DE69522443D1 - THIONATION-PROZESS UNTER VERWENDUNG VON ELEMENTAREN PHOSPHOR UND Schwefel - Google Patents
THIONATION-PROZESS UNTER VERWENDUNG VON ELEMENTAREN PHOSPHOR UND SchwefelInfo
- Publication number
- DE69522443D1 DE69522443D1 DE69522443T DE69522443T DE69522443D1 DE 69522443 D1 DE69522443 D1 DE 69522443D1 DE 69522443 T DE69522443 T DE 69522443T DE 69522443 T DE69522443 T DE 69522443T DE 69522443 D1 DE69522443 D1 DE 69522443D1
- Authority
- DE
- Germany
- Prior art keywords
- phosphorus
- reaction
- sulfur
- elemental
- mix
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 title abstract 5
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title abstract 5
- 229910052698 phosphorus Inorganic materials 0.000 title abstract 5
- 239000011574 phosphorus Substances 0.000 title abstract 5
- 229910052717 sulfur Inorganic materials 0.000 title abstract 3
- 239000011593 sulfur Substances 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 238000007280 thionation reaction Methods 0.000 title 1
- UHZZMRAGKVHANO-UHFFFAOYSA-M chlormequat chloride Chemical compound [Cl-].C[N+](C)(C)CCCl UHZZMRAGKVHANO-UHFFFAOYSA-M 0.000 abstract 3
- CYQAYERJWZKYML-UHFFFAOYSA-N phosphorus pentasulfide Chemical compound S1P(S2)(=S)SP3(=S)SP1(=S)SP2(=S)S3 CYQAYERJWZKYML-UHFFFAOYSA-N 0.000 abstract 2
- 239000003085 diluting agent Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 150000002894 organic compounds Chemical class 0.000 abstract 1
- 150000002903 organophosphorus compounds Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D237/00—Heterocyclic compounds containing 1,2-diazine or hydrogenated 1,2-diazine rings
- C07D237/02—Heterocyclic compounds containing 1,2-diazine or hydrogenated 1,2-diazine rings not condensed with other rings
- C07D237/06—Heterocyclic compounds containing 1,2-diazine or hydrogenated 1,2-diazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D237/10—Heterocyclic compounds containing 1,2-diazine or hydrogenated 1,2-diazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D237/18—Sulfur atoms
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/14—Sulfur, selenium, or tellurium compounds of phosphorus
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C327/00—Thiocarboxylic acids
- C07C327/02—Monothiocarboxylic acids
- C07C327/04—Monothiocarboxylic acids having carbon atoms of thiocarboxyl groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C327/06—Monothiocarboxylic acids having carbon atoms of thiocarboxyl groups bound to hydrogen atoms or to acyclic carbon atoms to hydrogen atoms or to carbon atoms of an acyclic saturated carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
- C07F9/165—Esters of thiophosphoric acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
- C07F9/165—Esters of thiophosphoric acids
- C07F9/18—Esters of thiophosphoric acids with hydroxyaryl compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Inorganic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/219,227 US5464601A (en) | 1994-03-29 | 1994-03-29 | Process for preparing sulfides of phosphorus |
| PCT/US1995/003790 WO1995026357A1 (en) | 1994-03-29 | 1995-03-27 | Thionation process using elemental phosphorus and sulfur |
| US08/409,011 US5663402A (en) | 1994-03-29 | 1995-03-27 | Process for the preparation of phosphorodithioic compounds via thionation reaction |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69522443D1 true DE69522443D1 (de) | 2001-10-04 |
| DE69522443T2 DE69522443T2 (de) | 2002-06-13 |
Family
ID=26913695
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE69522443T Expired - Fee Related DE69522443T2 (de) | 1994-03-29 | 1995-03-27 | THIONATION-PROZESS UNTER VERWENDUNG VON ELEMENTAREN PHOSPHOR UND Schwefel |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US5663402A (de) |
| EP (1) | EP0752998B1 (de) |
| JP (1) | JPH09510977A (de) |
| CN (1) | CN1141879A (de) |
| AT (1) | ATE204876T1 (de) |
| CA (1) | CA2186765A1 (de) |
| DE (1) | DE69522443T2 (de) |
| WO (1) | WO1995026357A1 (de) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7488766B2 (en) * | 2005-10-06 | 2009-02-10 | Sabic Innovative Plastics Ip B.V. | Polymer composition, method, and article |
| CN101402451B (zh) * | 2008-10-27 | 2011-05-04 | 昆明理工大学 | 一种粉状五硫化二磷的制备方法 |
| CN104014292A (zh) * | 2013-03-01 | 2014-09-03 | 辽宁瑞兴化工集团有限公司 | 一种用于生产五硫化二磷的反应釜 |
| US9884764B2 (en) * | 2014-06-02 | 2018-02-06 | Tubitak | Purification of phosphorus decasulfide (P4S10) |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE119198C (de) * | ||||
| GB190303045A (en) * | 1903-02-09 | 1904-01-14 | Henri Ensminger | Improvements in the Manufacture of Compounds having a Nitro-cellulose and Casein Base. |
| DE309618C (de) * | 1915-02-03 | |||
| US2569128A (en) * | 1948-03-24 | 1951-09-25 | Monsanto Chemicals | Method of producing phosphorus sulfides |
| GB727573A (en) * | 1951-07-30 | 1955-04-06 | Standard Oil Dev Co | Improvements in or relating to phospho-sulphurisation of organic materials |
| US2794705A (en) * | 1954-07-23 | 1957-06-04 | Monsanto Chemicals | Method of continuously producing a phosphorus sulfide |
| GB855005A (en) * | 1958-07-24 | 1960-11-23 | Exxon Research Engineering Co | Method for producing metal salts of di-organo-dithiophosphates |
| US3524725A (en) * | 1967-12-21 | 1970-08-18 | Knapsack Ag | Process for the manufacture of phosphorus sulfides |
| DE2659295C2 (de) * | 1976-12-29 | 1982-10-28 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Erhöhung der Reaktivität von Phosphorpentasulfid |
| GB2025416A (en) * | 1978-07-14 | 1980-01-23 | Pfizer Ltd | Mercaptopyridazinethione antifungal agents |
| SU1301775A1 (ru) * | 1984-05-07 | 1987-04-07 | Волжский Филиал Ленинградского Государственного Научно-Исследовательского И Проектного Института Основной Химической Промышленности | Способ получени п тисернистого фосфора |
| FR2657341B1 (fr) * | 1990-01-24 | 1992-04-24 | Atochem | Procede continu de preparation de polysulfures de tetraphosphore. |
-
1994
- 1994-08-11 CN CN95109291A patent/CN1141879A/zh active Pending
-
1995
- 1995-03-27 JP JP7525251A patent/JPH09510977A/ja active Pending
- 1995-03-27 EP EP95914897A patent/EP0752998B1/de not_active Expired - Lifetime
- 1995-03-27 US US08/409,011 patent/US5663402A/en not_active Expired - Fee Related
- 1995-03-27 CA CA002186765A patent/CA2186765A1/en not_active Abandoned
- 1995-03-27 WO PCT/US1995/003790 patent/WO1995026357A1/en active IP Right Grant
- 1995-03-27 DE DE69522443T patent/DE69522443T2/de not_active Expired - Fee Related
- 1995-03-27 AT AT95914897T patent/ATE204876T1/de not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| CN1141879A (zh) | 1997-02-05 |
| EP0752998A1 (de) | 1997-01-15 |
| WO1995026357A1 (en) | 1995-10-05 |
| CA2186765A1 (en) | 1995-10-05 |
| DE69522443T2 (de) | 2002-06-13 |
| EP0752998B1 (de) | 2001-08-29 |
| US5663402A (en) | 1997-09-02 |
| JPH09510977A (ja) | 1997-11-04 |
| ATE204876T1 (de) | 2001-09-15 |
| MX9604467A (es) | 1997-07-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |