DE69830852T2 - Verfahren zum brennen von keramischen wabenkörpern - Google Patents
Verfahren zum brennen von keramischen wabenkörpern Download PDFInfo
- Publication number
- DE69830852T2 DE69830852T2 DE69830852T DE69830852T DE69830852T2 DE 69830852 T2 DE69830852 T2 DE 69830852T2 DE 69830852 T DE69830852 T DE 69830852T DE 69830852 T DE69830852 T DE 69830852T DE 69830852 T2 DE69830852 T2 DE 69830852T2
- Authority
- DE
- Germany
- Prior art keywords
- temperature
- firing
- raw materials
- cordierite
- honeycomb structural
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 238000000034 method Methods 0.000 title claims description 34
- 239000000919 ceramic Substances 0.000 title description 48
- 238000010304 firing Methods 0.000 claims description 83
- 229910052878 cordierite Inorganic materials 0.000 claims description 53
- JSKIRARMQDRGJZ-UHFFFAOYSA-N dimagnesium dioxido-bis[(1-oxido-3-oxo-2,4,6,8,9-pentaoxa-1,3-disila-5,7-dialuminabicyclo[3.3.1]nonan-7-yl)oxy]silane Chemical compound [Mg++].[Mg++].[O-][Si]([O-])(O[Al]1O[Al]2O[Si](=O)O[Si]([O-])(O1)O2)O[Al]1O[Al]2O[Si](=O)O[Si]([O-])(O1)O2 JSKIRARMQDRGJZ-UHFFFAOYSA-N 0.000 claims description 53
- 239000000203 mixture Substances 0.000 claims description 40
- 239000002994 raw material Substances 0.000 claims description 28
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 14
- 230000001590 oxidative effect Effects 0.000 claims description 14
- 229910052760 oxygen Inorganic materials 0.000 claims description 14
- 239000011230 binding agent Substances 0.000 claims description 12
- 238000001125 extrusion Methods 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 9
- 239000000454 talc Substances 0.000 claims description 7
- 229910052623 talc Inorganic materials 0.000 claims description 7
- 235000012211 aluminium silicate Nutrition 0.000 claims description 6
- 239000004927 clay Substances 0.000 claims description 6
- 239000013078 crystal Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000005995 Aluminium silicate Substances 0.000 claims description 5
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 5
- 230000035515 penetration Effects 0.000 claims description 5
- 229910052570 clay Inorganic materials 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 238000009472 formulation Methods 0.000 claims 1
- 241000264877 Hippospongia communis Species 0.000 description 45
- 230000035939 shock Effects 0.000 description 13
- 238000002360 preparation method Methods 0.000 description 7
- 238000002485 combustion reaction Methods 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 239000000758 substrate Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 3
- 238000011835 investigation Methods 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical class [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- SNAAJJQQZSMGQD-UHFFFAOYSA-N aluminum magnesium Chemical compound [Mg].[Al] SNAAJJQQZSMGQD-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical class [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 238000007731 hot pressing Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 235000010981 methylcellulose Nutrition 0.000 description 1
- 229910052863 mullite Inorganic materials 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000007781 pre-processing Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 229910000859 α-Fe Inorganic materials 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
- C04B38/0006—Honeycomb structures
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
- C04B35/18—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay rich in aluminium oxide
- C04B35/195—Alkaline earth aluminosilicates, e.g. cordierite or anorthite
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
- C04B35/632—Organic additives
- C04B35/636—Polysaccharides or derivatives thereof
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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- C04B2235/3218—Aluminium (oxy)hydroxides, e.g. boehmite, gibbsite, alumina sol
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- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
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- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
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- C04B2235/602—Making the green bodies or pre-forms by moulding
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- C04B2235/9615—Linear firing shrinkage
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US6126297P | 1997-10-03 | 1997-10-03 | |
| US61262P | 1997-10-03 | ||
| PCT/US1998/019008 WO1999018047A1 (en) | 1997-10-03 | 1998-09-10 | Method for firing ceramic honeycomb bodies |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69830852D1 DE69830852D1 (de) | 2005-08-18 |
| DE69830852T2 true DE69830852T2 (de) | 2006-05-11 |
Family
ID=22034678
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE69830852T Expired - Fee Related DE69830852T2 (de) | 1997-10-03 | 1998-09-10 | Verfahren zum brennen von keramischen wabenkörpern |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US6027684A (enExample) |
| EP (1) | EP1027304B1 (enExample) |
| JP (1) | JP2001519310A (enExample) |
| CN (1) | CN1098824C (enExample) |
| BR (1) | BR9812402A (enExample) |
| DE (1) | DE69830852T2 (enExample) |
| WO (1) | WO1999018047A1 (enExample) |
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BR9814710A (pt) * | 1997-12-02 | 2000-10-03 | Corning Inc | Método para queima de corpos alveolares cerâmicos |
| US6325963B1 (en) * | 1997-12-22 | 2001-12-04 | Corning Incorporated | Method for firing ceramic honeycomb bodies |
| JP4046925B2 (ja) * | 1999-04-09 | 2008-02-13 | 株式会社日本自動車部品総合研究所 | セラミック体、触媒担持能を有するセラミック担体、セラミック触媒体およびその製造方法 |
| EP1043067A3 (en) | 1999-04-09 | 2002-03-27 | Denso Corporation | A ceramic support capable of supporting a catalyst, a catalyst-ceramic body and processes for producing same |
| WO2001063194A1 (en) | 2000-02-22 | 2001-08-30 | Corning Incorporated | Method for controlling the firing of ceramics |
| JP4030320B2 (ja) | 2001-03-22 | 2008-01-09 | 株式会社デンソー | セラミック体およびセラミック触媒体 |
| JP2003095768A (ja) * | 2001-09-18 | 2003-04-03 | Ngk Insulators Ltd | ハニカム構造体及びその製造方法 |
| JP4222600B2 (ja) * | 2003-01-07 | 2009-02-12 | 日本碍子株式会社 | セラミックハニカム構造体の焼成方法 |
| US7238319B2 (en) * | 2003-06-26 | 2007-07-03 | Corning Incorporated | Method for fabricating ceramic articles containing organic compounds |
| CN100526041C (zh) * | 2003-08-20 | 2009-08-12 | 日本碍子株式会社 | 蜂窝成型体的制造方法、蜂窝过滤器的制造方法及蜂窝过滤器 |
| WO2005068396A1 (ja) * | 2004-01-13 | 2005-07-28 | Ngk Insulators, Ltd. | ハニカム構造体及びその製造方法 |
| US7897099B2 (en) | 2004-01-13 | 2011-03-01 | Ngk Insulators, Ltd. | Method for producing honeycomb structure |
| EP1890983B1 (en) * | 2005-05-31 | 2012-12-12 | Corning Incorporated | Aluminum titanate ceramic forming batch mixtures and green bodies including pore former combinations and methods of manufacturing and firing same |
| US7744980B2 (en) * | 2005-12-20 | 2010-06-29 | Corning Incorporated | Low CTE cordierite honeycomb article and method of manufacturing same |
| CN100445238C (zh) * | 2006-08-11 | 2008-12-24 | 北京创导奥福精细陶瓷有限公司 | 一种制造低膨胀系数蜂窝陶瓷灶具片的工艺 |
| CN100412026C (zh) * | 2007-03-16 | 2008-08-20 | 江苏高淳陶瓷股份有限公司 | 一种堇青石蜂窝陶瓷及制备方法 |
| US8444737B2 (en) * | 2009-02-27 | 2013-05-21 | Corning Incorporated | Ceramic structures and methods of making ceramic structures |
| US20110206828A1 (en) * | 2009-07-10 | 2011-08-25 | Bio2 Technologies, Inc. | Devices and Methods for Tissue Engineering |
| US9775721B2 (en) | 2009-07-10 | 2017-10-03 | Bio2 Technologies, Inc. | Resorbable interbody device |
| EP2451494B1 (en) | 2009-07-10 | 2017-03-01 | Bio2 Technologies, Inc. | Devices and methods for tissue engineering |
| PL2964587T3 (pl) * | 2013-03-08 | 2019-12-31 | Corning Incorporated | Sposób szybkiego wypalania ceramiki |
| US9321189B1 (en) * | 2013-03-15 | 2016-04-26 | Ibiden Co., Ltd. | Method for manufacturing ceramic honeycomb structure |
| JP2018520970A (ja) * | 2015-05-07 | 2018-08-02 | コーニング インコーポレイテッド | セラミックハニカム体を焼成する方法 |
| JP7076378B2 (ja) | 2016-05-31 | 2022-05-27 | コーニング インコーポレイテッド | 多孔質物品およびその製造方法 |
| US11447422B2 (en) | 2017-10-31 | 2022-09-20 | Corning Incorporated | Batch compositions comprising spheroidal pre-reacted inorganic particles and spheroidal pore-formers and methods of manufacture of honeycomb bodies therefrom |
| JP7022593B2 (ja) * | 2018-01-15 | 2022-02-18 | 日本碍子株式会社 | セラミックス焼成体の製造方法、及びセラミックス成形体の焼成方法 |
| CN110606768A (zh) * | 2019-10-15 | 2019-12-24 | 北京交通大学 | 堇青石多孔陶瓷膜支撑体及其近净尺寸制备方法 |
| WO2022046457A1 (en) * | 2020-08-31 | 2022-03-03 | Corning Incorporated | High oxygen fast firing methods for ceramics manufacture |
| JP7589184B2 (ja) * | 2022-02-09 | 2024-11-25 | 日本碍子株式会社 | 焼成後の柱状ハニカム成形体の強度と相関をもつ統計量を探索する方法、及び、所定の設計仕様の焼成後の柱状ハニカム成形体が得られるか否かを予測する方法 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3755204A (en) * | 1970-10-22 | 1973-08-28 | Grace W R & Co | Porous ceramic-exhaust oxidation catalyst |
| US4051231A (en) * | 1974-09-23 | 1977-09-27 | Ford, Bacon & Davis Texas, Inc. | Production of internal atmospheres for kilns |
| US3985846A (en) * | 1975-04-16 | 1976-10-12 | W. R. Grace & Co. | Ceramic firing process |
| US4404166A (en) * | 1981-01-22 | 1983-09-13 | Witec Cayman Patents, Limited | Method for removing binder from a green body |
| US4474731A (en) * | 1983-03-28 | 1984-10-02 | International Business Machines Corporation | Process for the removal of carbon residues during sintering of ceramics |
| GB2198433B (en) * | 1986-12-05 | 1990-11-07 | Romain Louis Billiet | Improvements in or relating to the removal of organic binding agents from articles moulded from sinterable materials |
| JPH079358B2 (ja) * | 1987-02-27 | 1995-02-01 | 日本碍子株式会社 | セラミツクハニカム構造体の焼成法 |
| JPH0745348B2 (ja) * | 1988-02-10 | 1995-05-17 | 日本碍子株式会社 | セラミックハニカム構造体の焼成法 |
| US5078929A (en) * | 1989-12-26 | 1992-01-07 | Matsushita Electric Works, Ltd. | Process of debinding ceramic products |
| JPH03255807A (ja) * | 1990-03-02 | 1991-11-14 | Inax Corp | 焼成物の表面還元処理用バーナ |
| JP2981034B2 (ja) * | 1991-09-30 | 1999-11-22 | 日本碍子株式会社 | セラミックハニカム構造体の焼成方法 |
| US5258150A (en) * | 1991-12-06 | 1993-11-02 | Corning Incorporated | Fabrication of low thermal expansion, high porosity cordierite body |
| US5409870A (en) * | 1992-11-20 | 1995-04-25 | Corning Incorporated | Modified cordierite precursors |
| US5419857A (en) * | 1993-08-17 | 1995-05-30 | Praxair Technology, Inc. | Thermal removal of binders from ceramic-particle bodies |
-
1998
- 1998-09-10 EP EP98946043A patent/EP1027304B1/en not_active Expired - Lifetime
- 1998-09-10 CN CN98809798A patent/CN1098824C/zh not_active Expired - Fee Related
- 1998-09-10 JP JP2000514861A patent/JP2001519310A/ja active Pending
- 1998-09-10 DE DE69830852T patent/DE69830852T2/de not_active Expired - Fee Related
- 1998-09-10 BR BR9812402-1A patent/BR9812402A/pt not_active IP Right Cessation
- 1998-09-10 WO PCT/US1998/019008 patent/WO1999018047A1/en not_active Ceased
- 1998-09-22 US US09/157,916 patent/US6027684A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP1027304A4 (en) | 2002-07-17 |
| EP1027304A1 (en) | 2000-08-16 |
| WO1999018047A1 (en) | 1999-04-15 |
| DE69830852D1 (de) | 2005-08-18 |
| US6027684A (en) | 2000-02-22 |
| CN1272833A (zh) | 2000-11-08 |
| BR9812402A (pt) | 2000-09-19 |
| JP2001519310A (ja) | 2001-10-23 |
| EP1027304B1 (en) | 2005-07-13 |
| CN1098824C (zh) | 2003-01-15 |
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| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |