EP0234170B1 - Method for spinning flax or mixtures thereof - Google Patents

Method for spinning flax or mixtures thereof Download PDF

Info

Publication number
EP0234170B1
EP0234170B1 EP86440019A EP86440019A EP0234170B1 EP 0234170 B1 EP0234170 B1 EP 0234170B1 EP 86440019 A EP86440019 A EP 86440019A EP 86440019 A EP86440019 A EP 86440019A EP 0234170 B1 EP0234170 B1 EP 0234170B1
Authority
EP
European Patent Office
Prior art keywords
fibres
flax
spinning
roving
short
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
EP86440019A
Other languages
German (de)
French (fr)
Other versions
EP0234170A1 (en
Inventor
Léon Salmon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to AT86440019T priority Critical patent/ATE47434T1/en
Publication of EP0234170A1 publication Critical patent/EP0234170A1/en
Application granted granted Critical
Publication of EP0234170B1 publication Critical patent/EP0234170B1/en
Expired legal-status Critical Current

Links

Images

Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01HSPINNING OR TWISTING
    • D01H1/00Spinning or twisting machines in which the product is wound-up continuously
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01GPRELIMINARY TREATMENT OF FIBRES, e.g. FOR SPINNING
    • D01G21/00Combinations of machines, apparatus, or processes, e.g. for continuous processing
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01HSPINNING OR TWISTING
    • D01H13/00Other common constructional features, details or accessories
    • D01H13/30Moistening, sizing, oiling, waxing, colouring, or drying yarns or the like as incidental measures during spinning or twisting
    • D01H13/302Moistening, e.g. for wet spinning

Definitions

  • the invention relates to a process for spinning linen. It will find its application in particular in the textile industry for the production of spools of pure linen thread or in mixture with other natural, artificial or synthetic fibers.
  • the flaxseed harvest is done during the summer.
  • the stems are torn off and subjected to retting and scutching operations.
  • the elementary fibers with an average length of 2 to 3 cm and an average diameter of 13 to 15 microns, are agglutinated to each other by a pecto-woody complex, to constitute the fibrous bundles. These are located at the periphery of the stem, in the Liberian zone and, at maturity, are strongly adherent to the central woody trunk.
  • Retting is a biological operation, the main purpose of which is to separate the fibrous bundles from the woody trunk. There is retting on the ground and retting with water. When retting on the ground, at the time of uprooting, the stems are spread out on the ground and they remain there for 3 to 6 weeks. Under the effect of humidity and temperature, saprophytic fungi present on the plant at the time of uprooting, proliferate and secrete enzymes which partially dissolve pectic cements welding the fibers to the wood.
  • the main role of scutching is to separate the fibers from the wood.
  • the stems undergo the crushing operation which breaks the wood while leaving the fibers intact, then they are beaten to make the shives fall or woody debris.
  • the useful product is flax or flax; but one of the by-products also has a textile value: these are the weaving tows, more or less short fibers, separated from the dyed flax during threshing.
  • Dyeed flax the apparent length of which is generally between 70 cm and 1 meter, consists of bundles adhering to each other longitudinally and transversely.
  • the dyed flax delivered to the spinning machine corresponds to the entire fibrous corona of the Liberian zone in which the elementary cellulosic fibers represent only 70% by weight, the rest being non-cellulosic substances decomposing into hemicelluloses, pectic materials, lignins and mineral elements.
  • dyed flax undergoes the combing operation, the role of which is threefold: to clean the tow by ridding it of the last traces of shives; separate the bundles linked together by the cortex and cortical parenchyma and thereby refine the technical fibers; eliminate the short fibers of the foot and head that are the combs.
  • the resulting combed linen is spread out and the tablecloth thus obtained is stretched to provide a continuous ribbon.
  • This is stretched and doubled successively on 5 machines called drawing benches whose role is threefold: to improve the mass regularity of the ribbon as much as possible; gradually reduce its linear density (or title); refine the technical fibers by cleaving the fibrous bundles.
  • This third function which is fundamental to allow suitable spinnability, is obtained by stretching the ribbon in a field of increasingly fine needles by means of a stretching train (steel-wood) working in a thin layer.
  • This operation in known processes is carried out on very specific equipment with a particularly high purchase price.
  • the ribbon emerging from the last pass is then stretched on a spindle bench, which is also very specific and very expensive, in order to obtain a slightly twisted wick intended to be worked on a spinning loom.
  • the constituent fibrous elements are themselves very fine and close to the elementary fiber.
  • the fibrous elements making up the unbleached wick have an average length of between 15 and 20 cm and often have between 3 and 10 elementary fibers in section. It is therefore necessary to dissociate the elementary fibers during the spinning operation or before it.
  • the unbleached wick was wet for a long time by passing it through a tank of water brought to a temperature of about 70 ° C. and drawing it in a rolling train with fluted rollers, at high pressure and with spacing between 65 and 80 mm. But this way of proceeding leads to very difficult working conditions and does not allow obtaining thinner yarns than Nm 21 (48 tex) validly marketable.
  • the main object of the present invention is to present a very economical method of spinning flax.
  • the substantial gains that can be made are in terms of reduced labor and also in terms of investment in equipment.
  • Another object of the present invention is to present a process for spinning flax which makes it possible to obtain a pure flax yarn or a blended yarn of a cleanliness hitherto unequaled industrially, while retaining the appearance of traditional flax.
  • the raw material used is very short technical flax fiber of variable length and very mechanically refined, for example using an opener (without any chemical or physico-chemical treatment), the length and fineness of which are fairly close to the characteristics of elementary fiber.
  • the prior shortening is carried out on lengths of the order of 5 to 6 cm and then the material is refined, that is to say that the bundle which initially comprised ten to forty elementary fibers in section is reduced to a fibrous element much finer and comprising only a few elementary fibers.
  • the preparation i.e. the different physical operations before spinning, is derived from that used for other short fibers such as cotton or other artificial fibers of the same size: card, two drawing passes and bench -to-pin.
  • the spinning according to the invention which is carried out after physical preparation, is derived from the conventional spinning of flax in the wet: soaking the wick continuously in water which may be cold; rolling comprising a stretch control system.
  • Linen fiber has not undergone any chemical or physico-chemical treatment, it is unbleached and therefore has retained a good part of its non-cellulosic constituents: hemi-celluloses and pectic substances.
  • the yarn thus obtained has a real "linen look" even when it is made in a mixture with artificial or synthetic fibers. This is due to the fact that the flax fiber remained unbleached and that it was spun in the wet state.
  • the present invention relates to a process for spinning pure or mixed flax.
  • the present invention has a large number of advantages, among which there may be mentioned:
  • the processing cost is greatly reduced compared to that of the traditional process, to the point of approaching that of short fiber spinning.
  • the raw material used is short fiber, preferably mechanically refined (without chemical or physico-chemical treatment), the length and fineness of which are fairly close to the characteristics of the elementary fiber. It is unbleached and therefore has not suffered a significant loss and has retained a good part of its non-cellulosic constituents. Consequently, its cost is limited; it is very accessible to water because of its great finesse and its short length and does not require chemical treatment prior to spinning; it provides pectic cements which, after softening and drying, help to give more cohesion between the fibers in the yarn.
  • the type of preparation used makes it possible to make any mixture of flax and other fibers without any difficulty and the fibrous mixture is very homogeneous.
  • the flax spinning process thanks to the stretching system, makes it possible to spin not only pure flax, but also any type of mixture of flax and other fibers.
  • the yarn thus obtained has a real "linen look” as does the canvas or knitting made from this yarn. This is due to the fact that the flax fiber remained natural and was spun in the wet state. This gives the yarn a high technological and commercial added value compared to the same yarn made in the dry state. Furthermore, the yarn obtained has no major defects as opposed to traditional flax yarn.
  • the flax spinning process of the present invention one starts from a raw material composed of bundles of dyed flax fibers.
  • the first operation that these fibers must undergo consists in reducing their length associated with refining.
  • the length of the fibers which initially is of the order of 70 cm to 1 m, must in fact be reduced by appropriate treatments to a length of short fibers, that is to say substantially of the order of 2 to 5 cm.
  • This reduction in length is done mechanically by cutting or cracking followed by a process which refines. It is necessary to obtain short and very fine fibers. This first operation does not generally require chemical or physico-chemical intervention. It is indeed necessary that the fiber retains its natural qualities so that the resulting yarn has the "linen character" from the point of view of its appearance and its feel.
  • the prior shortening is carried out on lengths of the order of 5 to 6 cm and then the material is refined, that is to say that the bundle which initially comprised ten to forty elementary fibers in section is reduced to a fibrous element much finer and comprising only a few elementary fibers.
  • the carded ribbon obtained is then grouped with other ribbons and the assembly is then stretched to form a new ribbon whose regularity is improved.
  • one or more passes can be made to obtain a ribbon of substantially constant linear density.
  • the ribbon is then stretched and slightly twisted to form a wick. This phase of the process can be carried out on pin banks.
  • One of the characteristics of the invention is to spin this wick of short fibers in the wet state. To do this, the wick first passes through a water tank which can be cold, integrated into the spinning machine, then it is stretched in a rolling train designed to work this type of material as well as possible.
  • Figure 1 shows schematically a drawing machine of spinning loom.
  • a spool 1 of a bench bit wick is used to power the drawing train 2 which delivers a wire 3 which is wound around a spindle 4.
  • the control of the short fibers is achieved by the use of a drawing train 2 with sleeve 5.
  • the drawing train with sleeve in fact makes it possible to guide the short fibers.
  • the wick undergoes a pre-stretching between the supply cylinders 6 and the sleeves 5 and then a proper stretching between the sleeves 5 and the delivery cylinders 7.
  • the path of these in the drawing train 2 is carried out in an arc.

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
  • Artificial Filaments (AREA)
  • Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
  • Nonwoven Fabrics (AREA)

Abstract

1. Process for spinning pure or blended flax, designed for the textile industry to form a yarn by twisting flax fibres from bundles of long fibres swingled and agglomerated by pectins, implementing at least one spinning frame, characterized in that : - the length of the fibres is mechanically reduced by a suitable treatment, followed by another mechanical operation so as to obtain only short, extremely fine fibres, - the short fibres are carded to form a ribbon, - the ribbon is drawn to adjust its weight per unit length and the said short fibres are controlled while they are being drawn on the spinning frame, - the ribbon is twisted to form a roving, - the roving is wetted, - the wetted roving is drawn and is twisted to form the yarn.

Description

L'invention est relative à un procédé de filage du lin. Elle trouvera notamment son application dans l'indutrie textile pour la réalisation de bobines de fil de lin pur ou en mélange avec d'autres fibres naturelles, artificielles ou synthétiques.The invention relates to a process for spinning linen. It will find its application in particular in the textile industry for the production of spools of pure linen thread or in mixture with other natural, artificial or synthetic fibers.

Depuis la plus haute antiquité, le lin est cultivé pour ses fibres textiles et sa graine qui fournit une huile siccative. Il réclame des terres profondes, fertiles et riches en humus, ce qui a localisé sa culture dans certaines régions du monde en particulier, l'URSS, la Chine et l'Europe du Nord.Since ancient times, flax has been cultivated for its textile fibers and its seed which provides a drying oil. He claims deep, fertile land rich in humus, which has localized his culture in certain regions of the world in particular, the USSR, China and Northern Europe.

La récolte du lin à filasse se fait durant l'été. On arrache les tiges et on leur fait subir les opérations de rouissage et de teillage.The flaxseed harvest is done during the summer. The stems are torn off and subjected to retting and scutching operations.

Dans la tige, les fibres élémentaires d'une longueur moyenne de 2 à 3 cm et d'un diamètre moyen de 13 à 15 microns, sont agglutinées les unes aux autres par un complexe pecto-ligneux, pour constituer les faisceaux fibreux. Ceux-ci se situent à la périphérie de la tige, dans la zone libérienne et, à maturité, sont fortement adhérents au tronc ligneux central.In the stem, the elementary fibers with an average length of 2 to 3 cm and an average diameter of 13 to 15 microns, are agglutinated to each other by a pecto-woody complex, to constitute the fibrous bundles. These are located at the periphery of the stem, in the Liberian zone and, at maturity, are strongly adherent to the central woody trunk.

Le rouissage est une opération biologique dont l'objet essentiel est de désolidariser les faisceaux fibreux du tronc ligneux, Il existe le rouissage à terre et le rouissage à l'eau. Lors du rouissage à terre, au moment de l'arrachage, les tiges sont étalées à même le sol et elles y demeurent pendant 3 à 6 semaines. Sous l'effet de l'humidité et de la température, des champignons saprophytes présents sur la plante au moment de l'arrachage, prolifèrent et secrè- tent des enzymes qui dissolvent partiellement les ciments pectiques soudant les fibres au bois.Retting is a biological operation, the main purpose of which is to separate the fibrous bundles from the woody trunk. There is retting on the ground and retting with water. When retting on the ground, at the time of uprooting, the stems are spread out on the ground and they remain there for 3 to 6 weeks. Under the effect of humidity and temperature, saprophytic fungi present on the plant at the time of uprooting, proliferate and secrete enzymes which partially dissolve pectic cements welding the fibers to the wood.

Le teillage a pour rôle essentiel de séparer les fibres du bois. Pour cela, les tiges subissent l'opération de broyage qui casse le bois tout en laissant les fibres intactes, puis elles sont battues pour en faire tomber les anas ou débris ligneux. Le produit utile est le lin teillé ou filasse ; mais un des sous-produits a également une valeur textile : ce sont les étoupes de teillage, fibres plus ou moins courtes, séparées du lin teillé au moment du battage.The main role of scutching is to separate the fibers from the wood. For this, the stems undergo the crushing operation which breaks the wood while leaving the fibers intact, then they are beaten to make the shives fall or woody debris. The useful product is flax or flax; but one of the by-products also has a textile value: these are the weaving tows, more or less short fibers, separated from the dyed flax during threshing.

Le lin teillé dont la longueur apparente est généra- lemant comprise entre 70 cm et 1 mètre, est constitué de faisceaux adhérant entre eux longitudinalement et transversalement. En fait, le lin teillé livré au filateur, correspond à toute la couronne fibreuse de la zone libérienne dans laquelle les fibres élémentaires cellulosiques ne représentent que 70 % en poids, le reste étant des substances non-cellulosiques se décomposant en hémicelluloses, matières pectiques, lignines et éléments minéraux.Dyeed flax, the apparent length of which is generally between 70 cm and 1 meter, consists of bundles adhering to each other longitudinally and transversely. In fact, the dyed flax delivered to the spinning machine, corresponds to the entire fibrous corona of the Liberian zone in which the elementary cellulosic fibers represent only 70% by weight, the rest being non-cellulosic substances decomposing into hemicelluloses, pectic materials, lignins and mineral elements.

C'est cette morphologie fibreuse particulière qui rend le travail du lin très spécifique et pour le moins difficile et coûteux au regard de celui des autres fibres bien connues telles que le coton, la laine et les fibres synthétiques.It is this particular fibrous morphology which makes the work of linen very specific and at the very least difficult and expensive compared to that of other well known fibers such as cotton, wool and synthetic fibers.

Parmi les procédés de filage connus, le lin teillé subit l'opération de peignage dont le rôle est triple : nettoyer la filasse en la débarrassant des dernières traces d'anas; séparer les faisceaux liés entre eux par l'écorce et le parenchyme cortical et par là même, affiner les fibres techniques; éliminer les fibres courtes de pied et de tête que sont les étoupes de peignage.Among the known spinning processes, dyed flax undergoes the combing operation, the role of which is threefold: to clean the tow by ridding it of the last traces of shives; separate the bundles linked together by the cortex and cortical parenchyma and thereby refine the technical fibers; eliminate the short fibers of the foot and head that are the combs.

Cette opération déjà particulièrement onéreuse, présente au surplus, l'inconvénient d'être réalisée sur une machine lourde, peu productive et de conception presque centenaire. Cette machine connue sous le nom de grande peigneuse est très onéreuse à l'achat puisque de dimension imposante et effectuant des opérations alternatives répétées.This already particularly expensive operation, has the additional disadvantage of being carried out on a heavy machine, not very productive and of almost century-old design. This machine known as a large combing machine is very expensive to buy since it is large and performs repeated alternative operations.

Le lin peigné résultant est étalé et la nappe ainsi obtenue est étirée pour fournir un ruban continu.The resulting combed linen is spread out and the tablecloth thus obtained is stretched to provide a continuous ribbon.

Celui-ci est étiré et doublé successivement sur 5 machines appelées bancs d'étirage dont le rôle est triple : améliorer le plus possible la régularité de masse du ruban; réduire progressivement sa masse linéique (ou titre) ; affiner les fibres techniques en clivant les faisceaux fibreux. Cette troisième fonction qui est fondamentale pour permettre une filabilité convenable, est obtenue en étirant le ruban dans un champ d'aiguilles de plus en plus fines au moyen d'un train étireur (acier-bois) travaillant en couche mince.This is stretched and doubled successively on 5 machines called drawing benches whose role is threefold: to improve the mass regularity of the ribbon as much as possible; gradually reduce its linear density (or title); refine the technical fibers by cleaving the fibrous bundles. This third function, which is fundamental to allow suitable spinnability, is obtained by stretching the ribbon in a field of increasingly fine needles by means of a stretching train (steel-wood) working in a thin layer.

Cette opération dans les procédés connus est réalisée sur un matériel très spécifique d'un prix d'achat particulièrement élevé.This operation in known processes is carried out on very specific equipment with a particularly high purchase price.

Le ruban sortant du dernier passage est ensuite étiré sur un banc-à-broches, lui aussi très spécifique et très coûteux, dans le but d'obtenir une mèche légèrement tordue destinée à être travaillée sur métier à filer.The ribbon emerging from the last pass is then stretched on a spindle bench, which is also very specific and very expensive, in order to obtain a slightly twisted wick intended to be worked on a spinning loom.

Pour réaliser un fil fin, il est indispensable que les éléments fibreux constitutifs soient eux-mêmes très fins et proches de la fibre élémentaire. Or, les éléments fibreux composant la mèche écrue, ont une longueur moyenne comprise entre 15 et 20 cm et comportent souvent entre 3 et 10 fibres élémentaires en section. Il est donc nécessaire de dissocier les fibres élémentaires au cours de l'opération de filage ou avant celle-ci.To make a fine wire, it is essential that the constituent fibrous elements are themselves very fine and close to the elementary fiber. However, the fibrous elements making up the unbleached wick have an average length of between 15 and 20 cm and often have between 3 and 10 elementary fibers in section. It is therefore necessary to dissociate the elementary fibers during the spinning operation or before it.

Pour ce faire, on a longtemps filé la mèche écrue au mouillé en la faisant passer dans un bac d'eau portée à une température de 70 °C environ et en l'étirant dans un train de laminage à rouleaux cannelés, à forte pression et à écartement compris entre 65 et 80 mm. Mais cette façon de procéder conduit à des conditions de travail très pénibles et ne permet pas l'obtention de fils plus fins que Nm 21 (48 tex) valablement commercialisables.To do this, the unbleached wick was wet for a long time by passing it through a tank of water brought to a temperature of about 70 ° C. and drawing it in a rolling train with fluted rollers, at high pressure and with spacing between 65 and 80 mm. But this way of proceeding leads to very difficult working conditions and does not allow obtaining thinner yarns than Nm 21 (48 tex) validly marketable.

Depuis deux décennies, la filature industrielle du lin au mouillé est réalisée à partir de mèches ayant subi un traitement chimique de lessivage ou de blanchiment. Les fibres élémentaires ainsi traitées chimiquement, sont partiellement désolidarisées et il est alors possible de filer à l'eau froide et de réaliser des fils plus fins, plus réguliers et plus forts. Cependant, à côté de ses avantages, un tel traitement présente un certain nombre d'inconvénients : il est coûteux, occasionne une perte en matière de l'ordre de 10 % et ne permet pas toujours l'obtention d'un nuance constante.For two decades, the industrial spinning of flax in the wet has been carried out from wicks having undergone a chemical treatment of leaching or bleaching. The elementary fibers thus chemically treated, are partially separated and it is then possible to spin with cold water and to make finer, more regular and stronger threads. However, in addition to its advantages, such a treatment has a certain number of drawbacks: it is expensive, causes a loss of material on the order of 10% and does not always allow a constant shade to be obtained.

Par ailleurs, la production de fils mélangés est plutôt le fait de la filature au sec, laquelle ne permet pas aisément la production de fils fins majoritaires en lin surtout dans les fibres courtes.Furthermore, the production of mixed yarns is rather the result of dry spinning, which does not easily allow the production of majority fine yarns in flax, especially in short fibers.

En bref, tous les procédés actuels de filature de lin utilisés industriellement, présentent de sérieux handicaps : ou bien ils sont très limités en filabilité et ne permettent pas la production de fils fins, ou bien l'obtention de fils fins de qualité n'est possible qu'en mettant en oeuvre des procédés de transformation onéreux à productivité réduite.In short, all the current flax spinning processes used industrially, have serious disadvantages: either they are very limited in spinnability and do not allow the production of fine yarns, or else obtaining fine quality yarns is not possible only by implementing expensive transformation processes with reduced productivity.

Le but principal de la présente invention est de présenter un procédé de filage du lin très économique. Les gains substantiels qui peuvent être réalisés le sont au niveau de la main d'oeuvre réduite et également au niveau des investissements en matériel.The main object of the present invention is to present a very economical method of spinning flax. The substantial gains that can be made are in terms of reduced labor and also in terms of investment in equipment.

En effet, selon l'invention, un grand nombre de manutentions peuvent être supprimées grâce à l'emploi de machines hautement productives telles qu'on les rencontre dans d'autres secteurs d'activités textiles, comme celui de la fibre courte.Indeed, according to the invention, a large number of handling operations can be eliminated thanks to the use of highly productive machines such as are encountered in other sectors of textile activities, such as that of short fiber.

Des économies en matériel peuvent également être réalisées étant donné que l'invention permet de s'affranchir des besoins en machines spécifiques au lin (peignage et préparation).Savings in material can also be made since the invention makes it possible to overcome the needs for machines specific to linen (combing and preparation).

Un autre but de la présente invention est de présenter un procédé de filage du lin qui permette d'obtenir un fil de lin pur ou en mélange d'une propreté jusqu'alors inégalée industriellement, tout en conservant l'aspect du lin traditionnel.Another object of the present invention is to present a process for spinning flax which makes it possible to obtain a pure flax yarn or a blended yarn of a cleanliness hitherto unequaled industrially, while retaining the appearance of traditional flax.

La matière première mise en oeuvre est de la fibre technique de lin très raccourcie de longueur variable et très affinée mécaniquement par exemple en utilisant une ouvreuse (sans aucun traitement chimique ou physico-chimique) dont la longueur et la finesse sont assez proches des caractéristiques de la fibre élémentaire.The raw material used is very short technical flax fiber of variable length and very mechanically refined, for example using an opener (without any chemical or physico-chemical treatment), the length and fineness of which are fairly close to the characteristics of elementary fiber.

Le raccourcissement préalable est réalisé sur des longueurs de l'ordre de 5 à 6 cm puis la matière est affinée c'est-à-dire que le faisceau qui comprenait au départ dix à quarante fibres élémentaires en section est ramené à un élément fibreux beaucoup plus fin et ne comprenant plus que quelques fibres élémentaires.The prior shortening is carried out on lengths of the order of 5 to 6 cm and then the material is refined, that is to say that the bundle which initially comprised ten to forty elementary fibers in section is reduced to a fibrous element much finer and comprising only a few elementary fibers.

Dans le cas de réalisation de fils mélanges, on met aussi en oeuvre une autre fibre naturelle ou de la fibre artificielle ou synthétique, le mélange intime se faisant en tout début de préparation.In the case of production of mixed yarns, another natural fiber or artificial or synthetic fiber is also used, the intimate mixing being carried out at the very start of preparation.

La préparation c'est-à-dire les différentes opérations physiques avant la filature, est dérivée de celle utilisée pour d'autres fibres courtes comme le coton ou d'autres fibres artificielles de même dimension : carde, deux passages d'étirage et banc-à-broches.The preparation, i.e. the different physical operations before spinning, is derived from that used for other short fibers such as cotton or other artificial fibers of the same size: card, two drawing passes and bench -to-pin.

La filature selon l'invention, qui est réalisée après la préparation physique, est dérivée de la filature classique du lin au mouillé : trempage de la mèche à la continue dans de l'eau qui peut être froide ; laminage comportant un système de contrôle d'étirage.The spinning according to the invention, which is carried out after physical preparation, is derived from the conventional spinning of flax in the wet: soaking the wick continuously in water which may be cold; rolling comprising a stretch control system.

La fibre de lin n'a subi aucun traitement chimique ou physico-chimique, elle est écrue et de ce fait, a conservé une bonne partie de ses constituants non- cellulosiques : hémi-celluloses et substances pectiques.Linen fiber has not undergone any chemical or physico-chemical treatment, it is unbleached and therefore has retained a good part of its non-cellulosic constituents: hemi-celluloses and pectic substances.

Elle présente donc plusieurs avantages :

  • - elle n'a pas subi de perte de matière non récupérable importante et conséquemment, son coût est limité,
  • - elle est très accessible à l'eau en raison de sa grande finesse et de sa faible longueur et ne nécessite pas de traitement chimique préalable à la filature,
  • - elle apporte les ciments pectiques qui, après ramollissement et séchage, contribuent à donner plus de cohésion entre les fibres dans le fil.
It therefore has several advantages:
  • - it has not suffered any significant loss of non-recoverable material and consequently, its cost is limited,
  • - it is very accessible to water because of its great finesse and its short length and does not require any chemical treatment prior to spinning,
  • - it provides pectic cements which, after softening and drying, help to give more cohesion between the fibers in the yarn.

Le fil ainsi obtenu a un véritable "aspect lin" même lorsqu'il est réalisé en mélange avec des fibres artificielles ou synthétiques. Cela est dû au fait que la fibre de lin est restée écrue et qu'elle a été filée à l'état mouillé.The yarn thus obtained has a real "linen look" even when it is made in a mixture with artificial or synthetic fibers. This is due to the fact that the flax fiber remained unbleached and that it was spun in the wet state.

Cela confère au fil une haute plus-value technologique et commerciale par rapport au même fil réalisé à l'état sec, car l'aspect du fil obtenu par le procédé de l'invention ressemble beaucoup aux fils de lin traditionnels.This gives the yarn a high technological and commercial added value compared to the same yarn produced in the dry state, because the appearance of the yarn obtained by the process of the invention is very similar to traditional flax yarns.

La filature au mouillé et le séchage subséquent évitent le fixage par vaporisage à chaud qui doit souvent être effectué lorsqu'un fil mélange est réalisé à l'état sec.Wet spinning and subsequent drying avoids hot spray fixing which often has to be done when a blended yarn is made in the dry state.

Parmi les avantages du procédé, on peut citer:

  • - l'aspect du fil et sa régularité sont très proches des mêmes caractéristiques du fil classique lin; en propreté, le fil relevant de l'invention est même supérieur car il ne comporte aucun gros défaut,
  • - le prix du fil se situe entre celui du fil de lin classique et celui du fil de coton, mais cependant plus proche de celui du fil de coton.
Among the advantages of the process, we can cite:
  • - the appearance of the thread and its regularity are very close to the same characteristics of the classic linen thread; in terms of cleanliness, the yarn covered by the invention is even superior because it has no major defects,
  • - the price of the thread is between that of the classic linen thread and that of the cotton thread, but however closer to that of the cotton thread.

D'autres buts et avantages de la présente invention apparaitront au cours de la description qui va suivre qui n'est cependant donnée qu'à titre indicatif et qui n'a pas pour but de la limiter.Other objects and advantages of the present invention will appear during the description which follows which is however given only for information and which is not intended to limit it.

Selon la présente invention, le procédé de filage du lin pur ou en mélange, destiné à l'industrie textile pour la formation d'un fil par torsion des fibres de lin, à partir de faisceaux de fibres longues teillées et agglomérées par des pectines mettant en oeuvre au moins un métier à filer, est caractérisé en ce que:

  • - on réduit mécaniquement par un traitement approprié la longueur des fibres suivie d'une autre opération mécanique de façon à n'obtenir que des fi- brs courtes et excessivement fines,
  • - on carde les fibres courtes pour former un ruban,
  • - on étire le ruban afin d'en réguler la masse linéique et on contrôle les dites fibres courtes durant leur étirage sur le métier à filer,
  • - on tord le ruban pour former une mèche,
  • - on mouille la mèche,
  • - on étire la mèche mouillée et on lui donne une torsion pour former le fil.
According to the present invention, the process for spinning pure or mixed flax, intended for the textile industry for the formation of a yarn by twisting the flax fibers, from bundles of long fibers spotted and agglomerated by pectins using using at least one spinning loom, is characterized in that:
  • the length of the fibers is mechanically reduced by an appropriate treatment followed by another mechanical operation so as to obtain only short and excessively fine fibers,
  • - the short fibers are carded to form a ribbon,
  • the ribbon is stretched in order to regulate the linear mass thereof and the said short fibers are checked during their stretching on the spinning machine,
  • - the ribbon is twisted to form a wick,
  • - we wet the wick,
  • - stretch the wet wick and give it a twist to form the wire.

L'invention sera mieux comprise à la lecture de la description suivante accompagnée d'un dessin en annexe qui schématise le train d'étirage du métier à filer de la présente invention.The invention will be better understood on reading the following description accompanied by an appended drawing which schematizes the drawing train of the spinning machine of the present invention.

La présente invention vise un procédé de filage du lin pur ou en mélange.The present invention relates to a process for spinning pure or mixed flax.

Elle trouvera notamment son application dans l'industrie textile pour la formation d'un fil réalisé par torsion de fibres de lin enchevêtrées.It will in particular find its application in the textile industry for the formation of a thread produced by twist of tangled flax fibers.

La présente invention comporte un grand nombre d'avantages parmi lesquels on peut citer:The present invention has a large number of advantages, among which there may be mentioned:

Le coût de transformation est fortement réduit par rapport à celui du procédé traditionnel, au point d'approcher celui de la filature type fibres courtes.The processing cost is greatly reduced compared to that of the traditional process, to the point of approaching that of short fiber spinning.

Le matériel de peignage et de préparation spécifique au lin, excessivement coûteux à l'achat, consommant beaucoup d'énergie, exigeant énormément d'entretien et nécessitant une main d'oeuvre importante, est exclu du circuit relevant de l'invention. Il est remplacé par un matériel plus léger, fabriqué en grande série et nécessitant une main d'oeuvre et un entretien reduits.Combing and specific linen preparation equipment, excessively expensive to purchase, consuming a lot of energy, requiring a great deal of maintenance and requiring a large workforce, is excluded from the circuit covered by the invention. It is replaced by a lighter material, mass produced and requiring reduced labor and maintenance.

La matière première mise en oeuvre est de la fibre courte, affinée mécaniquement de préférence (sans traitement chimique ou physico-chimique) dont la longueur et la finesse sont assez proches des caractéristiques de la fibre élémentaire. Elle est écrue et de ce fait, n'a pas subi une perte importante et a conservé une bonne partie de ses constituants non- cellulosiques. Conséquemment, son coût est limité; elle est très accessible à l'eau en raison de sa grande finesse et de sa faible longueur et ne nécessite pas de traitement chimique préalable à la filature; elle apporte les ciments pectiques qui, après ramollissement et séchage, contribuent à donner plus de cohésion entre les fibres dans le fil.The raw material used is short fiber, preferably mechanically refined (without chemical or physico-chemical treatment), the length and fineness of which are fairly close to the characteristics of the elementary fiber. It is unbleached and therefore has not suffered a significant loss and has retained a good part of its non-cellulosic constituents. Consequently, its cost is limited; it is very accessible to water because of its great finesse and its short length and does not require chemical treatment prior to spinning; it provides pectic cements which, after softening and drying, help to give more cohesion between the fibers in the yarn.

Le type de préparation utilisé permet de réaliser n'importe quel mélange lin et autres fibres sans aucune difficulté et le mélange fibreux est très homogène.The type of preparation used makes it possible to make any mixture of flax and other fibers without any difficulty and the fibrous mixture is very homogeneous.

Le procédé de filage du lin, grâce au système d'étirage, permet de filer non seulement le lin pur, mais aussi tout type de mélange lin et autres fibres. Le fil ainsi obtenu a un véritable "aspect lin" de même que la toile ou le tricot fait de ce fil. Cela est dû au fait que la fibre de lin est restée naturelle et qu'elle a été filée à l'état mouillé. Cela confère au fil une haute plus-value technologique et commerciale par rapport au même fil réalisé à l'état sec. Par ailleurs, le fil obtenu ne comporte aucun gros défaut par opposition au fil de lin traditionnel.The flax spinning process, thanks to the stretching system, makes it possible to spin not only pure flax, but also any type of mixture of flax and other fibers. The yarn thus obtained has a real "linen look" as does the canvas or knitting made from this yarn. This is due to the fact that the flax fiber remained natural and was spun in the wet state. This gives the yarn a high technological and commercial added value compared to the same yarn made in the dry state. Furthermore, the yarn obtained has no major defects as opposed to traditional flax yarn.

La filature au mouillé et le séchage subséquent évitent le fixage par vaporisage à chaud qui est souvent effectué lorsqu'un fil mélange est réalisé à l'état sec.Wet spinning and subsequent drying avoids fixing by hot spraying, which is often done when a blended yarn is made in the dry state.

Selon le procédé de filage du lin de la présente invention, on part d'une matière première composée de faisceaux de fibres de lin teillées.According to the flax spinning process of the present invention, one starts from a raw material composed of bundles of dyed flax fibers.

Il s'agit de lin ayant été cultivé dans des conditions traditionnelles, qui a subi un rouissage puis un teillage. Les faisceaux de fibres longues sont alors agglomérés par des pectines.It is flax having been cultivated under traditional conditions, which has undergone a retting then a scutching. The bundles of long fibers are then agglomerated by pectins.

La première opération que doivent subir ces fibres consiste en une réduction de leur longueur associée à un affinage. Il faut en effet réduire par traitements appropriés la longueur des fibres qui initialement est de l'ordre de 70 cm à 1 m, à une longueur de fibres courtes c'est-à-dire sensiblement de l'ordre de 2 à 5 cm.The first operation that these fibers must undergo consists in reducing their length associated with refining. The length of the fibers, which initially is of the order of 70 cm to 1 m, must in fact be reduced by appropriate treatments to a length of short fibers, that is to say substantially of the order of 2 to 5 cm.

Cette réduction de longueur se fait mécaniquement par une coupe ou un craquage suivi d'une ouvraison qui réalise l'affinage. Il est nécessaire d'obtenir des fibres courtes et-très fines. Cette première opération ne nécessite généralement pas une intervention chimique ou physico-chimique. Il est en effet nécessaire que la fibre garde ses qualités naturelles afin que le fil résultant possède le "caractère lin" du point de vue de son aspect et de son toucher.This reduction in length is done mechanically by cutting or cracking followed by a process which refines. It is necessary to obtain short and very fine fibers. This first operation does not generally require chemical or physico-chemical intervention. It is indeed necessary that the fiber retains its natural qualities so that the resulting yarn has the "linen character" from the point of view of its appearance and its feel.

Le raccourcissement préalable est réalisé sur des longueurs de l'ordre de 5 à 6 cm puis la matière est affinée c'est-à-dire que le faisceau qui comprenait au départ dix à quarante fibres élémentaires en section est ramené à un élément fibreux beaucoup plus fin et ne comprenant plus que quelques fibres élémentaires.The prior shortening is carried out on lengths of the order of 5 to 6 cm and then the material is refined, that is to say that the bundle which initially comprised ten to forty elementary fibers in section is reduced to a fibrous element much finer and comprising only a few elementary fibers.

Il est ensuite nécessaire de parfaire le nettoyage des fibres, de les paralléliser et d'en produire un voile puis un ruban. Selon le procédé de la présente invention, cela est réalisé sur une carde à haute productivité dérivée de celles utilisées en fibres courtes. L'alimentation et la décharge de la machine sont automatiques ce qui minimise les frais de main d'oeuvre, contrastant ainsi avec le coût élevé du peignage pratiqué en filature traditionnelle.It is then necessary to perfect the cleaning of the fibers, to parallelize them and to produce a veil then a ribbon. According to the process of the present invention, this is carried out on a high productivity card derived from those used in short fibers. The feeding and unloading of the machine is automatic which minimizes labor costs, contrasting with the high cost of combing practiced in traditional spinning.

Le ruban cardé obtenu est ensuite regroupé avec d'autres rubans puis l'ensemble est étiré pour former un nouveau ruban dont la régularité est améliorée. De plus, un ou plusieurs passages peuvent être réalisés pour obtenir un ruban de densité linéaire sensiblement constante.The carded ribbon obtained is then grouped with other ribbons and the assembly is then stretched to form a new ribbon whose regularity is improved. In addition, one or more passes can be made to obtain a ribbon of substantially constant linear density.

Le ruban est ensuite étiré puis légèrement tordu pour former une mèche. Cette phase du procédé peut être réalisée sur bancs à broches.The ribbon is then stretched and slightly twisted to form a wick. This phase of the process can be carried out on pin banks.

L'une des caractéristiques de l'invention est de filer à l'état mouillé cette mèche de fibres courtes. Pour ce faire, la mèche passe d'abord dans un bac d'eau qui peut être froide, intégré au métier à filer, puis elle est étirée dans un train de laminage conçu pour travailler au mieux ce type de matériau.One of the characteristics of the invention is to spin this wick of short fibers in the wet state. To do this, the wick first passes through a water tank which can be cold, integrated into the spinning machine, then it is stretched in a rolling train designed to work this type of material as well as possible.

Comme cela a été décrit précédemment, le travail du lin en fibres courtes sur métier à filer requiert quelques précautions. En particulier, le contrôle des fibres courtes est nécessaire durant leur passage dans le train d'étirage du métier à filer.As described above, working with short fiber flax on a spinning machine requires some precautions. In particular, control of the short fibers is necessary during their passage through the drawing train of the spinning machine.

La figure 1 schématise un train d'étirage de métier à filer. Une bobine 1 de mèche de banc à broches sert à l'alimentation du train d'étirage 2 qui délivre un fil 3 qui s'enroule autour d'un fuseau 4.Figure 1 shows schematically a drawing machine of spinning loom. A spool 1 of a bench bit wick is used to power the drawing train 2 which delivers a wire 3 which is wound around a spindle 4.

Selon l'invention, le contrôle des fibres courtes est réalisé grâce à l'utilisation d'un train d'étirage 2 à manchon 5. Le train d'étirage à manchon permet en effet d'assurer le guidage des fibres courtes.According to the invention, the control of the short fibers is achieved by the use of a drawing train 2 with sleeve 5. The drawing train with sleeve in fact makes it possible to guide the short fibers.

La mèche subit un pré-étirage entre les cylindres d'alimentation 6 et les manchons 5 puis un étirage proprement dit entre les manchons 5 et les cylindres délivreurs 7.The wick undergoes a pre-stretching between the supply cylinders 6 and the sleeves 5 and then a proper stretching between the sleeves 5 and the delivery cylinders 7.

Pour améliorer le contrôle des fibres, le parcours de celles-ci dans le train d'étirage 2 se réalise selon un arc de cercle.To improve the control of the fibers, the path of these in the drawing train 2 is carried out in an arc.

Claims (6)

1. Process for spinning pure or blended flax, designed for the textile industry to form a yarn by twisting flax fibres from bundles of long fibres swin- gled and agglomerated by pectins, implementing at least one spinning frame, characterized in that:
- the length of the fibres is mechanically reduced by a suitable treatment, followed by another mechanical operation so as to obtain only short, extremely fine fibres,
- the short fibres are carded to form a ribbon,
- the ribbon is drawn to adjust its weight per unit length and the said short fibres are controlled while they are being drawn on the spinning frame,
- the ribbon is twisted to form a roving,
- the roving is wetted,
- the wetted roving is drawn and is twisted to form the yarn.
2. Flax spinning process according to claim 1, characterized in that the flax roving is wetted with cold water.
3. Flax spinning process according to claim 1, characterized in that the short fibres are inspected while they are being drawn on a spinning frame by passing through a drawing train (2) having a sleeve (5).
4. Flax spinning process according to claim 1, characterized in that the unbleached fibres are given length and fineness properties close to those of the elementary fibre.
5. Flax spinning process according to claim 1, characterized by the fact that the length of the fibres is between 1.5 and 5 cm.
6. Spinning process according to claim 1, characterized by the fact that the roving describes an arc of a circle during its passage through the drawing train (2).
EP86440019A 1986-02-14 1986-03-05 Method for spinning flax or mixtures thereof Expired EP0234170B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AT86440019T ATE47434T1 (en) 1986-02-14 1986-03-05 PROCESS FOR SPINNING PURE OR MIXED FLAX FIBERS.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR8602281 1986-02-14
FR8602281A FR2594448B1 (en) 1986-02-14 1986-02-14 PROCESS FOR SPINNING PURE LINEN OR MIXTURE

Publications (2)

Publication Number Publication Date
EP0234170A1 EP0234170A1 (en) 1987-09-02
EP0234170B1 true EP0234170B1 (en) 1989-10-18

Family

ID=9332312

Family Applications (1)

Application Number Title Priority Date Filing Date
EP86440019A Expired EP0234170B1 (en) 1986-02-14 1986-03-05 Method for spinning flax or mixtures thereof

Country Status (5)

Country Link
EP (1) EP0234170B1 (en)
AT (1) ATE47434T1 (en)
DE (1) DE3666467D1 (en)
ES (1) ES2000127A6 (en)
FR (1) FR2594448B1 (en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2734846B1 (en) * 1995-05-31 1997-08-22 Teillage Du Neubourg Soc Coop FLAX LINED FIBERS AND METHOD OF PREPARATION
DE19546153A1 (en) * 1995-11-29 1997-06-05 Windi Winderlich Gmbh Process for wet spinning sclerenchyma fibers, especially flax
GB2314094A (en) * 1996-06-11 1997-12-17 Yarns Killyleagh Spinning flax
JP2007107145A (en) * 2005-10-14 2007-04-26 Kawasaki Nenshi Kk Method for spinning
CA2698308A1 (en) * 2007-08-20 2009-02-26 Jiangsu Redbud Textile Technology Co., Ltd. Bast fibre yarn, multi-fibre yarn and process for making the same eof
CN103088499B (en) * 2012-11-05 2015-05-27 杭州商辂丝绸有限公司 Method for preparing mixed-color single yarns and device for implementing method
CN104195707B (en) * 2014-08-13 2016-06-22 武汉纺织大学 A kind of damp and hot drawing-off Fushun formula improves the post-treatment method of ring ingot spun yarn structure
CN107151840B (en) * 2017-07-06 2019-04-16 武汉纺织大学 A kind of liquid film Yarn spinning method

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE332058A (en) *
FR663810A (en) * 1928-11-12 1929-08-26 Process for spinning flax and other textile fibers
GB579797A (en) * 1944-12-29 1946-08-15 Mackie & Sons Ltd J Improvements relating to the wet spinning of flax
US2721440A (en) * 1951-02-13 1955-10-25 American Viscose Corp Process for producing direct spun yarns from strands of continuous fibers
GB1076842A (en) * 1963-05-08 1967-07-26 Mackie & Sons Ltd J Improvements relating to spining
BG40087A1 (en) * 1983-05-26 1986-10-15 Iliev Method for manufacture of fine jute and jute type yarns

Also Published As

Publication number Publication date
FR2594448B1 (en) 1988-10-07
DE3666467D1 (en) 1989-11-23
EP0234170A1 (en) 1987-09-02
ATE47434T1 (en) 1989-11-15
ES2000127A6 (en) 1987-12-16
FR2594448A1 (en) 1987-08-21

Similar Documents

Publication Publication Date Title
CN102534905B (en) Cashmere-Apocynum venetum roving blended yarn
EP0234170B1 (en) Method for spinning flax or mixtures thereof
FR2666100A1 (en) PROCESS FOR PRODUCING ANGORA RABBIT HAIR YARN.
US2044130A (en) Textile yarn and the manufacture thereof
EP0317681B1 (en) Method and apparatus for the continuous preparation of plant stalks
KR102475234B1 (en) A method for manufacturing kudzu fiber, a method for manufacturing kudzu spun yarn including the same, and a fabric prepared therefrom
EP0527666B1 (en) Linen yarn wet production method and linen yarn so obtained
US1795528A (en) Process of producing fiber and yarn from unretted flax plants
EP0745709B1 (en) Flax fiber lint and preparation method
BE342080A (en)
BE1024457B1 (en) PROCESS FOR TREATING FLAX, LINEN AND LINEN FIBER
CN112981641B (en) Preparation method of cashmere and alpaca blended fiber
JPH02242982A (en) Production of cotton yarn material, roving, cotton yarn and cotton cloth
Eyre The modern treatment of flax from the time of harvesting to the completion of spinning
BE458543A (en) New textile articles such as horsehair, straws, ribbons, etc.
Ghodke et al. Research trends in silk spinning process: A review
BE434725A (en)
BE408283A (en)
BE412872A (en)
Gibson Flax from Fibre to Fabric
BE434726A (en)
CN108914369A (en) A kind of production technology of silk spunlace non-woven cloth
BE648109A (en)
Caldwell FLAX FIBRE CHARACTERISTICS: THEIR BEARING ON THE PRODUCTION AND PROPERTIES OF WET SPUN YARNS
BE415599A (en)

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 19870312

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AT BE CH DE GB IT LI LU NL SE

TCNL Nl: translation of patent claims filed
17Q First examination report despatched

Effective date: 19881129

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AT BE CH DE GB IT LI LU NL SE

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SE

Effective date: 19891018

Ref country code: NL

Effective date: 19891018

Ref country code: GB

Effective date: 19891018

Ref country code: AT

Effective date: 19891018

REF Corresponds to:

Ref document number: 47434

Country of ref document: AT

Date of ref document: 19891115

Kind code of ref document: T

ITF It: translation for a ep patent filed

Owner name: UFFICIO BREVETTI RICCARDI & C.

REF Corresponds to:

Ref document number: 3666467

Country of ref document: DE

Date of ref document: 19891123

NLV1 Nl: lapsed or annulled due to failure to fulfill the requirements of art. 29p and 29m of the patents act
PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LI

Effective date: 19900331

Ref country code: CH

Effective date: 19900331

GBV Gb: ep patent (uk) treated as always having been void in accordance with gb section 77(7)/1977 [no translation filed]
PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

26N No opposition filed
REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

ITTA It: last paid annual fee
PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 19930319

Year of fee payment: 8

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: BE

Payment date: 19930409

Year of fee payment: 8

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: LU

Payment date: 19930421

Year of fee payment: 8

EPTA Lu: last paid annual fee
PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LU

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 19940305

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: BE

Effective date: 19940331

BERE Be: lapsed

Owner name: SALMON LEON

Effective date: 19940331

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: DE

Effective date: 19941201

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES;WARNING: LAPSES OF ITALIAN PATENTS WITH EFFECTIVE DATE BEFORE 2007 MAY HAVE OCCURRED AT ANY TIME BEFORE 2007. THE CORRECT EFFECTIVE DATE MAY BE DIFFERENT FROM THE ONE RECORDED.

Effective date: 20050305