DE69809899D1 - Wirbelschichtreaktor zur abscheidung eines materiales auf einer oberfläche mittels cvd und verfahren zur herstellung eines beschichteten substrats mit diesem reaktor - Google Patents

Wirbelschichtreaktor zur abscheidung eines materiales auf einer oberfläche mittels cvd und verfahren zur herstellung eines beschichteten substrats mit diesem reaktor

Info

Publication number
DE69809899D1
DE69809899D1 DE69809899T DE69809899T DE69809899D1 DE 69809899 D1 DE69809899 D1 DE 69809899D1 DE 69809899 T DE69809899 T DE 69809899T DE 69809899 T DE69809899 T DE 69809899T DE 69809899 D1 DE69809899 D1 DE 69809899D1
Authority
DE
Germany
Prior art keywords
reactor
substrate
cvd
depositing
producing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69809899T
Other languages
English (en)
Other versions
DE69809899T2 (de
Inventor
Angel Sanjurjo
Kai-Hung Lau
M Lowe
Liqiang Jiang
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SRI International Inc
Original Assignee
SRI International Inc
Stanford Research Institute
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SRI International Inc, Stanford Research Institute filed Critical SRI International Inc
Publication of DE69809899D1 publication Critical patent/DE69809899D1/de
Application granted granted Critical
Publication of DE69809899T2 publication Critical patent/DE69809899T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1836Heating and cooling the reactor
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/4412Details relating to the exhausts, e.g. pumps, filters, scrubbers, particle traps
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/442Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating using fluidised bed process
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/448Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00026Controlling or regulating the heat exchange system
    • B01J2208/00035Controlling or regulating the heat exchange system involving measured parameters
    • B01J2208/00044Temperature measurement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00389Controlling the temperature using electric heating or cooling elements
    • B01J2208/00415Controlling the temperature using electric heating or cooling elements electric resistance heaters

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Combustion & Propulsion (AREA)
  • Chemical Vapour Deposition (AREA)
DE69809899T 1997-04-30 1998-04-28 Wirbelschichtreaktor zur abscheidung eines materiales auf einer oberfläche mittels cvd und verfahren zur herstellung eines beschichteten substrats mit diesem reaktor Expired - Fee Related DE69809899T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/847,145 US5855678A (en) 1997-04-30 1997-04-30 Fluidized bed reactor to deposit a material on a surface by chemical vapor deposition, and methods of forming a coated substrate therewith
PCT/US1998/008566 WO1998049366A1 (en) 1997-04-30 1998-04-28 Fluidized bed reactor to deposit a material on a surface by chemical vapour deposition, and methods of forming a coated substrate therewith

Publications (2)

Publication Number Publication Date
DE69809899D1 true DE69809899D1 (de) 2003-01-16
DE69809899T2 DE69809899T2 (de) 2003-08-28

Family

ID=25299883

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69809899T Expired - Fee Related DE69809899T2 (de) 1997-04-30 1998-04-28 Wirbelschichtreaktor zur abscheidung eines materiales auf einer oberfläche mittels cvd und verfahren zur herstellung eines beschichteten substrats mit diesem reaktor

Country Status (6)

Country Link
US (1) US5855678A (de)
EP (1) EP0979316B1 (de)
JP (1) JP2001512533A (de)
AT (1) ATE229096T1 (de)
DE (1) DE69809899T2 (de)
WO (1) WO1998049366A1 (de)

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FI118158B (sv) * 1999-10-15 2007-07-31 Asm Int Förfarande för modifiering av utgångsämneskemikalierna i en ALD-prosess
US6464912B1 (en) * 1999-01-06 2002-10-15 Cvd, Incorporated Method for producing near-net shape free standing articles by chemical vapor deposition
EP1165852A4 (de) * 1999-02-08 2003-05-02 Quality Heat Technologies Pty Oberflächenbehandlungsverfahren und -vorrichtung
KR100447248B1 (ko) * 2002-01-22 2004-09-07 주성엔지니어링(주) Icp 에쳐용 가스 확산판
JP2004071970A (ja) * 2002-08-08 2004-03-04 Shin Etsu Chem Co Ltd 太陽電池用シリコン基板の製造方法およびその製造システム
DE10260745A1 (de) * 2002-12-23 2004-07-01 Outokumpu Oyj Verfahren und Anlage zur thermischen Behandlung von körnigen Feststoffen
EP1670961B1 (de) * 2003-09-19 2010-07-07 Sri International Verfahren und vorrichtungen zur herstellung von metallischen zusammensetzungen durch reduktion von metallhalogeniden
EP1756836B1 (de) * 2004-03-01 2010-04-21 Pebble Bed Modular Reactor (Proprietary) Limited Verfahren zur herstellung von nuklearem brennmaterial
US7959707B2 (en) * 2006-04-28 2011-06-14 Sri International Methods for producing consolidated materials
EP2257655A2 (de) * 2008-03-05 2010-12-08 SRI International Substrate für siliciumsolarzellen und herstellungsverfahren dafür
US8377408B2 (en) 2010-04-20 2013-02-19 High Temperature Physics, Llc Process for the production of carbon nanoparticles and sequestration of carbon
US8420042B2 (en) 2010-09-21 2013-04-16 High Temperature Physics, Llc Process for the production of carbon graphenes and other nanomaterials
US9260308B2 (en) 2011-04-19 2016-02-16 Graphene Technologies, Inc. Nanomaterials and process for making the same
CN102337517A (zh) * 2011-05-03 2012-02-01 中国科学院福建物质结构研究所 氧化物薄膜生长用金属有机物化学气相沉积反应室
CN102888593B (zh) * 2011-07-20 2014-07-02 航天材料及工艺研究所 一种在石墨球体表面包覆热解碳的设备及气相沉碳方法
US9587993B2 (en) * 2012-11-06 2017-03-07 Rec Silicon Inc Probe assembly for a fluid bed reactor
CN109415814A (zh) 2016-06-20 2019-03-01 奥特莱斯科技有限公司 颗粒基材的涂层
US10814386B2 (en) 2016-06-20 2020-10-27 D-Block Coating Pty Ltd Coating process and coated materials
CN111283215B (zh) * 2020-02-24 2021-06-11 北京科技大学 一种气-固流化制备无氧钝化钛及钛合金粉末制品的方法
FR3126231B1 (fr) * 2021-08-20 2023-11-17 Safran Ceram Dispositif pour le dépôt chimique en phase vapeur

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US4027607A (en) * 1976-04-20 1977-06-07 Continental Can Company, Inc. Pulsed powder application system
JPS5523025A (en) * 1978-08-04 1980-02-19 Hitachi Ltd Production of polycrystal silicon
JPS57145021A (en) * 1981-02-27 1982-09-07 Shin Etsu Chem Co Ltd Preparation of silicon granule
JPS57175797A (en) * 1981-04-22 1982-10-28 Hitachi Ltd Epitaxial growth under reduced pressure
JPS59107917A (ja) * 1982-12-07 1984-06-22 Denki Kagaku Kogyo Kk 多結晶シリコンの製造装置
US4585560A (en) * 1983-12-19 1986-04-29 University Of South Alabama, A Public Body Corporate Inhibition of inorganic and biological CaCO3 deposition by a polysaccharide fraction obtained from CaCO3 -forming organisms
US4574093A (en) * 1983-12-30 1986-03-04 At&T Bell Laboratories Deposition technique
US5244698A (en) * 1985-02-21 1993-09-14 Canon Kabushiki Kaisha Process for forming deposited film
US4623400A (en) * 1985-02-22 1986-11-18 Procedyne Corp. Hard surface coatings for metals in fluidized beds
US4748052A (en) * 1987-08-21 1988-05-31 Ethyl Corporation Fluid bed reactor and process
US5139762A (en) * 1987-12-14 1992-08-18 Advanced Silicon Materials, Inc. Fluidized bed for production of polycrystalline silicon
US5149514A (en) * 1989-04-04 1992-09-22 Sri International Low temperature method of forming materials using one or more metal reactants and a halogen-containing reactant to form one or more reactive intermediates
US5227195A (en) * 1989-04-04 1993-07-13 Sri International Low temperature method of forming materials using one or more metal reactants and a halogen-containing reactant to form one or more reactive intermediates
US5054420A (en) * 1989-09-29 1991-10-08 Alcan International Limited Use of a particulate packed bed at the inlet of a vertical tube MOCVD reactor to achieve desired gas flow characteristics
US5171734A (en) * 1991-04-22 1992-12-15 Sri International Coating a substrate in a fluidized bed maintained at a temperature below the vaporization temperature of the resulting coating composition
JPH11510560A (ja) * 1995-06-07 1999-09-14 アドバンスド シリコン マテリアルズ インコーポレーテツド 流動床反応炉におけるシリコン沈積方法及び装置

Also Published As

Publication number Publication date
ATE229096T1 (de) 2002-12-15
EP0979316B1 (de) 2002-12-04
WO1998049366A1 (en) 1998-11-05
JP2001512533A (ja) 2001-08-21
EP0979316A1 (de) 2000-02-16
DE69809899T2 (de) 2003-08-28
US5855678A (en) 1999-01-05

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