper strand 7 and the lower strand of the carpet 24, is wetted at the wetting point 23 and then goes to a preliminary consolidation station by water jets before being further consolidated on the cylinder 8 by the devices 10 with water jets.
- a conveyor 28 having a deflection roller 29, a tensioning roller and a roller 31 for guiding a water-permeable belt 32 which is wound on a hollow cylinder 33 facing which are mounted devices 34 consolidation by water jets.
- Another conveyor 35 carried by supports 36 and brackets 37, comprises on a frame three return rollers 38, a tensioning roller 39 and a guide roll 40.
- the conveyor carries a device 41 for spraying water which will be used for wetting. This water projection device is vertical above the peak of the cylinder 33.
- a web of about 50 g / m 2 made of 100% polyester fibers of 1.7 dtex and 38 mm in length is produced at a speed of 50 m / min. by a carding card for nonwovens.
- This sheet is delivered continuously to a conveyor for transporting and compacting a water jet binding installation in accordance with the figure 1 .
- the transport conveyor is an 800 CFM permeability polyester fabric.
- the transport conveyor has a linear speed of 50 m / min.
- the transport conveyor is in contact over a length of 10 nm with the cylinder.
- the speed of the cylinder is synchronized with the speed of the transport conveyor at a linear speed of 50 m / min.
- the ply of fibers is compacted between the transport conveyor and the binding roll coated with a micro-perforated envelope, the holes being arranged in a random manner, as described in the French patent. 2,734,285 .
- the web is wet and slightly consolidated by a hydraulic injector projecting jets of water of 140 microns in diameter at a speed of 54 m / s or a pressure of 15 bar.
- the jets being spaced from each other by a distance of 0.8 mm in two rows.
- the veil thus compacted and wet and slightly consolidated is then subjected to the action of two successive hydraulic injectors projecting jets of water of 120 microns in diameter at increasing speeds of 100 m / s and 133 m / s, the jets being spaced from each other by 1.2 mm in two rows.
- the nonwoven thus obtained is then transferred to a suction mat connected to a vacuum generator and then dried at a temperature of 110 ° C in a through air oven.
- a nonwoven weighing approximately 50 g / m 2 is obtained.
- the nonwoven has a regular, uniform appearance.
- Example 1 The conditions of Example 1 are repeated. For this test, the speed of the roll is reduced by 10% with respect to the speed of the conveyor. That is, the speed of the transport and compaction conveyor is always 50 m / min. and the speed of the cylinder is 45 m / min.
- the nonwoven has a regular appearance.
- Example 1 The conditions of Example 1 are repeated. For this test, the speed of the cylinder is reduced by 20% relative to the speed of the conveyor. That is, the speed of the transport and compaction conveyor is always 50 m / min. and the speed of the cylinder is 40 m / min.
- the nonwoven is regular.
- Example 1 The conditions of Example 1 are repeated. For this test, the speed of the cylinder is reduced by 25% with respect to the speed of the conveyor. That is, the speed of the transport and compaction conveyor is always 50 m / min. and the speed of the cylinder is 40 m / min.
- the nonwoven is irregular and has wavelets of fibers in cross-direction.
- Example 1 The conditions of Example 1 are repeated. For this test, the transport conveyor is no longer in contact with the cylinder. It is now tangent to it and is about 1 mm from the cylinder. This new adjustment is obtained by lowering the return roller of the conveyor immediately downstream of the point of tangency of the conveyor relative to the cylinder.
- the speed conditions are identical to Example 2 in which the speed of the conveyor is 50 m / min. and the speed of the cylinder is 45 m / min.
- the nonwoven is regular.
- Example 5 The conditions of Example 5 are repeated. For this test, the speed of the cylinder is reduced by 20% relative to the speed of the conveyor. That is, the speed of the transport and compaction conveyor is always 50 m / min, and the speed of the cylinder is 40 m / min. The nonwoven is regular.
- Example 5 The conditions of Example 5 are repeated. For this test, the speed of the roll is reduced by 30% with respect to the speed of the conveyor. That is, the speed of the transport and compaction conveyor is always 50 m / min. and the speed of the cylinder is 35 m / min.
- the nonwoven is regular.
- Example 5 The conditions of Example 5 are repeated. For this test, the speed of the cylinder is reduced by 40% with respect to the speed of the conveyor. That is, the speed of the transport and compaction conveyor is always 50 m / min. and the speed of the cylinder is 30 m / min.
- the nonwoven has surface irregularities, wavelets oriented in the cross direction of the web and an irregularity of its opacity.
- a sheet of about 90 g / m 2 consisting of 65% viscose fibers of 1.7 dtex and 40 mm in length and 35% polyester fibers of 1.7 dtex and 38 mm in length is produced at a speed of 25 m / min. by a carding card for nonwovens.
- This sheet is delivered continuously to a conveyor for transporting and compacting a water jet binding installation in accordance with the figure 2 .
- the installation differs from that of the figure 1 by the addition of an upper conveyor winding around the cylinder.
- the transport conveyor is approximately 800 CFM permeability polyester fabric.
- the transport conveyor has a linear speed of 30 m / min.
- the upper conveyor winding around the cylinder is also a polyester fabric of about 500 CFM permeability.
- the transport conveyor is tangent to the second conveyor and the cylinder and is about 1.5 mm apart from the second conveyor at the point of convergence.
- the speed of the upper conveyor and the cylinder is synchronized with the speed of the transport conveyor at a speed of 25 m / min.
- the sheet of fibers is compacted progressively between the two conveyors immediately after compacting, the web is wet and slightly consolidated by a hydraulic injector projecting jets of water of 140 microns in diameter at a speed of 63 m / s or 20 bars of water. pressure.
- the jets being spaced from each other by a distance of 0.8 mm in two rows.
- the veil thus compacted and wet and slightly consolidated is then subjected to the action of two successive hydraulic injectors projecting jets of water of 120 microns in diameter at increasing speeds of 125 m / s and 160 m / s, the jets being spaced from each other by 1.2 mm in two rows.
- the nonwoven thus obtained is then transferred to a suction mat connected to a vacuum generator and then dried at a temperature of 110 ° C in a through air oven.
- the nonwoven thus obtained is regular, uniform.
- Example 9 The conditions of Example 9 are repeated. For this test, the speed of the upper conveyor and the cylinder is reduced by 20% relative to the speed of the conveyor. That is, the speed of the transport and compaction conveyor is always 25-m / min. and the speed of the cylinder is 20 m / min.
- the nonwoven is regular.
- Example 9 The conditions of Example 9 are repeated. For this test, the speed of the upper conveyor and the roll is reduced by 30% with respect to the speed of the conveyor. That is, the speed of the transport and compaction conveyor is always 25 m / min, and the speed of the cylinder is 17.5 m / min.
- the nonwoven is regular.
- Example 9 The conditions of Example 9 are repeated. For this test, the speed of the upper conveyor and the cylinder is reduced by 40% relative to the speed of the conveyor. That is, the speed of the transport and compaction conveyor is always 25 m / min. and the speed of the cylinder is 17.5 m / min.
- the non-woven is slightly irregular with a variation in its opacity reminiscent of a sliding of fibers in the transverse direction.
- a sheet of about 60 g / m 2 made of 80% polyester fibers of 1.7 dtex and 38 mm in length and 20% of polyester and polyethylene bicomponent fibers of 3 dtex and 38 mm in length is produced at a speed of 30 m / min. by a carding card for nonwovens.
- This sheet is delivered continuously to a transport and compacting conveyor XX of a water jet binding installation according to the invention.
- the transport conveyor is a polyester fabric.
- the transport conveyor has a linear speed of 30 m / min.
- the transport conveyor is tangent to a cylinder.
- the speed of the cylinder is synchronized with the speed of the transport conveyor at a speed of 30 M / min.
- the ply of fibers is compacted between the transport conveyor and the binding roll coated with a micro-perforated envelope, the holes being arranged in a random manner, as described in the French patent. 2,734,285 .
- the web is wet and slightly consolidated by a hydraulic injector projecting jets of water of 140 microns in diameter at a pressure of 70-bars. The jets being spaced from each other by a distance of 1.2 mm in two rows.
- the veil thus compacted and wet and slightly consolidated is then transferred to a suction belt connected to a vacuum generator and then dried at a temperature of 130 ° C in a through air oven.
- a nonwoven weighing approximately 60 g / m 2 is obtained.
- the nonwoven has a regular, uniform appearance and is bulky.
- Example 9 The conditions of Example 9 are repeated. For this test, the speed of the upper conveyor and the roll is reduced by 30% with respect to the speed of the conveyor. That is, the speed of the transport and compaction conveyor is always 30 m / min. and the speed of the cylinder is 21 m / min.
- the nonwoven is regular and bulky.
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Mechanical Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Nonwoven Fabrics (AREA)
- Treatment Of Fiber Materials (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Confectionery (AREA)
Claims (13)
- Verfahren zur Herstellung eines Vliesstoffs, bei welchem eine bewegte Bahn aus Fäden oder Fasern aus einem organischen Material an einer Stelle ihres Bewegungsweges in der Richtung der Dicke verdichtet wird und dann die verdichtete Bahn stromab an einer Verfestigungsstelle zu einer verfestigten Bahn verfestigt wird, dadurch gekennzeichnet, dass sie durch Bilden einer Stelle zum Quetschen der Bahn zwischen einem ersten beweglichen Element und einem anderen beweglichen Element verdichtet wird, und dass die Bewegungsgeschwindigkeit der Bahn verringert wird, indem dem anderen beweglichen Element eine lineare Geschwindigkeit gegeben wird, die um 5 bis 50% kleiner als diejenige des ersten Elements ist.
- Verfahren nach Anspruch 1, dadurch gekennzeichnet, dass die Dicke der Bahn beim Verdichten auf 99% bis 30% verringert wird.
- Verfahren nach einem der Ansprüche 1 oder 2, dadurch gekennzeichnet, dass die Bahn beim Verdichten oder unmittelbar stromab des Verdichtens befeuchtet wird.
- Verfahren nach einem der Ansprüche 1 bis 3, dadurch gekennzeichnet, dass die Bahn verfestigt wird, indem sie an der Verfestigungsstelle mit der verringerten Geschwindigkeit vorbeigeführt wird.
- Verfahren nach einem der Ansprüche 1 bis 4, dadurch gekennzeichnet, dass die Bahn durch hydraulische Verwickelung, durch thermische Bindung, durch chemische Bindung und/oder mechanische Nadelung verfestigt wird.
- Verfahren nach einem der Ansprüche 1 bis 5, dadurch gekennzeichnet, dass die Bahn eine von einer mittels Schmelze arbeitenden Vorrichtung stammende Bahn aus Fäden ist, oder dass die Bahn eine von einer Karde für Vliesstoffe oder eine von einer durch Luftablegung, "air laid" genannt, arbeitenden Vorrichtung stammende Bahn aus Fasern ist.
- Verfahren nach einem der Ansprüche 1 bis 6, dadurch gekennzeichnet, dass die Bahn gehalten wird, indem sie zwischen der Stelle, an welcher sie verdichtet wird, und der Verfestigungsstelle mit einem Unterdruck beaufschlagt wird.
- Vorrichtung zur Herstellung eines Vliesstoffs aus organischem Material, mit einem ersten Element (7) zum Leiten einer Bahn zu Mitteln, welche dazu bestimmt sind, sie in der Richtung der Dicke zu verdichten, und zu Mitteln, welche dazu bestimmt sind, ihre Geschwindigkeit zu verringern, dadurch gekennzeichnet, dass Mittel (10) zum Verfestigen der Bahn vorgesehen sind, die stromab, in der Bewegungsrichtung der Bahn, der Mittel zum Verdichten angeordnet sind, und dass die Mittel zum Verdichten und zum Verringern der Geschwindigkeit durch die Bildung einer Quetschungsstelle zwischen dem ersten Element (7) und einem anderen beweglichen Element (8) realisiert sind, wobei das andere bewegliche Element (8) eine lineare Geschwindigkeit aufweist, die um 5 bis 50% kleiner als diejenige des ersten Elements (7) ist.
- Vorrichtung nach Anspruch 8, dadurch gekennzeichnet, dass das andere bewegliche Element eine Fördereinrichtung oder ein Zylinder ist.
- Vorrichtung nach einem der Ansprüche 8 oder 9, gekennzeichnet durch Mittel (9), welche zum Befeuchten der Bahn, während die Bahn verdichtet wird oder wenn sie gerade verdichtet wurde, bestimmt sind.
- Vorrichtung nach einem Ansprüche 7 bis 9, dadurch gekennzeichnet, dass die Mittel (13) zum Verfestigen so angeordnet sind, dass die Bahn verfestigt wird, wenn diese über dem anderen beweglichen Element vorbeiläuft.
- Vorrichtung nach einem der Ansprüche 7 bis 11, gekennzeichnet durch Mittel zum Halten der Bahn durch Unterdruck zwischen den Mitteln zum Verdichten und den Mitteln zum Verfestigen.
- Verwendung eines Verfahrens oder einer Vorrichtung nach einem der Ansprüche 1 bis 12 zum Verringern des Verhältnisses einer Eigenschaft eines Vliesstoffs in der Längsrichtung zu dieser Eigenschaft in der Querrichtung.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0212652 | 2002-10-11 | ||
FR0212652A FR2845697B1 (fr) | 2002-10-11 | 2002-10-11 | Procede et machine de production d'un non-tisse a reduction de la vitesse de deplacement de la nappe compactee |
PCT/FR2003/002940 WO2004033781A2 (fr) | 2002-10-11 | 2003-10-07 | Procede et machine de production d'un non-tisse a reduction de la vitesse de deplacement de la nappe compactee |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1554421A2 EP1554421A2 (de) | 2005-07-20 |
EP1554421B1 true EP1554421B1 (de) | 2010-06-23 |
Family
ID=32039642
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP03775475A Expired - Lifetime EP1554421B1 (de) | 2002-10-11 | 2003-10-07 | Verfahren und vorrichtung zur herstellung von vliesstoffen unter verminderung der bewegungsgeschwindigkeit der verdichteten faserbahn |
Country Status (10)
Country | Link |
---|---|
US (1) | US7392575B2 (de) |
EP (1) | EP1554421B1 (de) |
CN (1) | CN100457996C (de) |
AT (1) | ATE472002T1 (de) |
AU (1) | AU2003283501A1 (de) |
BR (1) | BR0315245B1 (de) |
DE (1) | DE60333113D1 (de) |
FR (1) | FR2845697B1 (de) |
IL (1) | IL167871A (de) |
WO (1) | WO2004033781A2 (de) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102013101431A1 (de) * | 2013-02-13 | 2014-08-14 | TRüTZSCHLER GMBH & CO. KG | Vorrichtung und Verfahren zum hydrodynamischen Verfestigen von Vliesen, Geweben und Gewirken |
Families Citing this family (15)
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DE102004030413A1 (de) * | 2004-06-23 | 2006-02-23 | Fleissner Gmbh | Vorrichtung zum hydrodynamischen Verschlingen der Fasern einer Faserbahn |
DE102005033070A1 (de) * | 2005-07-15 | 2007-01-25 | Fleissner Gmbh | Vorrichtung zum Verfestigen einer Faserbahn mit Druckwasserstrahlen |
US7478463B2 (en) * | 2005-09-26 | 2009-01-20 | Kimberly-Clark Worldwide, Inc. | Manufacturing process for combining a layer of pulp fibers with another substrate |
FR2911616B1 (fr) * | 2007-01-19 | 2009-07-03 | Rieter Perfojet Soc Par Action | Installation et procede de production d'une nappe a base de fibres ou de filaments |
DE102008018976A1 (de) * | 2008-04-14 | 2009-10-15 | Fleissner Gmbh | Verfahren und Vorrichtung zur Herstellung eines Vliesstoffes |
DE102008013817A1 (de) * | 2008-03-12 | 2009-09-17 | Fleissner Gmbh | Verfahren und Vorrichtung zur Vorverfestigung eines Vlieses |
DE102009012607A1 (de) | 2009-03-11 | 2010-09-16 | Fleissner Gmbh | Vorrichtung zum Bearbeiten eines Flors |
PL2417290T3 (pl) * | 2009-04-08 | 2013-08-30 | Truetzschler Nonwovens Gmbh | Urządzenie do wzmacniania wstęgi włókien |
DE102009017729A1 (de) * | 2009-04-11 | 2010-10-14 | Fleissner Gmbh | Vorrichtung zum Verfestigen einer Faserbahn |
JP6364804B2 (ja) * | 2014-02-14 | 2018-08-01 | セイコーエプソン株式会社 | シート製造装置、原料解繊装置 |
CN109322062B (zh) * | 2018-10-26 | 2021-02-02 | 大连民族大学 | 3d堆叠式多层电纺纤维逐层喷射方法 |
US11987916B2 (en) | 2019-01-08 | 2024-05-21 | Andritz Perfojet Sas | Apparatus and method for producing nonwovens |
FR3099495B1 (fr) | 2019-07-30 | 2021-08-13 | Andritz Perfojet Sas | Installation de production de non-tissés |
FR3091541B1 (fr) | 2019-01-08 | 2022-04-22 | Andritz Perfojet Sas | Installation de production de non-tissés |
DE102021107902A1 (de) | 2021-03-29 | 2022-09-29 | Andritz Küsters Gmbh | Anlage zur Verfestigung mindestens einer nass- oder trockengelegten Faserlage zu einer Vliesbahn, mit einem Förderer, der ein umlaufendes Band mit einem oberen Trum umfasst, auf welches die mindestens eine Faserlage ablegbar und in einer Produktionsrichtung verlagerbar ist |
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FR2548695B1 (fr) * | 1983-07-07 | 1986-06-20 | Saint Gobain Isover | Formation de feutres a structure isotrope |
DE3832773C2 (de) * | 1988-09-27 | 1996-08-22 | Heraklith Holding Ag | Verfahren und Vorrichtung zur Herstellung von Mineralfaserplatten |
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FR2729404B1 (fr) * | 1995-01-12 | 1997-04-11 | Asselin | Aiguilleteuse et procede de commande d'avance associe |
FR2730246B1 (fr) * | 1995-02-03 | 1997-03-21 | Icbt Perfojet Sa | Procede pour la fabrication d'une nappe textile non tissee par jets d'eau sous pression, et installation pour la mise en oeuvre de ce procede |
GB2300429B (en) * | 1995-05-03 | 1999-01-13 | Courtaulds Eng Ltd | Non-woven fabric manufacture |
EP0888259A4 (de) * | 1996-03-20 | 2001-04-11 | Owens Corning Fiberglass Corp | Verfahren zur herstellung ein isalationsprodukt |
EP0859076B1 (de) * | 1997-02-12 | 2002-08-28 | Fleissner GmbH & Co. Maschinenfabrik | Vorrichtung zum hydrodynamischen Verschlingen der Fasern einer Faserbahn |
US5900206A (en) * | 1997-11-24 | 1999-05-04 | Owens Corning Fiberglas Technology, Inc. | Method of making a fibrous pack |
US6010785A (en) * | 1998-02-25 | 2000-01-04 | E. I. Du Pont De Nemours And Company | Cardable blends of dual glass fibers |
FR2777575B1 (fr) * | 1998-04-17 | 2000-07-07 | Thibeau | Procede et installation pour la formation d'un voile fibreux par voie aeraulique |
DE19827567A1 (de) * | 1998-06-20 | 1999-12-23 | Corovin Gmbh | Verfahren zur Herstellung eines Vlieses aus Fasern |
FR2781818B1 (fr) * | 1998-07-31 | 2000-09-01 | Icbt Perfojet Sa | Procede pour la realisation d'un materiau non-tisse complexe et nouveau type de materiau ainsi obtenu |
DE10006763A1 (de) * | 2000-02-15 | 2001-08-16 | Fleissner Gerold | Vorrichtung zum hydrodynamischen Beaufschlagen der Fasern einer Faserbahn mit einem Fluid |
DE10008746A1 (de) * | 2000-02-24 | 2001-08-30 | Fleissner Maschf Gmbh Co | Verfahren und Vorrichtung zur Herstellung von Verbundvliesstoffen mittels hydrodynamischer Vernadelung |
FR2815647B1 (fr) | 2000-10-20 | 2003-02-14 | Rieter Perfojet | Installation de production d'une nappe non tissee a difusseur et a separation des filaments par voie electrostatique |
FR2821866B1 (fr) * | 2001-03-06 | 2003-05-16 | Rieter Perfojet | Dispositif et procede de compactage d'une nappe de fibres a reglage de la pression applique a la nappe |
TW508390B (en) * | 2001-05-09 | 2002-11-01 | Ind Tech Res Inst | Feeding device for preneedling nonwoven fabrics |
DE10146907B4 (de) * | 2001-09-24 | 2007-02-22 | Oskar Dilo Maschinenfabrik Kg | Vlieszuführvorrichtung |
FR2838457B1 (fr) * | 2002-04-12 | 2004-08-27 | Rieter Perfojet | Tambour pour installation de production d'une nappe non-tissee, procede de production d'une nappe non-tissee et nappe non-tissee obtenue |
EP1447213A1 (de) * | 2003-02-11 | 2004-08-18 | Saint-Gobain Vetrotex France S.A. | Struktur enthaltend einen trockengelegten Vliesstoff aus Glasfasern und einen Vliesstoff aus organischen Fasern |
-
2002
- 2002-10-11 FR FR0212652A patent/FR2845697B1/fr not_active Expired - Lifetime
-
2003
- 2003-10-07 AU AU2003283501A patent/AU2003283501A1/en not_active Abandoned
- 2003-10-07 BR BRPI0315245-6A patent/BR0315245B1/pt active IP Right Grant
- 2003-10-07 DE DE60333113T patent/DE60333113D1/de not_active Expired - Lifetime
- 2003-10-07 CN CNB2003801012307A patent/CN100457996C/zh not_active Expired - Lifetime
- 2003-10-07 WO PCT/FR2003/002940 patent/WO2004033781A2/fr not_active Application Discontinuation
- 2003-10-07 US US10/529,844 patent/US7392575B2/en active Active
- 2003-10-07 AT AT03775475T patent/ATE472002T1/de active
- 2003-10-07 EP EP03775475A patent/EP1554421B1/de not_active Expired - Lifetime
-
2005
- 2005-04-05 IL IL167871A patent/IL167871A/en unknown
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102013101431A1 (de) * | 2013-02-13 | 2014-08-14 | TRüTZSCHLER GMBH & CO. KG | Vorrichtung und Verfahren zum hydrodynamischen Verfestigen von Vliesen, Geweben und Gewirken |
DE102013101431B4 (de) * | 2013-02-13 | 2016-06-23 | TRüTZSCHLER GMBH & CO. KG | Vorrichtung und Verfahren zum hydrodynamischen Verfestigen von Vliesen, Geweben und Gewirken |
Also Published As
Publication number | Publication date |
---|---|
EP1554421A2 (de) | 2005-07-20 |
ATE472002T1 (de) | 2010-07-15 |
US20060080816A1 (en) | 2006-04-20 |
AU2003283501A8 (en) | 2004-05-04 |
IL167871A (en) | 2010-12-30 |
US7392575B2 (en) | 2008-07-01 |
CN100457996C (zh) | 2009-02-04 |
WO2004033781A2 (fr) | 2004-04-22 |
FR2845697A1 (fr) | 2004-04-16 |
DE60333113D1 (de) | 2010-08-05 |
WO2004033781A3 (fr) | 2004-05-27 |
FR2845697B1 (fr) | 2005-05-27 |
AU2003283501A1 (en) | 2004-05-04 |
BR0315245A (pt) | 2005-08-23 |
CN1774533A (zh) | 2006-05-17 |
BR0315245B1 (pt) | 2013-05-07 |
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