DK2361298T3 - Fremgangsmåde til reducering af 3-MCPD-indholdet i raffinerede planteolier - Google Patents

Fremgangsmåde til reducering af 3-MCPD-indholdet i raffinerede planteolier Download PDF

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Publication number
DK2361298T3
DK2361298T3 DK09771302.8T DK09771302T DK2361298T3 DK 2361298 T3 DK2361298 T3 DK 2361298T3 DK 09771302 T DK09771302 T DK 09771302T DK 2361298 T3 DK2361298 T3 DK 2361298T3
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DK
Denmark
Prior art keywords
oil
bleaching
acid
mcpd
process according
Prior art date
Application number
DK09771302.8T
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English (en)
Inventor
Klaus Schurz
Original Assignee
Süd-Chemie IP GmbH & Co KG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Süd-Chemie IP GmbH & Co KG filed Critical Süd-Chemie IP GmbH & Co KG
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Publication of DK2361298T3 publication Critical patent/DK2361298T3/da

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/006—Refining fats or fatty oils by extraction
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/10—Refining fats or fatty oils by adsorption
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/12—Refining fats or fatty oils by distillation
    • C11B3/14—Refining fats or fatty oils by distillation with the use of indifferent gases or vapours, e.g. steam

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Paper (AREA)

Claims (10)

1. Fremgangsmåde til reducering af 3-monochlorpropan-1,2-diol-indholdet i raffinerede planteolier, hvor en rå olie først afslimes, således at der opnås en afslimet olie, det afslimede olie blandes med en blegejord og bleges, hvorved der opnås en bleget olie, blegejorden frasepareres fra den blegede olie, således at der opnås en filterolie, og filterolien desodoriseres, kendetegnet ved, at - der til afslimningen tilsættes vand til den rå olie, og afslimningen udføres uden tilsætning af syre ved en temperatur på mindre end 70 °C, - den afslimede olie opvarmes til en temperatur i området fra 80 til 110 °C, og blegejorden tilsættes til den opvarmede afslimede olie i en mængde på mere end 1,5 vægt-%, - blegningen udføres ved en temperatur i området fra 80 til 100 °C.
2. Fremgangsmåde ifølge krav 1, kendetegnet ved, at der med henblik på afslimningen tilsættes vand til den rå olie i en mængde på mindre end 15 vægt-%.
3. Fremgangsmåde ifølge krav 1 eller 2, kendetegnet ved, at den afslimede olie frasepareres fra en vandig fase.
4. Fremgangsmåde ifølge et af de foregående krav, kendetegnet ved, at blegejorden har en specifik overflade på mere end 175 m2/g.
5. Fremgangsmåde ifølge et af de foregående krav, kendetegnet ved, at blegejorden har et porevolumen på mere end 0,2 ml/g.
6. Fremgangsmåde ifølge et af de foregående krav, kendetegnet ved, at blegejordens ionbytningskapacitet udgør mere end 15 meq/100g.
7. Fremgangsmåde ifølge et af de foregående krav, kendetegnet ved, at blegejorden er en syreaktiveret blegejord.
8. Fremgangsmåde ifølge krav 7, kendetegnet ved, at den syreaktiverede blegejord er en HPBE.
9. Fremgangsmåde ifølge et af de foregående krav, kendetegnet ved, at olien er en planteolie.
10. Fremgangsmåde ifølge et af de foregående krav, kendetegnet ved, at olien er palmeolie.
DK09771302.8T 2008-12-02 2009-12-01 Fremgangsmåde til reducering af 3-MCPD-indholdet i raffinerede planteolier DK2361298T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102008060059A DE102008060059A1 (de) 2008-12-02 2008-12-02 Verfahren zur Reduzierung des 3-MCPD-Gehalts in raffinierten Pflanzenölen
PCT/EP2009/008557 WO2010063450A1 (de) 2008-12-02 2009-12-01 Verfahren zur reduzierung des 3-mcpd-gehalts in raffinierten pflanzenöllen

Publications (1)

Publication Number Publication Date
DK2361298T3 true DK2361298T3 (da) 2017-07-24

Family

ID=41728488

Family Applications (1)

Application Number Title Priority Date Filing Date
DK09771302.8T DK2361298T3 (da) 2008-12-02 2009-12-01 Fremgangsmåde til reducering af 3-MCPD-indholdet i raffinerede planteolier

Country Status (8)

Country Link
EP (1) EP2361298B1 (da)
DE (1) DE102008060059A1 (da)
DK (1) DK2361298T3 (da)
ES (1) ES2637347T3 (da)
HU (1) HUE035623T2 (da)
PL (1) PL2361298T3 (da)
PT (1) PT2361298T (da)
WO (1) WO2010063450A1 (da)

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ES2424671T3 (es) 2009-06-30 2013-10-07 Sime Darby Malaysia Berhad Proceso para la eliminación de componentes no deseados de propanol de aceite de triglicéridos sin usar
KR101795819B1 (ko) * 2009-09-30 2017-11-09 후지세유 그룹 혼샤 가부시키가이샤 글리세리드 유지 중의 클로로프로판올류 및 그 형성 물질, 글리시돌 지방산 에스테르를 저감하는 방법
CN102334563B (zh) 2010-07-16 2015-03-25 丰益(上海)生物技术研发中心有限公司 控制油脂中3-氯-1,2-丙二醇或其酯含量的方法
CZ303281B6 (cs) * 2010-10-27 2012-07-11 Vysoká škola chemicko-technologická v Praze Zpusob zabránení vzniku acylderivátu monochlorpropandiolu pri vysokoteplotních úpravách oleju a tuku
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DK3388502T3 (da) * 2011-02-10 2021-05-31 Cargill Inc Fremgangsmåde til reduktion af indholdet af 3-mcpd-glycidylester i olier
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MY159241A (en) * 2011-07-29 2016-12-30 Nisshin Oillio Group Ltd Purified glyceride composition and method for producing purified glyceride composition
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WO2014012548A1 (en) 2012-07-18 2014-01-23 Aarhuskarlshamn Ab Reduction of mcpd-compounds in refined plant oil for food
WO2014081279A1 (en) 2012-11-21 2014-05-30 Universiti Putra Malaysia An improved palm oil refining process
CN103525548B (zh) * 2013-11-06 2014-10-01 江南大学 一种用于降低植物油中氯源及3-氯-1,2-丙二醇酯前体物质含量的脱胶方法
LT3154374T (lt) 2014-05-16 2018-12-10 Sime Darby Malaysia Berhad Neapdoroto palmių vaisių aliejaus produkto rafinavimo būdas
EP3098292A1 (en) 2015-05-27 2016-11-30 Evonik Degussa GmbH A process for refining glyceride oil comprising a basic quaternary ammonium salt treatment
EP3098293A1 (en) 2015-05-27 2016-11-30 Evonik Degussa GmbH A process for removing metal from a metal-containing glyceride oil comprising a basic quaternary ammonium salt treatment
GB2538758A (en) 2015-05-27 2016-11-30 Green Lizard Tech Ltd Process for removing chloropropanols and/or glycidol
EP3341457A4 (en) 2015-08-25 2019-05-01 DSM IP Assets B.V. REFINED OIL COMPOSITIONS AND METHODS OF MAKING SAME
WO2018156013A1 (en) 2017-02-21 2018-08-30 Sime Darby Plantation Berhad Process for producing refined palm fruit oil
ES2770068T3 (es) 2017-08-23 2020-06-30 Bunge Loders Croklaan B V Proceso para refinar aceite vegetal con supresión de impurezas no deseadas
EP3483237A1 (de) 2017-11-10 2019-05-15 Evonik Degussa GmbH Verfahren zur extraktion von fettsäuren aus triglyceridölen
WO2019157141A1 (en) * 2018-02-07 2019-08-15 Cargill, Incorporated Liquid oils without unwanted contaminants
BR112020015727A2 (pt) * 2018-02-07 2020-12-08 Cargill, Incorporated Processo para a preparação de um óleo vegetal purificado, e, uso de um adsorvente
EP3790947B1 (en) 2018-05-07 2021-11-10 Arisdyne Systems, Inc. Methods for refined palm oil production with reduced 3-mcpd formation
PL238351B1 (pl) 2018-08-27 2021-08-09 Komagra Spolka Z Ograniczona Odpowiedzialnoscia Sposób wytwarzania rafinowanego oleju jadalnego o niskiej zawartości niepożądanych 3-MPCD, 2-MPCD oraz glicydów
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Also Published As

Publication number Publication date
PL2361298T3 (pl) 2017-10-31
DE102008060059A1 (de) 2010-06-10
EP2361298B1 (de) 2017-05-17
ES2637347T3 (es) 2017-10-11
WO2010063450A1 (de) 2010-06-10
PT2361298T (pt) 2017-08-25
EP2361298A1 (de) 2011-08-31
HUE035623T2 (en) 2018-05-28

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