DE69620240T2 - Herstellung von levulinsäure aus kohlenhydrathaltigen materialien - Google Patents

Herstellung von levulinsäure aus kohlenhydrathaltigen materialien

Info

Publication number
DE69620240T2
DE69620240T2 DE69620240T DE69620240T DE69620240T2 DE 69620240 T2 DE69620240 T2 DE 69620240T2 DE 69620240 T DE69620240 T DE 69620240T DE 69620240 T DE69620240 T DE 69620240T DE 69620240 T2 DE69620240 T2 DE 69620240T2
Authority
DE
Germany
Prior art keywords
carbohydrate
production
containing materials
levulinic acid
levulinic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69620240T
Other languages
English (en)
Other versions
DE69620240D1 (de
Inventor
W Fitzpatrick
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Biofine Inc
Original Assignee
Biofine Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Biofine Inc filed Critical Biofine Inc
Application granted granted Critical
Publication of DE69620240D1 publication Critical patent/DE69620240D1/de
Publication of DE69620240T2 publication Critical patent/DE69620240T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C07D307/50—Preparation from natural products
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE69620240T 1995-06-07 1996-05-17 Herstellung von levulinsäure aus kohlenhydrathaltigen materialien Expired - Lifetime DE69620240T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/475,630 US5608105A (en) 1995-06-07 1995-06-07 Production of levulinic acid from carbohydrate-containing materials
PCT/US1996/007231 WO1996040609A1 (en) 1995-06-07 1996-05-17 Production of levulinic acid from carbohydrate-containing materials

Publications (2)

Publication Number Publication Date
DE69620240D1 DE69620240D1 (de) 2002-05-02
DE69620240T2 true DE69620240T2 (de) 2002-11-14

Family

ID=23888434

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69620240T Expired - Lifetime DE69620240T2 (de) 1995-06-07 1996-05-17 Herstellung von levulinsäure aus kohlenhydrathaltigen materialien

Country Status (8)

Country Link
US (1) US5608105A (de)
EP (1) EP0873294B1 (de)
AU (1) AU5798596A (de)
CA (1) CA2223600C (de)
DE (1) DE69620240T2 (de)
IN (1) IN185298B (de)
NO (1) NO308464B1 (de)
WO (1) WO1996040609A1 (de)

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US7378549B2 (en) 2004-01-26 2008-05-27 Shell Oil Company Process for the reactive extractive extraction of levulinic acid
US7317116B2 (en) * 2004-12-10 2008-01-08 Archer-Daniels-Midland-Company Processes for the preparation and purification of hydroxymethylfuraldehyde and derivatives
US7393963B2 (en) * 2004-12-10 2008-07-01 Archer-Daniels-Midland Company Conversion of 2,5-(hydroxymethyl)furaldehyde to industrial derivatives, purification of the derivatives, and industrial uses therefor
ATE527230T1 (de) * 2004-12-23 2011-10-15 Shell Int Research Verfahren zur hydrierung eines lactons oder einer carbonsäure oder eines esters mit einer gamma- carbonylgruppe
US7501062B2 (en) 2005-02-22 2009-03-10 Shell Oil Company Process for permeation enhanced reactive extraction of levulinic acid
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US20070100192A1 (en) * 2005-10-27 2007-05-03 Harmer Mark A Olefin isomerization
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US7815741B2 (en) * 2006-11-03 2010-10-19 Olson David A Reactor pump for catalyzed hydrolytic splitting of cellulose
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US8350056B2 (en) * 2008-12-04 2013-01-08 E I Du Pont De Nemours And Company Functionalized N-substituted pyrrolidonium ionic liquids
US8119818B2 (en) * 2008-12-04 2012-02-21 E. I. Du Pont De Nemours And Company Functionalized N-substituted pyrrolidonium ionic liquids
US8138354B2 (en) 2008-12-04 2012-03-20 E. I. Du Pont De Nemours And Company N-substituted pyrrolidonium ionic liquids
WO2010065841A1 (en) 2008-12-04 2010-06-10 E. I. Du Pont De Nemours And Company N-substituted pyrrolidonium ionic liquids with expanded linker
EP2364198A2 (de) 2008-12-04 2011-09-14 E. I. du Pont de Nemours and Company Entfernung von kohlendioxid und dabei verwendbare ionische flüssigkeiten
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US8580978B2 (en) * 2009-08-07 2013-11-12 Shell Oil Company Process for preparing a hydroxyacid or hydroxyester
US20110112326A1 (en) * 2009-08-07 2011-05-12 Jean-Paul Lange Process for hydrogenation
US8362306B2 (en) * 2009-10-26 2013-01-29 University Of Maine System Board Of Trustees Energy densification of biomass-derived organic acids
US20110173877A1 (en) * 2009-12-24 2011-07-21 Jeroen Van Buijtenen Process for preparing a hydrocarbon or mixture of hydrocarbons
US7960592B1 (en) 2010-01-12 2011-06-14 Wisconsin Alumni Research Foundation Production of methyl-vinyl ketone from levulinic acid
BR112012028720A2 (pt) 2010-05-10 2016-07-19 Segetis Inc alquil cetal ésteres com dispersantes e agentes deslizantes para partículas sólidas, métodos de fabricação e suas utilizações
CA2798436A1 (en) 2010-05-12 2011-11-17 Klaas Lambertus Von Hebel Process for liquefying a cellulosic material
CA2798440A1 (en) 2010-05-12 2011-11-17 Klaas Lambertus Von Hebel Process for liquefying a cellulosic material
CN102030646B (zh) * 2010-11-18 2013-09-04 郑州大学 一种纤维素类物质水解直接转化生成乙酰丙酸乙酯的工艺
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AR088124A1 (es) 2011-04-01 2014-05-14 Dsm Ip Assets Bv Proceso para la preparacion de esteres de acido alcanoico en un proceso de carbonilacion utilizando ligandos de bifosfato bidentados de paladio
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US8389761B2 (en) 2011-05-25 2013-03-05 Wisconsin Alumni Research Foundation Method to produce and recover levulinic acid and/or gamma-valerolactone from aqueous solutions using alkylphenols
US8962867B2 (en) 2011-05-25 2015-02-24 Wisconsin Alumni Research Foundation Solute-enhanced production of gamma-valerolactone (GVL) from aqueous solutions of levulinic acid
US8389749B2 (en) 2011-05-25 2013-03-05 Wisconsin Alumni Research Foundation Method to produce, recover and convert furan derivatives from aqueous solutions using alkylphenol extraction
MY163070A (en) 2011-06-21 2017-08-15 Dsm Ip Assets Bv Process to produce valerolactone from levulinic acid
EP2537841B1 (de) 2011-06-22 2013-09-25 DSM IP Assets B.V. Kontinuierliche Herstellung von Furfural- und Levulinsäure
EP2573064B1 (de) 2011-09-23 2013-11-13 DSM IP Assets B.V. Verfahren zur Herstellung von Alkensaüreestern von Lactonen
US20130079566A1 (en) * 2011-09-27 2013-03-28 Nevada, Catalytic process for conversion of biomass into hydrocarbon fuels
CN104066705B (zh) * 2011-11-23 2016-12-07 Gf生化有限公司 制备乙酰丙酸的方法
CN102558106B (zh) * 2011-12-15 2014-12-17 北京金骄生物质化工有限公司 一种利用废弃生物质制备2-甲基四氢呋喃的方法
EP2675782B1 (de) 2011-12-20 2015-06-17 DSM IP Assets B.V. Verfahren zur herstellung von alkensäureestern aus lactonen
WO2013102002A1 (en) 2011-12-28 2013-07-04 E. I. Du Pont De Nemours And Company Processes for making furfurals
WO2013102007A1 (en) * 2011-12-28 2013-07-04 E. I. Du Pont De Nemours And Company Process for the production of furfural
BR112014015988A8 (pt) 2011-12-28 2017-07-04 Du Pont processo
US9181211B2 (en) 2011-12-28 2015-11-10 E I Du Pont De Nemours And Company Process for the production of furfural
WO2013106137A1 (en) * 2012-01-10 2013-07-18 Archer Daniels Midland Company Process for making levulinic acid
WO2013107904A1 (en) 2012-01-19 2013-07-25 Dsm Ip Assets B.V. Process to produce alkanoic acid esters in a carbonylation process using lewis acids as acid promotor
US9174909B2 (en) * 2012-02-02 2015-11-03 Wisconsin Alumni Research Foundation Two-stage, acid-catalyzed conversion of carbohydrates into levulinic acid
EP2814912A2 (de) 2012-02-16 2014-12-24 Karl A. Seck Bioraffinerie zur umwandlung von kohlenhydraten und lignocellulose über primäres hydrolysat-cmf in flüssigbrennstoffe
MX368591B (es) 2012-03-12 2019-10-08 Georgia Pacific Llc Metodo para producir acido levulinico a partir de una biomasa lignocelulosica.
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EP2872495B1 (de) * 2012-07-13 2016-08-24 DSM IP Assets B.V. Verfahren zur herstellung von furfural und levulinsäure aus einer lignocellulosebiomasse
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US20160122278A1 (en) * 2013-05-22 2016-05-05 Segetis, Inc. Process to prepare levulinic acid
US9346731B2 (en) 2013-09-18 2016-05-24 Georgia-Pacific LLC Method for producing levulinic acid from sludge and lignocellulosic biomass
US9403734B2 (en) 2013-09-18 2016-08-02 Georgia-Pacific LLC Method for producing organic acids and organic acid degradation compounds from biomass
WO2015063033A1 (en) 2013-11-01 2015-05-07 Dsm Ip Assets B.V. Process for the separation of levulinic acid
LT3132005T (lt) 2014-03-26 2021-12-27 Neste Oyj Ketorūgščių terminės konversijos ir hidrinimo iki angliavandenilių būdas
ES2762517T3 (es) 2014-03-26 2020-05-25 Neste Oyj Método para la conversión catalítica de cetoácidos e hidrotratamiento en hidrocarburos
CN104292194B (zh) * 2014-09-05 2016-10-12 中国科学院广州能源研究所 一种生物质分级处理后制备糠醛和快速变温法制备乙酰丙酸的方法
CN104292195B (zh) * 2014-09-05 2016-10-12 中国科学院广州能源研究所 一种生物质分级处理后制备糠醛和调变流量制备乙酰丙酸的方法
CN104292193B (zh) * 2014-09-05 2017-01-11 中国科学院广州能源研究所 一种生物质分级处理后制备糠醛和两步制备乙酰丙酸的方法
CN104311411B (zh) * 2014-09-15 2015-12-02 淮阴师范学院 多级酸水解制备乙酰丙酸的方法
ES2767081T3 (es) 2015-01-30 2020-06-16 Neste Oyj Método para la conversión catalítica de cetoácidos mediante un intermedio de cetoácido dimérico e hidrotratamiento de hidrocarburos
EP3050868B1 (de) 2015-01-30 2019-11-13 Neste Oyj Verfahren zur katalytischen Umwandlung von Ketosäuren und Wasserstoffbehandlung in Kohlenwasserstoffe
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JP2018508485A (ja) 2015-02-18 2018-03-29 ディーエスエム アイピー アセッツ ビー．ブイ． レブリン酸の連続水素化
CN104945446B (zh) * 2015-05-20 2017-11-14 中国科学院广州能源研究所 一种利用秸秆类生物质制备甲酸酯、乙酸酯、乙酰丙酸酯的方法
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FI127020B (en) 2015-12-23 2017-09-29 Neste Oyj Selective process for the conversion of levulinic acid to gamma valerolactone
FI127191B (en) 2015-12-23 2018-01-15 Neste Oyj Co-production of levulinic acid and furfural from biomass
ES2866043T3 (es) 2015-12-29 2021-10-19 Neste Oyj Método para producir una composición de destilado medio renovable, uso de la composición y combustible que la contiene
EP3187570B1 (de) 2015-12-29 2019-11-20 Neste Oyj Verfahren zur herstellung einer brennstoffmischung
EP3187482A1 (de) 2015-12-29 2017-07-05 Neste Oyj Erneuerbare kohlenwasserstoffe, verfahren zur herstellung davon und verwendung davon
CN105642204B (zh) * 2016-02-26 2016-10-26 河南省科学院能源研究所有限公司 一种生物质水解装置
CN106748711B (zh) * 2016-12-08 2019-07-09 农业部环境保护科研监测所 一种乙酰丙酸的制备方法
CN114315554B (zh) * 2021-12-23 2024-05-28 山东理工大学 水合物熔盐中甲酸和乙酰丙酸的分离方法
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Also Published As

Publication number Publication date
US5608105A (en) 1997-03-04
EP0873294B1 (de) 2002-03-27
IN185298B (de) 2000-12-23
CA2223600A1 (en) 1996-12-19
NO975727D0 (no) 1997-12-05
WO1996040609A1 (en) 1996-12-19
EP0873294A4 (de) 1999-05-26
EP0873294A1 (de) 1998-10-28
NO308464B1 (no) 2000-09-18
CA2223600C (en) 2004-02-10
DE69620240D1 (de) 2002-05-02
AU5798596A (en) 1996-12-30
NO975727L (no) 1998-02-04

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