DE929092C - Process for the production of polyamide solutions - Google Patents

Process for the production of polyamide solutions

Info

Publication number
DE929092C
DE929092C DEK11674D DEK0011674D DE929092C DE 929092 C DE929092 C DE 929092C DE K11674 D DEK11674 D DE K11674D DE K0011674 D DEK0011674 D DE K0011674D DE 929092 C DE929092 C DE 929092C
Authority
DE
Germany
Prior art keywords
water
trichloroethanol
production
parts
alcohols
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DEK11674D
Other languages
German (de)
Inventor
Edgar Dr Krumbein
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kalle GmbH and Co KG
Original Assignee
Kalle GmbH and Co KG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kalle GmbH and Co KG filed Critical Kalle GmbH and Co KG
Priority to DEK11674D priority Critical patent/DE929092C/en
Application granted granted Critical
Publication of DE929092C publication Critical patent/DE929092C/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/02Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/09Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in organic liquids
    • C08J3/091Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in organic liquids characterised by the chemical constitution of the organic liquid
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2377/00Characterised by the use of polyamides obtained by reactions forming a carboxylic amide link in the main chain; Derivatives of such polymers

Description

Verfahren zur Herstellung von Polyamidlösungen Nach dem Verfahren des Patents goS 067 verwendet man zur Herstellung von Polyamidlösungen als Lösungsmittel Trichloräthanol, gegebenenfalls in Mischung mit Alkoholen und/oder halogenierten Kohlenwasserstoffen, oder Chloralhydrat in Mischung mit Trichloräthanol und/oder Alkoholen und/oder halogenierten Kohlenwasserstoffen.Process for the production of polyamide solutions According to the procedure of GoS 067 patents are used as a solvent for the production of polyamide solutions Trichloroethanol, optionally mixed with alcohols and / or halogenated Hydrocarbons, or chloral hydrate mixed with trichloroethanol and / or Alcohols and / or halogenated hydrocarbons.

Es wurde nun gefunden, daß man Polyamidlösungen auch herstellen kann, indem man als Lösungsmittel Trichloräthanol anstatt in Verdünnung mit Alkoholen undXoder mit halogenierten Kohlenwasserstoffen in Mischung mit Wasser und gegebenenfalls zusätzlich Chloralhydrat oder aber letzteres anstatt in Verdünnung mit Trichloräthanol und/oder Alkoholen und/oder halogenierten Kohlenwasserstoffen ebenfalls in Mischung mit Wasser verwendet. It has now been found that polyamide solutions can also be produced by using trichloroethanol as a solvent instead of diluting it with alcohols andXor with halogenated hydrocarbons mixed with water and optionally additionally chloral hydrate or the latter instead of diluted with trichloroethanol and / or alcohols and / or halogenated hydrocarbons, likewise in a mixture used with water.

Wenn man Trichloräthanol und Chloralhydrat bzw. aus beiden Stoffen bestehende Gemische mit Wasser verschneidet, so tritt nicht eine Beeinträchtigung der Lösewirkung auf, sondern es konnte im Gegenteil festgestellt werden, daß durch den Zusatz von Wasser die Polynmidlösungen sich sogar leichter herstellen lassen. Das Wasser kann in einer Menge bis zu 40 ovo zugesetzt werden. If you have trichloroethanol and chloral hydrate or from both substances If existing mixtures are mixed with water, there is no impairment the dissolving effect on, but on the contrary it could be established that by the addition the polynmide solutions are even easier to produce with water permit. The water can be added in an amount up to 40 ovo.

Beispiele I. Es werden 60 Teile Chloralhydrat mit 20 Teilen Wasser und 20 Teilen Polyhexamethylenadipinamid I Stunde bis zur klaren Lösung verrührt. Examples I. 60 parts of chloral hydrate with 20 parts of water and 20 parts of polyhexamethylene adipamide 1 hour stirred until a clear solution.

2. 50 Teile Chloralhydrat werden mit 40 Teilen Wasser und 10 Teilen Polyhexamethylenadipinamid vermischt und bis zur klaren Lösung gerührt. 2. 50 parts of chloral hydrate are mixed with 40 parts of water and 10 parts Polyhexamethylene adipamide mixed and stirred until a clear solution.

3. 40 Teile Chloralhydrat, 20 Teile Wasser, 20 Teile Trichloräthanol und 20 Teile Polyhexamethylenadipinamid werden etwa I Stunde miteinander verrührt, bis eine klare Lösung entstanden ist, die auf Filme verarbeitet werden kann. 3. 40 parts of chloral hydrate, 20 parts of water, 20 parts of trichloroethanol and 20 parts of polyhexamethylene adipamide are stirred together for about 1 hour, until a clear solution is obtained that can be processed onto films.

Claims (1)

PATENTANSPRUCH: Weitere Ausgestaltung des Verfahrens zur Herstellung von Polyamidlösungen nach Patent 908 067, dadurch gekennzeichnet, daß man als Lösungsmittel Trichloräthanol anstatt in Verdünnung mit Alkoholen und/oder halogenierten Kohlenwasserstoffen in Mischung mit Wasser und gegebenenfalls zusätzlich Chloralhydrat oder aber letzteres anstatt in Verdünnung mit Trichloräthanol und/oder Alkoholen und/oder halogenierten Kohlenwasserstoffen ebenfalls in Mischung mit Wasser verwendet. PATENT CLAIM: Further development of the manufacturing process of polyamide solutions according to Patent 908 067, characterized in that the solvent Trichloroethanol instead of diluted with alcohols and / or halogenated hydrocarbons in a mixture with water and optionally also chloral hydrate or the latter instead of being diluted with trichloroethanol and / or alcohols and / or halogenated Hydrocarbons are also used in admixture with water. Angezogene Druckschriften: Deutsche Patentschrift Nr. 908 067. Referenced publications: German patent specification No. 908 067.
DEK11674D 1941-08-08 1941-08-08 Process for the production of polyamide solutions Expired DE929092C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DEK11674D DE929092C (en) 1941-08-08 1941-08-08 Process for the production of polyamide solutions

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEK11674D DE929092C (en) 1941-08-08 1941-08-08 Process for the production of polyamide solutions

Publications (1)

Publication Number Publication Date
DE929092C true DE929092C (en) 1955-06-20

Family

ID=7213432

Family Applications (1)

Application Number Title Priority Date Filing Date
DEK11674D Expired DE929092C (en) 1941-08-08 1941-08-08 Process for the production of polyamide solutions

Country Status (1)

Country Link
DE (1) DE929092C (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1107399B (en) * 1957-03-27 1961-05-25 Du Pont Process for dissolving nitrogen-containing polycondensation products

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE908067C (en) * 1941-02-07 1954-05-06 Kalle & Co Ag Process for the production of polyamide solutions

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE908067C (en) * 1941-02-07 1954-05-06 Kalle & Co Ag Process for the production of polyamide solutions

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1107399B (en) * 1957-03-27 1961-05-25 Du Pont Process for dissolving nitrogen-containing polycondensation products

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