DE69307701D1 - Verfahren zur reinigung von acetonitril - Google Patents

Verfahren zur reinigung von acetonitril

Info

Publication number
DE69307701D1
DE69307701D1 DE69307701T DE69307701T DE69307701D1 DE 69307701 D1 DE69307701 D1 DE 69307701D1 DE 69307701 T DE69307701 T DE 69307701T DE 69307701 T DE69307701 T DE 69307701T DE 69307701 D1 DE69307701 D1 DE 69307701D1
Authority
DE
Germany
Prior art keywords
acetonitrile
ozone
treatment
purifying acetonitrile
unachievable
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69307701T
Other languages
English (en)
Other versions
DE69307701T2 (de
Inventor
Barry Himes
R Greenough
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Cryodyne Technologies Inc
Original Assignee
Cryodyne Technologies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cryodyne Technologies Inc filed Critical Cryodyne Technologies Inc
Publication of DE69307701D1 publication Critical patent/DE69307701D1/de
Application granted granted Critical
Publication of DE69307701T2 publication Critical patent/DE69307701T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives
    • C07C253/34—Separation; Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Steroid Compounds (AREA)
DE69307701T 1992-05-21 1993-05-18 Verfahren zur reinigung von acetonitril Expired - Lifetime DE69307701T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US88674592A 1992-05-21 1992-05-21
PCT/US1993/004731 WO1993023366A1 (en) 1992-05-21 1993-05-18 Method for purification of acetonitrile

Publications (2)

Publication Number Publication Date
DE69307701D1 true DE69307701D1 (de) 1997-03-06
DE69307701T2 DE69307701T2 (de) 1997-05-15

Family

ID=25389676

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69307701T Expired - Lifetime DE69307701T2 (de) 1992-05-21 1993-05-18 Verfahren zur reinigung von acetonitril

Country Status (6)

Country Link
US (1) US5292919A (de)
EP (1) EP0641314B1 (de)
AT (1) ATE148102T1 (de)
CA (1) CA2136235C (de)
DE (1) DE69307701T2 (de)
WO (1) WO1993023366A1 (de)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5426208A (en) * 1992-05-21 1995-06-20 Cryodyne Technologies, Inc. Method of purification of acetonitrile
WO1994026698A1 (en) * 1993-05-14 1994-11-24 Asahi Kasei Kogyo Kabushiki Kaisha High-purity acetonitrile and purification of crude acetonitrile
DE4397378T1 (de) * 1993-05-14 1995-05-11 Asahi Chemical Ind Hochgereinigtes Acetonitril und Verfahren zur Reinigung von rohem Acetonitril
US5629443A (en) * 1993-05-14 1997-05-13 Asahi Kasei Kogyo Kabushiki Kaisha Highly purified acetonitrile and process for purifying crude acetonitrile
KR0171245B1 (ko) * 1993-05-14 1999-03-30 유미꾸라 레이이찌 고 순도 아세토니트릴 및 미정제 아세토니트릴의 정제 방법
US5440068A (en) * 1993-12-30 1995-08-08 The Standard Oil Company Acetonitrile purification via an adsorption-based process
ES2131269T3 (es) * 1995-01-25 1999-07-16 Standard Oil Co Ohio Purificacion de acetonitrilo por medio de un proceso basado en la adsorcion.
ZA95629B (en) * 1995-01-26 1995-10-05 Standard Oil Co Ohio Acetonitrile purification via an adsorption-based process
TR28966A (tr) * 1995-03-14 1997-07-21 Standard Oil Co Ohio Adsorpsiyona dayali islem vasitasiyla asetonitrilin saflastirilmasi.
DE69906848T2 (de) * 1998-02-23 2003-10-30 Standard Oil The Company Chica Reinigung und Gewinnung von Acetonitril
US6395142B1 (en) 1999-10-14 2002-05-28 Chemcycles, Inc. Method and apparatus for purifying low grade acetonitrile and other constituents from hazardous waste
CN102911973A (zh) * 2005-10-07 2013-02-06 三井化学株式会社 丙烯酰胺的制备方法
CN101597241B (zh) * 2008-06-06 2012-11-21 上海星可高纯溶剂有限公司 一种提纯超净高纯度乙腈的方法
CN101570498B (zh) * 2009-05-27 2013-07-17 安徽时联特种溶剂股份有限公司 一种多级反应—精馏法生产hplc乙腈的方法
CN104584164B (zh) * 2012-09-04 2017-09-05 大金工业株式会社 电解液以及电化学器件
CN104744300A (zh) * 2013-12-31 2015-07-01 上海星可高纯溶剂有限公司 液相色谱-质谱联用仪用乙腈的提纯方法
CN107778198A (zh) * 2016-08-29 2018-03-09 中国石油化工股份有限公司 适用于生物法制备丙烯酰胺的丙烯腈的处理方法
CN107778197B (zh) * 2016-08-29 2020-07-10 中国石油化工股份有限公司 一种丙烯腈的提纯方法
CN116987009A (zh) * 2023-08-14 2023-11-03 西陇科学股份有限公司 一种梯度级乙腈及其制备方法

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2107904A (en) * 1936-09-14 1938-02-08 Armour & Co Process of separating nitrile-hydrocarbon mixtures
US2351157A (en) * 1943-10-30 1944-06-13 Goodrich Co B F Purification of nitriles
US3201451A (en) * 1962-03-23 1965-08-17 Standard Oil Co Purification of acetonitrile
US3322814A (en) * 1964-09-10 1967-05-30 Universal Oil Prod Co Purification of nitriles
US3328458A (en) * 1964-09-10 1967-06-27 Universal Oil Prod Co Purification of nitriles
DE2102886B2 (de) * 1971-01-22 1974-03-14 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt Verfahren zur Gewinnung von reinem Acetonitril
JPS5382722A (en) * 1976-12-13 1978-07-21 Nitto Chem Ind Co Ltd Purification of crude acetonitrile
US4141826A (en) * 1977-03-30 1979-02-27 The Standard Oil Company Treatment of acrylonitrile waste water with activated carbon
SU749828A1 (ru) * 1977-05-10 1980-07-23 Предприятие П/Я В-8873 Способ регенерации ацетонитрила
US4308108A (en) * 1979-03-28 1981-12-29 Asahi Kasei Kogyo Kabushiki Kaisha Process for purification of crude acetonitrile
US4328075A (en) * 1979-12-10 1982-05-04 Standard Oil Company Removal of cyanides from acetonitrile
US4287134A (en) * 1980-06-26 1981-09-01 E. I. Du Pont De Nemours And Company Purification of acetonitrile by caustic extraction
US4362603A (en) * 1981-01-02 1982-12-07 The Standard Oil Company Continuous acetonitrile recovery process
US4474709A (en) * 1982-06-28 1984-10-02 E. I. Du Pont De Nemours And Company Removal of oxazole from acetonitrile
DD217212A1 (de) * 1983-05-10 1985-01-09 Petrolchemisches Kombinat Verfahren zur reinigung von acetonitril
US4575434A (en) * 1984-09-28 1986-03-11 Akzona Incorporated Process for the separation of amides from nitriles
SU1318588A1 (ru) * 1985-08-26 1987-06-23 Всесоюзный Научно-Исследовательский Институт Химических Реактивов И Особо Чистых Химических Веществ Способ очистки ацетонитрила
US4730215A (en) * 1986-05-30 1988-03-08 Rca Corporation Compatible wide screen television system with variable image compression/expansion
US5120881A (en) * 1988-11-22 1992-06-09 Exxon Chemical Patents Inc Removal of nitrogenous components of a hydrocarbon feedstream
FR2655973B1 (fr) * 1989-12-18 1992-03-20 Elf Aquitaine Procede catalytique de degradation oxydative d'effluents aqueux contenant des composes hydrocarbones toxiques.

Also Published As

Publication number Publication date
US5292919A (en) 1994-03-08
EP0641314A1 (de) 1995-03-08
WO1993023366A1 (en) 1993-11-25
ATE148102T1 (de) 1997-02-15
CA2136235A1 (en) 1993-11-25
EP0641314A4 (en) 1995-03-22
EP0641314B1 (de) 1997-01-22
DE69307701T2 (de) 1997-05-15
CA2136235C (en) 2004-04-20

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Legal Events

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8364 No opposition during term of opposition