DE69931165T2 - Herstellung von organolithium- und organophosphor-derivaten - Google Patents

Herstellung von organolithium- und organophosphor-derivaten Download PDF

Info

Publication number
DE69931165T2
DE69931165T2 DE69931165T DE69931165T DE69931165T2 DE 69931165 T2 DE69931165 T2 DE 69931165T2 DE 69931165 T DE69931165 T DE 69931165T DE 69931165 T DE69931165 T DE 69931165T DE 69931165 T2 DE69931165 T2 DE 69931165T2
Authority
DE
Germany
Prior art keywords
group
compound
hal
general formula
alkyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69931165T
Other languages
German (de)
English (en)
Other versions
DE69931165D1 (de
Inventor
Eilenberg
Roelof Van Ginkel
Willem Alexander VAN DER MADE
Jan De With
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SRI International Inc
Original Assignee
SRI International Inc
Stanford Research Institute
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SRI International Inc, Stanford Research Institute filed Critical SRI International Inc
Publication of DE69931165D1 publication Critical patent/DE69931165D1/de
Application granted granted Critical
Publication of DE69931165T2 publication Critical patent/DE69931165T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F1/00Compounds containing elements of Groups 1 or 11 of the Periodic Table
    • C07F1/02Lithium compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/46Phosphinous acids [R2POH], [R2P(= O)H]: Thiophosphinous acids including[R2PSH]; [R2P(=S)H]; Aminophosphines [R2PNH2]; Derivatives thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/504Organo-phosphines containing a P-P bond
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/505Preparation; Separation; Purification; Stabilisation
    • C07F9/5063Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds
    • C07F9/5068Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds from starting materials having the structure >P-Hal
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/505Preparation; Separation; Purification; Stabilisation
    • C07F9/5063Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds
    • C07F9/5077Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds from starting materials having the structure P-Metal, including R2P-M+
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/505Preparation; Separation; Purification; Stabilisation
    • C07F9/5086Preparation; Separation; Purification; Stabilisation from phosphonium salts as starting materials
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/54Quaternary phosphonium compounds
    • C07F9/5463Compounds of the type "quasi-phosphonium", e.g. (C)a-P-(Y)b wherein a+b=4, b>=1 and Y=heteroatom, generally N or O

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyethers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE69931165T 1998-08-05 1999-08-03 Herstellung von organolithium- und organophosphor-derivaten Expired - Lifetime DE69931165T2 (de)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
EP98306254 1998-08-05
EP98306254 1998-08-05
EP98203587 1998-10-23
EP98203587 1998-10-23
PCT/EP1999/005748 WO2000008030A2 (en) 1998-08-05 1999-08-03 Preparation of organolithium and organophosphorus derivatives

Publications (2)

Publication Number Publication Date
DE69931165D1 DE69931165D1 (de) 2006-06-08
DE69931165T2 true DE69931165T2 (de) 2007-02-01

Family

ID=26150804

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69931165T Expired - Lifetime DE69931165T2 (de) 1998-08-05 1999-08-03 Herstellung von organolithium- und organophosphor-derivaten

Country Status (9)

Country Link
US (3) US6548708B1 (enExample)
EP (2) EP1671976B1 (enExample)
JP (2) JP5283807B2 (enExample)
CN (1) CN1311791A (enExample)
AT (1) ATE325126T1 (enExample)
AU (1) AU746518B2 (enExample)
CA (1) CA2339165A1 (enExample)
DE (1) DE69931165T2 (enExample)
WO (1) WO2000008030A2 (enExample)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6548708B1 (en) * 1998-08-05 2003-04-15 Sri International Preparation of biphosphine ligands for incorporation into catalytic complexes
DE102005005946A1 (de) * 2005-02-10 2006-08-17 Basf Ag Verfahren zur Herstellung tertiärer Phosphine
EP2213643A1 (en) 2009-01-28 2010-08-04 Hexion Specialty Chemicals Research Belgium S.A. Process for the preparation of an allyl aryl ether by catalytic o-allylation
JP6068482B2 (ja) * 2011-09-30 2017-01-25 ダウ テクノロジー インベストメンツ リミティド ライアビリティー カンパニー 精製プロセス
CN105111235B (zh) * 2015-08-14 2017-04-19 张玉清 一种烷基二苯基膦及制备烷基二苯基膦联产烷基苯的方法
CN108586528B (zh) * 2018-02-08 2020-03-24 新乡市润宇新材料科技有限公司 一种2,2′-双二苯基膦基-1,1′-联萘的合成方法
JP2022078365A (ja) * 2019-03-25 2022-05-25 丸善石油化学株式会社 リン化合物の製造方法
CN110669071B (zh) * 2019-10-10 2022-03-29 黄河三角洲京博化工研究院有限公司 一种聚酮配体1,3-双[双(2-甲氧基苯基)膦基]丙烷的合成方法

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3131204A (en) 1962-02-09 1964-04-28 Grace W R & Co Novel diquaternary aminophosphonium compounds
US3099691A (en) * 1962-07-24 1963-07-30 American Cyanamid Co Preparation of organic phosphines from phosphorus, an alkyl halide and an organic lithium or sodium compound
IL27446A (en) 1966-03-22 1972-04-27 Ceskoslovenska Akademie Ved Method of producing substituted aluminium hydrides
JPS4747014B1 (enExample) 1970-03-17 1972-11-27
US4006187A (en) 1971-10-06 1977-02-01 Lithium Corporation Of America Preparation of aryllithium compounds by metalation
CH651051A5 (en) * 1982-02-05 1985-08-30 Hoffmann La Roche Phosphorus compounds
DE3480845D1 (de) 1983-04-06 1990-02-01 Shell Int Research Verfahren zur herstellung von polyketonen.
US4698447A (en) * 1986-03-14 1987-10-06 American Cyanamid Company Process for producting 10-phenyl-10H-phenoxaphoshine
IE60363B1 (en) 1986-05-27 1994-07-13 Shell Int Research Process for the preparation of polymers
CA1331201C (en) 1987-04-08 1994-08-02 Johannes Adrianus Van Doorn Preparation of substituted diaryl phosphides
EP0290075A3 (en) 1987-05-08 1989-02-22 Shell Internationale Researchmaatschappij B.V. Novel diaryl phosphides
EP0294000A2 (en) 1987-06-05 1988-12-07 Shell Internationale Researchmaatschappij B.V. Novel diaryl phosphides
NL8800349A (nl) 1988-01-12 1989-09-01 Shell Int Research Bereiding van fosfiden.
EP0364046A3 (en) 1988-10-12 1991-03-27 Shell Internationale Researchmaatschappij B.V. Preparation of tetraaryldiphosphines
DE3911230A1 (de) 1989-04-07 1990-10-11 Hoechst Ag Verfahren zur herstellung von alkylphosphonigsaeurediestern und/oder dialkylphosphinigsaeureestern
AU1926292A (en) 1991-04-29 1992-12-21 Fmc Corporation Aryllithium process
US5288912A (en) * 1993-02-12 1994-02-22 Eastman Kodak Company Process for the preparation of lithium diarylphosphides and alkylated derivatives thereof
JPH0747014A (ja) * 1994-07-06 1995-02-21 Suzuno Kasei Kk カートリッジ式棒状化粧品繰出容器
DE19526464C1 (de) 1995-07-20 1997-03-06 Hoechst Ag Chirale tertiäre Phosphine und Verfahren zu ihrer Herstellung
DE69727460T2 (de) * 1996-04-04 2004-07-01 Bp Chemicals Ltd. Eine verbindung, die in einer katalytischen zusammensetzung verwendbar ist
US6548708B1 (en) * 1998-08-05 2003-04-15 Sri International Preparation of biphosphine ligands for incorporation into catalytic complexes
US6437164B1 (en) * 1999-01-06 2002-08-20 Yoshitomi Fine Chemicals, Ltd. Process for the preparation of phosphonite compounds

Also Published As

Publication number Publication date
WO2000008030A2 (en) 2000-02-17
US20040147785A1 (en) 2004-07-29
US6720442B2 (en) 2004-04-13
DE69931165D1 (de) 2006-06-08
EP1671976B1 (en) 2014-12-03
EP1671976A1 (en) 2006-06-21
JP2011201918A (ja) 2011-10-13
CN1311791A (zh) 2001-09-05
EP1102771B1 (en) 2006-05-03
JP5421328B2 (ja) 2014-02-19
AU5374399A (en) 2000-02-28
ATE325126T1 (de) 2006-06-15
JP5283807B2 (ja) 2013-09-04
AU746518B2 (en) 2002-05-02
WO2000008030A3 (en) 2000-05-25
US6548708B1 (en) 2003-04-15
CA2339165A1 (en) 2000-02-17
EP1102771A2 (en) 2001-05-30
JP2002522441A (ja) 2002-07-23
US20030109754A1 (en) 2003-06-12
US7067701B2 (en) 2006-06-27

Similar Documents

Publication Publication Date Title
JP4308427B2 (ja) ジアルキルホスフィン酸の製造方法
DE69907433T2 (de) Verfahren zur herstellung von bisphosphinen
DE69931165T2 (de) Herstellung von organolithium- und organophosphor-derivaten
DE2227939A1 (de) Alkyl- oder Arylphosphon- oder -phosphonothiodihalogenide und -phosphin- oder -phosphinothiomonohalogenide und Verfahren zu ihrer Herstellung
DE69412309T2 (de) Phosphinverbindung und diese als Ligand enthaltender Übergangsmetall-Phosphinkomplex
DE19523335B4 (de) 6-Vinyl-2,8,13-tetradecatrien-1-ol und Verfahren zur Herstellung von ungesättigten Alkoholen
DE68904558T2 (de) Verfahren zu herstellung von bidentatliganden.
US3673285A (en) Preparation of vinyl organo-phosphorous compounds
EP0345653B1 (de) Übergangsmetallkomplexe
DE19964298C2 (de) Verfahren zur Herstellung von substituierten Arylhalophosphinen
US3099691A (en) Preparation of organic phosphines from phosphorus, an alkyl halide and an organic lithium or sodium compound
EP0975643A1 (de) Verfahren zur herstellung von vinylphosphonsäure-verbindungen
DE19851618C2 (de) Verfahren zur Herstellung von Dialkylphosphinsäuren
EP0743316B1 (de) Optisch aktive Phosphine, deren Herstellung, deren Metallkomplexe und Anwendung in der asymmetrischen Synthese
EP2044092B1 (de) Verfahren zur herstellung von halogene enthaltenden organischen phosphorverbindungen
DE102008039167B4 (de) Verfahren zur Herstellung von Arylphosphanderivaten
DE4205115C1 (enExample)
DE4318013A1 (de) Fünfwertige Phosphorverbindungen und Verfahren zu ihrer Herstellung
EP0537197B1 (de) Verfahren zur herstellung von phosphonigsäure-arylester- halogeniden
DE1088955B (de) Verfahren zur Herstellung von monomeren, neutralen, aliphatischen Estern des Phosphors mit der Koordinationszahl 3
GB1597652A (en) Manufacture of a-formylethanephosphonic acid esters and compounds of this type
DD294264A5 (de) Verfahren zur herstellung von natriumorganophosphiden
DE3544064A1 (de) Verfahren zur herstellung von p-hydroxiarylphosphinoxiden bzw. -sulfiden
DE2612644A1 (de) Doppelylid-komplexe von metallen sowie verfahren zu ihrer herstellung

Legal Events

Date Code Title Description
8364 No opposition during term of opposition