EA200701842A1 - Модульное устройство для непрерывной дегазации и получения полимерных форконденсатов с реакционно-технически высоким соотношением между площадью поверхности продукта и его объёмом при щадящей обработке продукта реакции - Google Patents

Модульное устройство для непрерывной дегазации и получения полимерных форконденсатов с реакционно-технически высоким соотношением между площадью поверхности продукта и его объёмом при щадящей обработке продукта реакции

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Publication number
EA200701842A1
EA200701842A1 EA200701842A EA200701842A EA200701842A1 EA 200701842 A1 EA200701842 A1 EA 200701842A1 EA 200701842 A EA200701842 A EA 200701842A EA 200701842 A EA200701842 A EA 200701842A EA 200701842 A1 EA200701842 A1 EA 200701842A1
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EA
Eurasian Patent Office
Prior art keywords
product
surface area
reactor
volume
modular
Prior art date
Application number
EA200701842A
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English (en)
Other versions
EA012362B1 (ru
Inventor
Михаэль Штренг
Клиффорд Шэферскюппер
Штефан Биллер
Андреас Хильперт
Original Assignee
Эпк Индастриал Энджиниринг Гмбх
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Application filed by Эпк Индастриал Энджиниринг Гмбх filed Critical Эпк Индастриал Энджиниринг Гмбх
Publication of EA200701842A1 publication Critical patent/EA200701842A1/ru
Publication of EA012362B1 publication Critical patent/EA012362B1/ru

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/245—Stationary reactors without moving elements inside placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/247—Suited for forming thin films
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/02—Feed or outlet devices therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
    • B01J8/12—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by gravity in a downward flow
    • B01J8/125—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by gravity in a downward flow with multiple sections one above the other separated by distribution aids, e.g. reaction and regeneration sections
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/785—Preparation processes characterised by the apparatus used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00018—Construction aspects
    • B01J2219/0002—Plants assembled from modules joined together
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00018—Construction aspects
    • B01J2219/00024—Revamping, retrofitting or modernisation of existing plants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00121—Controlling the temperature by direct heating or cooling
    • B01J2219/00123—Controlling the temperature by direct heating or cooling adding a temperature modifying medium to the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00168—Controlling or regulating processes controlling the viscosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00245—Avoiding undesirable reactions or side-effects
    • B01J2219/00247—Fouling of the reactor or the process equipment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00245—Avoiding undesirable reactions or side-effects
    • B01J2219/00252—Formation of deposits other than coke
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/185—Details relating to the spatial orientation of the reactor vertical
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2461—Heat exchange aspects
    • B01J2219/2462—Heat exchange aspects the reactants being in indirect heat exchange with a non reacting heat exchange medium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)

Abstract

В заявке описано модульное устройство для непрерывной дегазации продуктов реакции карбоновой кислоты или дикарбоновых кислот с полифункциональным спиртом, которое может использоваться для получения форконденсатов (или же форполимеров) и в котором благодаря особой конструкции и особому расположению модульных днищ обеспечивается реакционно-технически высокое соотношение между площадью поверхности продукта и его объемом, при котором (соотношении) характеристическая вязкость продукта реакции составляет от 0,20 до 0,35 дл/г. Такое устройство имеет стандартизированную модульную конструкцию и состоит по меньшей мере из 3 модулей, которые обеспечивают небольшой перепад температур между массой продукта и теплоносителем и которыми являются загрузочный модуль для подачи продукта в реактор, нагреваемый кубовый модуль для сбора в нем и отбора из него продукта и головной модуль для сбора и выпуска выпара. Реактор при необходимости последующего повышения его производительности можно дооснащать неглубокими дополнительными модулями, обеспечивающими дополнительное увеличение реакционно-активной поверхности продукта. Подобное устройство обеспечивает наличие большой удельной поверхности продукта для максимизации массообмена низкокипящих компонентов продукта при одновременном исключении налипания на внутренние стенки реактора сконденсировавшихся и затвердевших компонентов продукта.
EA200701842A 2005-03-22 2006-03-22 Модульное устройство для непрерывной дегазации и получения полимерных форконденсатов с реакционно-технически высоким соотношением между площадью поверхности продукта и его объёмом при щадящей обработке продукта реакции EA012362B1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102005013764A DE102005013764B3 (de) 2005-03-22 2005-03-22 Modulare Vorrichtung zur kontinuierlichen Entgasung und Herstellung polymerer Vorkondensate, mit reaktionstechnisch hohem Verhältnis Produktoberfläche zu Volumen, bei schonender Behandlung der Reaktionsproduktmasse
PCT/EP2006/002832 WO2006100105A1 (de) 2005-03-22 2006-03-22 Modulare vorrichtung zur kontinuierlichen entgasung und herstellung polymerer vorkondensate, mit reaktions technisch hohem verhältnis produktoberfläche zu volumen, bei schonender behandlung der reaktionsproduktmasse

Publications (2)

Publication Number Publication Date
EA200701842A1 true EA200701842A1 (ru) 2008-12-30
EA012362B1 EA012362B1 (ru) 2009-10-30

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Family Applications (1)

Application Number Title Priority Date Filing Date
EA200701842A EA012362B1 (ru) 2005-03-22 2006-03-22 Модульное устройство для непрерывной дегазации и получения полимерных форконденсатов с реакционно-технически высоким соотношением между площадью поверхности продукта и его объёмом при щадящей обработке продукта реакции

Country Status (6)

Country Link
US (1) US8124018B2 (ru)
EP (1) EP1861195A1 (ru)
CN (1) CN101146602B (ru)
DE (1) DE102005013764B3 (ru)
EA (1) EA012362B1 (ru)
WO (1) WO2006100105A1 (ru)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20150051367A1 (en) * 2011-06-10 2015-02-19 Clive Alexander Hamilton Variable pressure drop up flow-pre-polymerizer (ufpp) systems and methods
US20130196053A1 (en) * 2012-01-10 2013-08-01 State of Oregon acting by and through the State Board of Higher Education on behalf of Oregon Stat Flow cell design for uniform residence time fluid flow
CN103361264B (zh) * 2012-03-30 2014-12-31 北京愿景宏能源环保科技发展有限公司 一种可调整容积的发酵罐及其控制装置和方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2727882A (en) * 1952-10-14 1955-12-20 Du Pont Process and apparatus for the continuous polymerization of bis-2-hydroxyethyl terephthalate
NL108873C (ru) * 1957-01-17
BE632261A (ru) * 1962-05-11
FR1357905A (fr) * 1962-05-11 1964-04-10 Hoechst Ag Appareil de réaction pour la préparation de polyphtalates d'éthylène
US3359074A (en) * 1963-06-11 1967-12-19 Monsanto Co Polycondensation apparatus
US3651125A (en) * 1968-08-12 1972-03-21 Eastman Kodak Co Continuous method for formation of a liquid monomer for a condensation polymer
US3620283A (en) * 1969-02-04 1971-11-16 Artisan Ind Falling film evaporator stripper
US4158092A (en) * 1974-07-25 1979-06-12 Hoechst Aktiengesellschaft Process for the manufacture of vinyl chloride polymer dispersions with a low monomer content
DE2504258A1 (de) * 1975-02-01 1976-08-05 Dynamit Nobel Ag Verfahren und apparatur zur herstellung von oligomeren alkylenterephthalaten
US5310955A (en) * 1991-01-18 1994-05-10 The Dow Chemical Company Vertical continuous reactor and process for liquid epoxy resin
DE10155419B4 (de) * 2001-11-12 2005-06-16 Inventa-Fischer Gmbh & Co. Kg Verfahren zur kontinuierlichen Herstellung von hochmolekularem Polyester sowie Vorrichtung zur Durchführung des Verfahrens

Also Published As

Publication number Publication date
WO2006100105A1 (de) 2006-09-28
US8124018B2 (en) 2012-02-28
CN101146602B (zh) 2011-03-09
US20090047186A1 (en) 2009-02-19
CN101146602A (zh) 2008-03-19
EP1861195A1 (de) 2007-12-05
EA012362B1 (ru) 2009-10-30
DE102005013764B3 (de) 2006-10-12

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