DE69618310T2 - Verfahren zur Selektion von Adsorptionsmitteln - Google Patents

Verfahren zur Selektion von Adsorptionsmitteln

Info

Publication number
DE69618310T2
DE69618310T2 DE69618310T DE69618310T DE69618310T2 DE 69618310 T2 DE69618310 T2 DE 69618310T2 DE 69618310 T DE69618310 T DE 69618310T DE 69618310 T DE69618310 T DE 69618310T DE 69618310 T2 DE69618310 T2 DE 69618310T2
Authority
DE
Germany
Prior art keywords
adsorbents
selection
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69618310T
Other languages
English (en)
Other versions
DE69618310D1 (de
Inventor
Frank Notaro
Joseph Timothy Mullhaupt
Frederick Wells Leavitt
Mark William Ackley
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Praxair Technology Inc
Original Assignee
Praxair Technology Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Praxair Technology Inc filed Critical Praxair Technology Inc
Publication of DE69618310D1 publication Critical patent/DE69618310D1/de
Application granted granted Critical
Publication of DE69618310T2 publication Critical patent/DE69618310T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047Pressure swing adsorption
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16Alumino-silicates
    • B01J20/165Natural alumino-silicates, e.g. zeolites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16Alumino-silicates
    • B01J20/18Synthetic zeolitic molecular sieves
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y15/00Nanotechnology for interacting, sensing or actuating, e.g. quantum dots as markers in protein assays or molecular motors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/106Silica or silicates
    • B01D2253/108Zeolites
    • B01D2253/1085Zeolites characterized by a silicon-aluminium ratio
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/10Single element gases other than halogens
    • B01D2257/102Nitrogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/40011Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058Number of sequence steps, including sub-steps, per cycle
    • B01D2259/4006Less than four
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/41Further details for adsorption processes and devices using plural beds of the same adsorbent in series
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/414Further details for adsorption processes and devices using different types of adsorbents
    • B01D2259/4141Further details for adsorption processes and devices using different types of adsorbents within a single bed
    • B01D2259/4145Further details for adsorption processes and devices using different types of adsorbents within a single bed arranged in series
    • B01D2259/4146Contiguous multilayered adsorbents

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Nanotechnology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
DE69618310T 1995-10-20 1996-10-18 Verfahren zur Selektion von Adsorptionsmitteln Expired - Fee Related DE69618310T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US08/546,325 US5674311A (en) 1995-10-20 1995-10-20 Adsorption process and system using multilayer adsorbent beds

Publications (2)

Publication Number Publication Date
DE69618310D1 DE69618310D1 (de) 2002-02-07
DE69618310T2 true DE69618310T2 (de) 2002-08-22

Family

ID=24179894

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69618310T Expired - Fee Related DE69618310T2 (de) 1995-10-20 1996-10-18 Verfahren zur Selektion von Adsorptionsmitteln

Country Status (11)

Country Link
US (2) US5674311A (de)
EP (1) EP0769320B1 (de)
JP (1) JP3238336B2 (de)
KR (1) KR100286386B1 (de)
CN (1) CN1090517C (de)
AR (1) AR004037A1 (de)
BR (1) BR9605166A (de)
CA (1) CA2188192C (de)
DE (1) DE69618310T2 (de)
ES (1) ES2166421T3 (de)
ID (1) ID16482A (de)

Families Citing this family (54)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB9422833D0 (en) * 1994-11-11 1995-01-04 Secr Defence Pressure and temperature swing absorbtion
US5989314A (en) * 1995-09-26 1999-11-23 Praxair Technology, Inc. Pressure swing adsorption air prepurifier
SE517561C2 (sv) * 1996-03-04 2002-06-18 Aga Ab Förfarande och anordning för framställning av en gas genom separation från en gasblandning
FR2749004B1 (fr) * 1996-05-24 1998-07-10 Air Liquide Procede pour la purification de melanges gazeux a base d'hydrogene utilisant une zeolithe x echangee au lithium
US5868818A (en) * 1996-08-08 1999-02-09 Tosoh Corporation Adsorbent for air separation, production method thereof, and air-separation method using it
FR2753108B1 (fr) * 1996-09-06 1998-10-16 Air Liquide Procede pour la separation de melanges gazeux contenant de l'oxygene et de l'azote
US6027548A (en) * 1996-12-12 2000-02-22 Praxair Technology, Inc. PSA apparatus and process using adsorbent mixtures
FR2758739B1 (fr) * 1997-01-24 1999-02-26 Ceca Sa Perfectionnement dans les procedes psa de purification de l'hydrogene
US6152991A (en) * 1997-04-17 2000-11-28 Praxair Technology, Inc. Multilayer adsorbent beds for PSA gas separation
FR2765491B1 (fr) * 1997-07-07 1999-08-06 Air Liquide Procede de separation d'un flux gazeux par un procede psa
FR2766476B1 (fr) * 1997-07-22 1999-09-03 Ceca Sa Adsorbant zeolitique ameliore pour la separation des gaz de l'air et son procede d'obtention
US6238460B1 (en) 1997-09-26 2001-05-29 The Boc Group, Inc. Air purification process
US5914455A (en) * 1997-09-30 1999-06-22 The Boc Group, Inc. Air purification process
US5906675A (en) * 1997-09-30 1999-05-25 The Boc Group, Inc. Air purification process
AU2796499A (en) 1998-02-27 1999-09-15 Praxair Technology, Inc. Vpsa process using improved adsorbent materials
US6017382A (en) * 1998-03-30 2000-01-25 The Boc Group, Inc. Method of processing semiconductor manufacturing exhaust gases
US6183539B1 (en) * 1998-07-01 2001-02-06 Zeochem Co. Molecular sieve adsorbent for gas purification and preparation thereof
US6106593A (en) * 1998-10-08 2000-08-22 Air Products And Chemicals, Inc. Purification of air
FR2784599B1 (fr) * 1998-10-20 2000-12-08 Air Liquide Procede de purification d'un flux gazeux en ses impuretes n2o
US6475265B1 (en) * 1998-10-22 2002-11-05 Praxair Technology, Inc. Pressure swing adsorption method for production of an oxygen-enriched gas
FR2792220B1 (fr) * 1999-04-19 2001-06-15 Air Liquide Procede psa mettant en oeuvre un adsorbant a resistance intrinseque favorable a la cinetique d'adsorption
US6231644B1 (en) * 1999-07-23 2001-05-15 The Boc Group, Inc. Air separation using monolith adsorbent bed
US6521019B2 (en) 1999-07-23 2003-02-18 The Boc Group, Inc. Air separation using monolith adsorbent bed
US6340382B1 (en) * 1999-08-13 2002-01-22 Mohamed Safdar Allie Baksh Pressure swing adsorption process for the production of hydrogen
FR2811241B1 (fr) * 2000-07-07 2002-12-13 Ceca Sa Procede pour la purification de melanges gazeux a base d'hydrogene utilisant une zeolite x au calcium
KR100377838B1 (ko) * 2000-09-01 2003-03-29 이창하 압력순환식 흡착장치
US6824590B2 (en) * 2000-11-07 2004-11-30 Air Products And Chemicals, Inc. Use of lithium-containing fau in air separation processes including water and/or carbon dioxide removal
US6483001B2 (en) * 2000-12-22 2002-11-19 Air Products And Chemicals, Inc. Layered adsorption zone for hydrogen production swing adsorption
US6544318B2 (en) * 2001-02-13 2003-04-08 Air Products And Chemicals, Inc. High purity oxygen production by pressure swing adsorption
AU2002332426A1 (en) * 2001-07-25 2003-02-17 Richard A. Haase Processes and apparatus for the manufacture of polynuclear aluminum compounds and disinfectants, and polynuclear aluminum compounds and disinfectants from such processes and apparatus
MXPA04000965A (es) 2001-07-31 2005-02-22 Praxair Technology Inc Recuperacion de helio.
US6719827B2 (en) * 2002-03-01 2004-04-13 Air Products And Chemicals, Inc. Process for nitrous oxide removal
US6893483B2 (en) * 2002-03-08 2005-05-17 Air Products And Chemicals, Inc. Multilayered adsorbent system for gas separations by pressure swing adsorption
PL372916A1 (en) 2002-04-11 2005-08-08 Richard A. Haase Water combustion technology-methods, processes, systems and apparatus for the combustion of hydrogen and oxygen
US6723155B2 (en) * 2002-04-29 2004-04-20 Air Products And Chemicals, Inc. Purification of gas streams
KR100468915B1 (ko) * 2002-05-03 2005-02-02 삼성전자주식회사 산소발생기의 질소흡착장치
WO2004058630A2 (en) * 2002-12-24 2004-07-15 Praxair Technology, Inc. Process and apparatus for hydrogen purification
DE10313575B4 (de) * 2003-03-21 2014-01-23 Wabco Gmbh Kartuscheeinrichtung für einen Lufttrockner
US6878186B2 (en) 2003-09-09 2005-04-12 David Lloyd Neary Pure vacuum swing adsorption system and apparatus
KR100792284B1 (ko) 2004-03-10 2008-01-07 삼성전자주식회사 이미지장치의 드라이버 프로그램에 대한 유저 인터페이스설정방법 및 트랜스패런트 기능을 적용한 이미지 처리시스템
US7179324B2 (en) * 2004-05-19 2007-02-20 Praxair Technology, Inc. Continuous feed three-bed pressure swing adsorption system
US7264651B2 (en) * 2004-07-02 2007-09-04 Praxair Technology, Inc. Adsorption process and system using multilayer adsorbent beds containing regenerator section
US7828877B2 (en) 2004-11-05 2010-11-09 Xebec Adsorption, Inc. Separation of carbon dioxide from other gases
US7311763B2 (en) * 2005-04-22 2007-12-25 David Lloyd Neary Gas separation vessel apparatus
US8268269B2 (en) 2006-01-24 2012-09-18 Clearvalue Technologies, Inc. Manufacture of water chemistries
JP5314408B2 (ja) * 2008-03-06 2013-10-16 株式会社神戸製鋼所 高純度水素ガス製造用psa装置
US7780764B2 (en) 2008-06-27 2010-08-24 Praxair Technology, Inc. Methods and systems for helium recovery
US8016914B2 (en) * 2009-03-25 2011-09-13 Praxair Technology, Inc. Adsorption control method and controller
WO2010129329A2 (en) * 2009-04-28 2010-11-11 Lehigh University Miniature oxygen concentrators and methods
JP5684898B2 (ja) * 2011-03-31 2015-03-18 大陽日酸株式会社 ガス精製方法
WO2014130833A1 (en) * 2013-02-21 2014-08-28 Lehigh University Oxygen concentrator system and method
US10322398B1 (en) 2015-09-16 2019-06-18 Arrowhead Center, Inc. Synthesis of Zn(NH3) (CO3) inorganic helical framework and its use for selective separation of carbon dioxide
KR101773437B1 (ko) * 2017-02-13 2017-08-31 (주)원하이테크 흡착제가 복합 충진된 산소발생기용 흡착탑
CN108452635B (zh) * 2018-02-09 2020-12-04 北京东方计量测试研究所 优化VOCs吸附材料组合配方的方法

Family Cites Families (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE154690C (de) *
US3140933A (en) * 1960-12-02 1964-07-14 Union Carbide Corp Separation of an oxygen-nitrogen mixture
US3140932A (en) * 1960-12-02 1964-07-14 Union Carbide Corp Separation of an oxygen-nitrogen mixture
FR1596425A (de) * 1968-12-27 1970-06-15
FR2135388B1 (de) * 1971-05-03 1973-05-11 Air Liquide
BE792039A (fr) * 1971-11-30 1973-05-29 Air Liquide Procede et installation de fractionnement d'un melange gazeux par adsorption
US3973931A (en) * 1974-10-30 1976-08-10 Union Carbide Corporation Air separation by adsorption
JPS5561915A (en) * 1978-11-06 1980-05-10 Hitachi Ltd Pressure swing type adsorption tower
DD154690A1 (de) 1980-08-15 1982-04-14 Friedrich Wolf Verfahren zur abtrennung von sauerstoff aus gasen
US4481018A (en) * 1982-11-15 1984-11-06 Air Products And Chemicals, Inc. Polyvalent ion exchanged adsorbent for air separation
JPS6125640A (ja) * 1984-07-13 1986-02-04 Kurita Water Ind Ltd 吸着剤の再生方法
US4557736A (en) * 1984-10-29 1985-12-10 Air Products And Chemicals, Inc. Binary ion exchanged type X zeolite adsorbent
US4859217A (en) * 1987-06-30 1989-08-22 Uop Process for separating nitrogen from mixtures thereof with less polar substances
US4950311A (en) * 1988-03-07 1990-08-21 White Jr Donald H Heaterless adsorption system for combined purification and fractionation of air
JPH0340902A (ja) * 1989-07-10 1991-02-21 Japan Pionics Co Ltd 水素化物ガスの精製方法
US5174979A (en) * 1989-10-06 1992-12-29 Uop Mixed ion-exchanged zeolites and processes for the use thereof in gas separations
US5074892A (en) * 1990-05-30 1991-12-24 Union Carbide Industrial Gases Technology Corporation Air separation pressure swing adsorption process
GB9104875D0 (en) * 1991-03-07 1991-04-17 Boc Group Plc Gas separation method and apparatus
JP3017552B2 (ja) * 1991-03-22 2000-03-13 昭和エンジニアリング株式会社 圧力変動吸着法による富酸素ガスの製造方法
GB9110038D0 (en) * 1991-05-09 1991-07-03 Boc Group Plc Improvements in pressure swing adsorption plants
US5169413A (en) * 1991-10-07 1992-12-08 Praxair Technology Inc. Low temperature pressure swing adsorption with refrigeration
US5203887A (en) * 1991-12-11 1993-04-20 Praxair Technology, Inc. Adsorbent beds for pressure swing adsorption operations
US5266102A (en) * 1992-09-23 1993-11-30 Air Products And Chemicals, Inc. O2 VSA process with low O2 capacity adsorbents
US5268023A (en) * 1992-10-05 1993-12-07 Air Products And Chemicals, Inc. Nitrogen adsorption with highly Li exchanged X-zeolites with low Si/Al ratio
US5529610A (en) * 1993-09-07 1996-06-25 Air Products And Chemicals, Inc. Multiple zeolite adsorbent layers in oxygen separation
US5454857A (en) * 1994-03-18 1995-10-03 Uop Air separation process
DE19528188C1 (de) * 1995-08-01 1996-12-05 Bayer Ag Verfahren zur Adsorption von Stickstoff aus Gasgemischen mittels Druckwechseladsorption mit Zeolithen
JP3040902U (ja) 1997-02-24 1997-09-05 蒲野建設株式会社 木炭板

Also Published As

Publication number Publication date
AR004037A1 (es) 1998-09-30
KR970020161A (ko) 1997-05-28
EP0769320A2 (de) 1997-04-23
EP0769320A3 (de) 1997-09-24
US5674311A (en) 1997-10-07
CA2188192A1 (en) 1997-04-21
DE69618310D1 (de) 2002-02-07
JP3238336B2 (ja) 2001-12-10
US5810909A (en) 1998-09-22
JPH09141037A (ja) 1997-06-03
CN1090517C (zh) 2002-09-11
KR100286386B1 (ko) 2001-04-16
BR9605166A (pt) 1998-07-14
ES2166421T3 (es) 2002-04-16
CA2188192C (en) 2000-09-05
EP0769320B1 (de) 2002-01-02
ID16482A (id) 1997-10-02
CN1156061A (zh) 1997-08-06

Similar Documents

Publication Publication Date Title
DE69618310D1 (de) Verfahren zur Selektion von Adsorptionsmitteln
DE69628712D1 (de) Verfahren zur Herstellung von Dihalogenazolopyrimidinen
DE59607656D1 (de) Verfahren zur Herstellung von Alkylhydrogenchlorsilanen
DE69633579D1 (de) Verfahren zur Rückgewinnung von Quecksilber
DE69433634D1 (de) Verfahren zur Umsetzung von Kohlenwasserstoffen
DE69410382T2 (de) Verfahren zur Isomerisierung von 2-Methyl-3-butennitril
DE59601030D1 (de) Verfahren zur Herstellung von Diarylethanen
DE69426868T2 (de) Verfahren zur Hydrierung von Chlorsilan
DE69600385D1 (de) Verfahren zur Herstellung von Aminonitropyridinen
DE69612815D1 (de) Verfahren zur Heissfraktionierung von Organosilanen
DE69611331D1 (de) Verfahren zur Herstellung von S-Phenyl-L-Cystein
DE59508333D1 (de) Verfahren zur Isolierung von Tetraphenylboraten
DE69620337T2 (de) Verfahren zur Reinigung von Halosilanen
DE69607541D1 (de) Verfahren zur Herstellung von p-Bromfluorobenzol
DE69513008T2 (de) Verfahren zur Herstellung von Hydroxyalkoxybenzophenonen
DE59605105D1 (de) Verfahren zur Herstellung von substituierten Aminocarbonyltriazolinonen
DE69603243D1 (de) Verfahren zur Herstellung von Ethenylamiden
DE69501535D1 (de) Verfahren zur Reinigung von Difluormethan
DE4496393T1 (de) Verfahren zur Trennung von Enantiomeren
DE59605227D1 (de) Verfahren zur Herstellung von ortho-Nitro-benzonitrilen
DE59507012D1 (de) Verfahren zur Herstellung von Adsorptionsmittelgranulaten
DE59600938D1 (de) Verfahren zur Regenerierung von Kunststoffdiaphragmen
DE59604010D1 (de) Verfahren zur Herstellung von 3-hydroxyoxetanen
DE59601809D1 (de) Verfahren zur Herstellung von substituierten Aminotriazolinonen
DE59604159D1 (de) Verfahren zur Herstellung von substituierten Chloraromaten

Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee