EP1101827B1 - Procédé de grenaillage par ultrasons de surfaces annulaires de grandes dimensions sur des pièces minces - Google Patents

Procédé de grenaillage par ultrasons de surfaces annulaires de grandes dimensions sur des pièces minces Download PDF

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Publication number
EP1101827B1
EP1101827B1 EP00403183A EP00403183A EP1101827B1 EP 1101827 B1 EP1101827 B1 EP 1101827B1 EP 00403183 A EP00403183 A EP 00403183A EP 00403183 A EP00403183 A EP 00403183A EP 1101827 B1 EP1101827 B1 EP 1101827B1
Authority
EP
European Patent Office
Prior art keywords
opening
shot blasting
enclosure
microbeads
shot
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP00403183A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP1101827A1 (fr
Inventor
Catherine Dominique Béatrice Duquenne
Véronique Christiane Raymonde Giffard
Gérard Michel Roland Gueldry
Claude Marcel Mons
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Safran Aircraft Engines SAS
Original Assignee
SNECMA Moteurs SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SNECMA Moteurs SA filed Critical SNECMA Moteurs SA
Publication of EP1101827A1 publication Critical patent/EP1101827A1/fr
Application granted granted Critical
Publication of EP1101827B1 publication Critical patent/EP1101827B1/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24CABRASIVE OR RELATED BLASTING WITH PARTICULATE MATERIAL
    • B24C5/00Devices or accessories for generating abrasive blasts
    • B24C5/005Vibratory devices, e.g. for generating abrasive blasts by ultrasonic vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24CABRASIVE OR RELATED BLASTING WITH PARTICULATE MATERIAL
    • B24C1/00Methods for use of abrasive blasting for producing particular effects; Use of auxiliary equipment in connection with such methods
    • B24C1/10Methods for use of abrasive blasting for producing particular effects; Use of auxiliary equipment in connection with such methods for compacting surfaces, e.g. shot-peening
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D7/00Modifying the physical properties of iron or steel by deformation
    • C21D7/02Modifying the physical properties of iron or steel by deformation by cold working
    • C21D7/04Modifying the physical properties of iron or steel by deformation by cold working of the surface
    • C21D7/06Modifying the physical properties of iron or steel by deformation by cold working of the surface by shot-peening or the like
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/04General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering with simultaneous application of supersonic waves, magnetic or electric fields
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00Metal working
    • Y10T29/47Burnishing
    • Y10T29/479Burnishing by shot peening or blasting

Definitions

  • the invention relates to a method of ultrasonic shot blasting using a mist of microbeads inside an enclosure and more particularly to a shot blasting of large annular surfaces on parts thin.
  • microbeads are commonly rolling bearing balls. They are usually ceramic or steel with a diameter of 0.2mm to 4mm. The shot peening is carried out inside a closed cabin using powered nozzles simultaneously with compressed gas and microbeads, the compressed gas ensuring the propulsion of microbeads.
  • the patent FR.2,689,431 discloses a method of blasting said improperly “by ultrasound “consisting of maintaining a” fog "of microbeads inside a pregnant, the interview being carried out using a vibrator acting at frequencies of the order of 20 KH, the enclosure being open, the part being applied against the opening of the enclosure, shot blasting being ensured by the impacts of the microbeads on the part, the enclosure and the room being animated by a relative movement aiming at passing the enclosure on the entire surface of the piece to be blasted.
  • the patent also shows how shot blast circular parts such as trees.
  • fog is used by analogy with fogs formed of tiny droplets of water. Indeed, in the process of ultrasonic shot blasting, the microbeads are animated with random speeds in modulus and direction, which makes them ricochet between them, against the walls of the enclosure and against the surface of the room in contact with the mist of microbeads.
  • This patent gives examples of massive pieces able to resume without distort the stresses resulting from shot blasting.
  • this process does not allow to blast thin circular pieces, because they start to deform very early during shot blasting even. Even if the surface is uniformly blasted, these deformations are only partially absorbed at the end of shot blasting because the stress is achieved by the plastic and non-linear deformation of the material.
  • the process requires that shot blasting be stopped accurately when the piece has made a turn if you want to get a uniform shot blasting. Indeed, a late stop shot blasting produce a localized excess of shot blasting on a lap premature will produce a localized lack of shot blasting that will be difficult to complete without causing excessive blasting just next door.
  • a first problem to solve is to blast without deforming the thin parts and the dimensions of which are greater than those of the shot blasting chamber.
  • a second problem to be solved is to guarantee uniform shot blasting over the entire surface to be blasted.
  • the invention proposes a method of ultrasonic blasting of annular surfaces of large dimensions on thin pieces, said method of passing the surface to be shot-blasted in front of the opening of a blasting chamber, said enclosure containing a "mist" of microbeads maintained by a vibrator inside the enclosure, said microbeads impinging the portion of the surface to be blasted presented in front of the opening, said impacts causing shot blasting, said enclosure and said part being driven by a relative rotational movement to make the whole of the surface to be blasted in front of the opening of the enclosure during shot blasting.
  • shotblasting is done in N passes in front of the opening of the enclosure, each point of the shot-blasting surface passing N times before the opening of the enclosure, each passage providing a fraction substantially equal to 1 / N of total shot blasting to be done.
  • N 5 revolutions. This result will obviously be better with a higher number of revolutions, for example 20 or 100. A large number N is needed for shot blasting very thin.
  • An advantage of the method is to allow to allow a large shot blasting and pushed to optimal on thin parts without deforming them, since during all shot peening, the stresses imposed on the part remain uniform.
  • Part 1 is a training cone on a turbine engine for aircraft.
  • Part 1 consists of a thin wall and has a shape circle of revolution around a geometric axis 2.
  • Part 1 has a barrel 3 truncated cone whose end of larger diameter is extended radially by a flange 4, said flange 4 itself having a bearing surface 5 to be blasted, said bearing surface 5 being annular, flat and radial.
  • An enclosure 10 is used inside which is maintained a fog of microbeads 11, said enclosure being delimited laterally by a wall 12, said enclosure having an opening 13 whose edges are referenced 14.
  • a vibrator 20 constituted by a sonotrode 21 resonated by one its ends by a vibration generator 22 which is usually quartz, the other end of the sonotrode 21 having a vibrating surface 23 and substantially plane, said vibrating surface 23 being placed at the bottom of the enclosure 10 and being opposite of the opening 13.
  • the vibration generator 22 puts in longitudinal resonance the sonotrode 21.
  • the vibrating surface 23 thus excited transmits energy to the microbeads which bounce on the surface to be blasted 5 opposite the opening 13 and on the walls of the chamber 12, said microbeads then gradually losing energy, said microbeads also arriving on the vibrating surface 23 which gives them a new energy.
  • the microbeads move inside the enclosure at speeds random in size and direction, these microbeads thus forming a real "fog" of microbeads inside the enclosure 10.
  • An advantage of the method is that the shot peening is carried out without contact between the piece 1 and the enclosure 10, which avoids any degradation of the surface of the room.
  • the microbeads are retained inside the enclosure 10 because the game E is less than the diameter of said microbeads.
  • This arrangement also has the advantage of avoiding the use of wear pads on the enclosure 10
  • T To x ⁇ x D / L in which To is the duration of exposure to shot blasting of each element of the surface to be shot blasted 5, D is the average diameter of said surface 5 and L is the width of the enclosure 10 taken tangentially to the displacement of said surface 5 in front of the opening 13, that is to say perpendicular to the plane of the single figure.
  • the edges 14 of the enclosure 10 will be given a shape complementary to said surface, in order to maintain the game E.

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Grinding And Polishing Of Tertiary Curved Surfaces And Surfaces With Complex Shapes (AREA)
  • Apparatuses For Generation Of Mechanical Vibrations (AREA)
  • Processing Of Stones Or Stones Resemblance Materials (AREA)
  • Sliding-Contact Bearings (AREA)
EP00403183A 1999-11-18 2000-11-16 Procédé de grenaillage par ultrasons de surfaces annulaires de grandes dimensions sur des pièces minces Expired - Lifetime EP1101827B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR9914481A FR2801322B1 (fr) 1999-11-18 1999-11-18 Procede de grenaillage par ultrasons de surfaces annulaires de grandes dimensions sur des pieces minces
FR9914481 1999-11-18

Publications (2)

Publication Number Publication Date
EP1101827A1 EP1101827A1 (fr) 2001-05-23
EP1101827B1 true EP1101827B1 (fr) 2005-01-26

Family

ID=9552239

Family Applications (1)

Application Number Title Priority Date Filing Date
EP00403183A Expired - Lifetime EP1101827B1 (fr) 1999-11-18 2000-11-16 Procédé de grenaillage par ultrasons de surfaces annulaires de grandes dimensions sur des pièces minces

Country Status (10)

Country Link
US (1) US6289705B1 (uk)
EP (1) EP1101827B1 (uk)
JP (1) JP4267199B2 (uk)
CA (1) CA2325897C (uk)
DE (1) DE60017681T2 (uk)
ES (1) ES2233310T3 (uk)
FR (1) FR2801322B1 (uk)
RU (1) RU2210602C2 (uk)
UA (1) UA66403C2 (uk)
WO (1) WO2001036692A1 (uk)

Families Citing this family (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6932876B1 (en) 1998-09-03 2005-08-23 U.I.T., L.L.C. Ultrasonic impact machining of body surfaces to correct defects and strengthen work surfaces
US6458225B1 (en) * 1998-09-03 2002-10-01 Uit, L.L.C. Company Ultrasonic machining and reconfiguration of braking surfaces
US20050145306A1 (en) * 1998-09-03 2005-07-07 Uit, L.L.C. Company Welded joints with new properties and provision of such properties by ultrasonic impact treatment
US6338765B1 (en) 1998-09-03 2002-01-15 Uit, L.L.C. Ultrasonic impact methods for treatment of welded structures
US20060016858A1 (en) * 1998-09-03 2006-01-26 U.I.T., Llc Method of improving quality and reliability of welded rail joint properties by ultrasonic impact treatment
FR2814099B1 (fr) * 2000-09-21 2002-12-20 Snecma Moteurs Grenaillage transversal par ultrassons des aubes sur un rotor
US7028378B2 (en) * 2000-10-12 2006-04-18 Sonats-Societe Des Nouvelles Applications Des Techniques De Surfaces Method of shot blasting and a machine for implementing such a method
FR2816636B1 (fr) 2000-11-16 2003-07-18 Snecma Moteurs Grenaillage des sommets des aubes refroidies
FR2816537B1 (fr) 2000-11-16 2003-01-17 Snecma Moteurs Procede et installation de grenaillage par ultrasons des alveoles annulaires d'attache d'aubes sur un rotor
FR2816538B1 (fr) * 2000-11-16 2003-01-17 Snecma Moteurs Procede pour augmenter la duree de vie des attaches d'aubes sur un rotor
FR2816536B1 (fr) 2000-11-16 2003-01-17 Snecma Moteurs Procede et dispositif de grenaillage par ultrasons des alveoles "axiales" d'attache des aubes sur un rotor
JP2005192194A (ja) * 2003-12-05 2005-07-14 Yazaki Corp 通信装置及び通信システム
US7399371B2 (en) * 2004-04-16 2008-07-15 Nippon Steel Corporation Treatment method for improving fatigue life and long-life metal material treated by using same treatment
US7301123B2 (en) 2004-04-29 2007-11-27 U.I.T., L.L.C. Method for modifying or producing materials and joints with specific properties by generating and applying adaptive impulses a normalizing energy thereof and pauses therebetween
DE102004029546A1 (de) * 2004-06-19 2006-01-05 Mtu Aero Engines Gmbh Verfahren und Vorrichtung zum Oberflächenstrahlen von Gasturbinenschaufeln im Bereich ihrer Schaufelfüße
US20060021410A1 (en) 2004-07-30 2006-02-02 Sonats-Societe Des Nouvelles Applications Des Techniques De Surfaces Shot, devices, and installations for ultrasonic peening, and parts treated thereby
DE102004037954A1 (de) * 2004-08-05 2006-03-16 Mtu Aero Engines Gmbh Vorrichtung zum Oberflächenstrahlen von Bauteilen
DE102004059592B4 (de) * 2004-12-10 2014-09-04 MTU Aero Engines AG Verfahren zum Oberflächenstrahlen von Hohlräumen, insbesondere von Hohlräumen an Gasturbinen
US7992416B2 (en) * 2005-05-12 2011-08-09 General Electric Company Ultrasonic peening treatment of assembled components
US7276824B2 (en) * 2005-08-19 2007-10-02 U.I.T., L.L.C. Oscillating system and tool for ultrasonic impact treatment
US20070068605A1 (en) * 2005-09-23 2007-03-29 U.I.T., Llc Method of metal performance improvement and protection against degradation and suppression thereof by ultrasonic impact
DE102005054866A1 (de) 2005-11-17 2007-05-31 Mtu Aero Engines Gmbh Verfahren zum Herstellen von metallischen Bauteilen, insbesondere für Turbomaschinen, mit kleinen Kantenradien
US20070244595A1 (en) * 2006-04-18 2007-10-18 U.I.T., Llc Method and means for ultrasonic impact machining of surfaces of machine components
DE102006036519A1 (de) * 2006-08-04 2008-02-07 Mtu Aero Engines Gmbh Deckelelement für eine Sonotrode und Strahlkammeranordnung zum Oberflächenstrahlen von Bauteilen
FR2907360B1 (fr) * 2006-10-20 2009-05-22 Sonats Soc Des Nouvelles Appli Procedes et installations de grenailles.
US7665338B2 (en) * 2006-10-20 2010-02-23 Sonats-Societe Des Nouvelles Applications Des Techniques De Surfaces Shot peening methods and units
DE102007009470A1 (de) * 2007-02-27 2008-08-28 Daimler Ag Verfahren und Vorrichtung zum Oberflächenstrahlen
US20090095043A1 (en) * 2007-10-11 2009-04-16 Bunting Billie W Conformable tooling for localized shot peening
FR2930184B1 (fr) * 2008-04-18 2010-12-31 Snecma Procede de grenaillage par ultrason de pieces de turbomachines.
JP5912916B2 (ja) * 2012-06-27 2016-04-27 日立Geニュークリア・エナジー株式会社 ショットピーニング方法
WO2019097275A1 (en) * 2017-11-15 2019-05-23 Arcelormittal Treatment method for a cutting piece, and associated equipment
CN113084714A (zh) * 2021-04-21 2021-07-09 中国科学院宁波材料技术与工程研究所 一种空化喷丸装置
CN114941066B (zh) * 2022-05-27 2023-06-02 南京航空航天大学 一种液氮冷却的超声喷丸加工装置及方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1435627A1 (ru) * 1987-04-06 1988-11-07 Кузнецкий металлургический комбинат им.В.И.Ленина Способ упрочнени стальных изделий
DE4041103A1 (de) * 1990-12-21 1992-07-02 Mtu Muenchen Gmbh Verfahren zur oberflaechenbehandlung von bauteilen
FR2689431B1 (fr) * 1992-04-06 1995-10-20 Teknoson Procede et dispositif notamment de durcissement par ultrasons de pieces metalliques.
FR2715884B1 (fr) * 1994-02-04 1996-04-12 Gec Alsthom Electromec Procédé et dispositif pour le traitement de surface et la mise en précontrainte de la paroi intérieure d'une cavité.
FR2743742B1 (fr) * 1996-01-24 1998-04-03 Seb Sa Procede de traitement d'une surface metallique et de fabrication d'un article culinaire
RU2130085C1 (ru) * 1997-05-29 1999-05-10 Казаков Владимир Михайлович Способ поверхностного упрочнения деталей

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Metals Handbook, Vol. 5, Surface cleaning, Finishing and Coating, 9ième édition, 1982, pages 138-140 *

Also Published As

Publication number Publication date
CA2325897A1 (fr) 2001-05-18
EP1101827A1 (fr) 2001-05-23
DE60017681D1 (de) 2005-03-03
RU2210602C2 (ru) 2003-08-20
FR2801322A1 (fr) 2001-05-25
JP4267199B2 (ja) 2009-05-27
WO2001036692A1 (fr) 2001-05-25
ES2233310T3 (es) 2005-06-16
CA2325897C (fr) 2007-09-18
JP2001170866A (ja) 2001-06-26
UA66403C2 (uk) 2004-05-17
FR2801322B1 (fr) 2002-02-08
DE60017681T2 (de) 2005-12-22
US6289705B1 (en) 2001-09-18

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