DE69124282D1 - Anorganische Oxydaerogel-Perlen mit einer schmalen Porendurchmesser-Verteilung - Google Patents

Anorganische Oxydaerogel-Perlen mit einer schmalen Porendurchmesser-Verteilung

Info

Publication number
DE69124282D1
DE69124282D1 DE69124282T DE69124282T DE69124282D1 DE 69124282 D1 DE69124282 D1 DE 69124282D1 DE 69124282 T DE69124282 T DE 69124282T DE 69124282 T DE69124282 T DE 69124282T DE 69124282 D1 DE69124282 D1 DE 69124282D1
Authority
DE
Germany
Prior art keywords
oxydaerogel
beads
inorganic
pore diameter
diameter distribution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69124282T
Other languages
English (en)
Other versions
DE69124282T2 (de
Inventor
Guido Cogliato
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Enichem SpA
Original Assignee
Enichem SpA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Enichem SpA filed Critical Enichem SpA
Application granted granted Critical
Publication of DE69124282D1 publication Critical patent/DE69124282D1/de
Publication of DE69124282T2 publication Critical patent/DE69124282T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14Methods for preparing oxides or hydroxides in general
    • C01B13/32Methods for preparing oxides or hydroxides in general by oxidation or hydrolysis of elements or compounds in the liquid or solid state or in non-aqueous solution, e.g. sol-gel process
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/157After-treatment of gels
    • C01B33/158Purification; Drying; Dehydrating
    • C01B33/1585Dehydration into aerogels
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/30Three-dimensional structures
    • C01P2002/34Three-dimensional structures perovskite-type (ABO3)
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/14Pore volume
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/16Pore diameter

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Catalysts (AREA)
DE69124282T 1990-04-24 1991-04-19 Anorganische Oxydaerogel-Perlen mit einer schmalen Porendurchmesser-Verteilung Expired - Lifetime DE69124282T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
IT20126A IT1240673B (it) 1990-04-24 1990-04-24 Microsfere di aerogels di ossidi inorganici a stretta distribuzione dei diametri dei pori e metodo per la loro preparazione

Publications (2)

Publication Number Publication Date
DE69124282D1 true DE69124282D1 (de) 1997-03-06
DE69124282T2 DE69124282T2 (de) 1997-07-10

Family

ID=11164018

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69124282T Expired - Lifetime DE69124282T2 (de) 1990-04-24 1991-04-19 Anorganische Oxydaerogel-Perlen mit einer schmalen Porendurchmesser-Verteilung

Country Status (8)

Country Link
US (1) US5391364A (de)
EP (1) EP0454239B1 (de)
AT (1) ATE148080T1 (de)
DE (1) DE69124282T2 (de)
DK (1) DK0454239T3 (de)
ES (1) ES2097179T3 (de)
GR (1) GR3022986T3 (de)
IT (1) IT1240673B (de)

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WO1995013132A1 (en) * 1993-11-08 1995-05-18 The Gillette Company Method of forming particles using a supercritical fluid, aerogel particles formed thereby, and antiperspirants containing aerogel particles
US5504042A (en) * 1994-06-23 1996-04-02 Texas Instruments Incorporated Porous dielectric material with improved pore surface properties for electronics applications
IT1275412B (it) * 1995-06-01 1997-08-05 Enichem Spa Procedimento per la preparazione di ossidi misti silice-allumina porosi in forma sferica
US5753305A (en) * 1995-11-16 1998-05-19 Texas Instruments Incorporated Rapid aging technique for aerogel thin films
US6319852B1 (en) 1995-11-16 2001-11-20 Texas Instruments Incorporated Nanoporous dielectric thin film formation using a post-deposition catalyst
US6130152A (en) 1995-11-16 2000-10-10 Texas Instruments Incorporated Aerogel thin film formation from multi-solvent systems
US6037277A (en) * 1995-11-16 2000-03-14 Texas Instruments Incorporated Limited-volume apparatus and method for forming thin film aerogels on semiconductor substrates
US6380105B1 (en) 1996-11-14 2002-04-30 Texas Instruments Incorporated Low volatility solvent-based method for forming thin film nanoporous aerogels on semiconductor substrates
US5807607A (en) 1995-11-16 1998-09-15 Texas Instruments Incorporated Polyol-based method for forming thin film aerogels on semiconductor substrates
US5955140A (en) * 1995-11-16 1999-09-21 Texas Instruments Incorporated Low volatility solvent-based method for forming thin film nanoporous aerogels on semiconductor substrates
US5736425A (en) * 1995-11-16 1998-04-07 Texas Instruments Incorporated Glycol-based method for forming a thin-film nanoporous dielectric
ATE224405T1 (de) * 1996-05-01 2002-10-15 Ineos Silicas Ltd Poröser, anorganischer katalysatorträger
DE19639016A1 (de) * 1996-09-23 1998-03-26 Basf Ag Mesoporöses Siliciumdioxid, Verfahren zu seiner Herstellung und seiner Verwendung
US5877100A (en) * 1996-09-27 1999-03-02 Cabot Corporation Compositions and insulation bodies having low thermal conductivity
JPH10202107A (ja) * 1997-01-22 1998-08-04 Mazda Motor Corp 排気ガス浄化用触媒及び排気ガス浄化方法
US6315971B1 (en) 1997-04-09 2001-11-13 Cabot Corporation Process for producing low density gel compositions
US6071486A (en) * 1997-04-09 2000-06-06 Cabot Corporation Process for producing metal oxide and organo-metal oxide compositions
US6172120B1 (en) 1997-04-09 2001-01-09 Cabot Corporation Process for producing low density gel compositions
FR2763258B1 (fr) * 1997-05-15 1999-06-25 Commissariat Energie Atomique Procede de fabrication d'oxydes metalliques, simples ou mixtes, ou d'oxyde de silicium
US6139816A (en) * 1997-06-09 2000-10-31 Merck Kanto Advanced Chemical Ltd Process for the preparation of ultra-fine powders of metal oxides
AU712920B2 (en) * 1997-06-13 1999-11-18 Nippon Shokubai Co., Ltd. Zirconia powder, method for producing the same, and zirconia ceramics using the same
US6090359A (en) * 1998-02-17 2000-07-18 The Dow Chemical Company Process for hydrogenating aromatic polymers
US6241955B1 (en) * 1998-10-02 2001-06-05 Aeronex, Inc. Method and apparatus for purification of hydride gas streams
US5958363A (en) * 1998-10-29 1999-09-28 The Regents Of The University Of California Method for making monolithic metal oxide aerogels
US6812259B2 (en) * 2001-10-26 2004-11-02 Battelle Memorial Institute Hydroetching of high surface area ceramics using moist supercritical fluids
CN100445204C (zh) * 2001-11-27 2008-12-24 三菱化学株式会社 二氧化硅及其制造方法
JP2003226515A (ja) * 2001-11-27 2003-08-12 Mitsubishi Chemicals Corp シリカ及びその製造方法
FR2843955B1 (fr) * 2002-08-30 2005-05-20 Centre Nat Rech Scient Procede de preparation de poudres d'oxydes inorganiques, de composes cristallins et utilisation de ces composes
US20040091411A1 (en) * 2002-11-08 2004-05-13 Bijan Modrek-Najafabadi High surface area, high porosity silica packing with narrow particle and pore diameter distribution and methods of making same
US7348293B2 (en) * 2003-12-05 2008-03-25 Chevron U.S.A. Inc. Homogeneous modified-alumina Fischer-Tropsch catalyst supports
CA2690537A1 (en) * 2007-06-04 2008-12-11 Alltech Associates, Inc. Silica particles and methods of making and using the same
EA201070098A1 (ru) * 2007-07-05 2010-06-30 Грейс Гмбх Унд Ко. Кг Способ получения катализаторов на носителе из неорганического оксида
WO2009140030A2 (en) 2008-05-15 2009-11-19 Arizona Board Of Regents For And On Behalf Of Arizona State University Porous metal oxide particles
ITMI20090950A1 (it) * 2009-05-29 2010-11-30 Gegussa Novara Technology Spa Processo per la preparazione di un aerogelo in pellets
WO2011046910A2 (en) 2009-10-14 2011-04-21 Arizona Board Of Regents For And On Behalf Of Arizona State University Fabricating porous materials using thixotropic gels
WO2011068830A2 (en) 2009-12-01 2011-06-09 Arizona Board Of Regents For And On Behalf Of Arizona State University Porous geopolymer materials
TWI411467B (zh) * 2010-08-02 2013-10-11 Ind Tech Res Inst 金屬孔洞材料、其製備方法及含氮化合物之檢測方法
BR112013002869A2 (pt) * 2010-08-05 2016-06-14 Pq Corp hidrogel de sílica impregnado com tio2 e métodos de preparar o mesmo
WO2012018890A2 (en) 2010-08-06 2012-02-09 Arizona Board Of Regents For And On Behalf Of Arizona State University Fabricating porous materials using intrepenetrating inorganic-organic composite gels
KR101187568B1 (ko) * 2010-09-29 2012-10-04 한국에너지기술연구원 실리카 에어로겔 과립의 제조방법
WO2013044016A2 (en) 2011-09-21 2013-03-28 Arizona Board Of Regents, A Body Corporate Of The State Of Arizona Acting For And On Behalf Of Arizona State University Geopolymer resin materials, geopolymer materials, and materials produced thereby
WO2015006010A2 (en) 2013-06-21 2015-01-15 Dong-Kyun Seo Metal oxides from acidic solutions
US10926241B2 (en) 2014-06-12 2021-02-23 Arizona Board Of Regents On Behalf Of Arizona State University Carbon dioxide adsorbents
TW201641544A (zh) * 2015-05-27 2016-12-01 Univ Kun Shan 氣凝膠顆粒及其製備方法
WO2018136695A1 (en) 2017-01-20 2018-07-26 Seo Dong Kyun Aluminosilicate nanorods
US11097242B2 (en) * 2017-11-27 2021-08-24 Taiwan Aerogel Technology Materials Co., Ltd. Wet gel granule of aerogel and preparation method thereof

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GB1170622A (en) * 1967-01-10 1969-11-12 British Petroleum Co Improvements relating to the preparation of Catalysts
US3862104A (en) * 1972-01-07 1975-01-21 Phillips Petroleum Co Large pore silica gel catalysts
DE2414478C3 (de) * 1974-03-26 1978-07-13 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt Aerogelartige strukturierte Kieselsäure und Verfahren zu ihrer Herstellung
NL7707961A (nl) * 1977-07-18 1979-01-22 Stamicarbon Werkwijze ter bereiding van poreus, zuiver siliciumdioxyde.
US4246137A (en) * 1979-05-31 1981-01-20 Chemplex Company Method of preparing zirconia-silica xerogels, the xerogels, and xerogel catalysts
US4299731A (en) * 1980-02-06 1981-11-10 Phillips Petroleum Company Large pore volume olefin polymerization catalysts
US4717708A (en) * 1983-12-27 1988-01-05 Stauffer Chemical Company Inorganic oxide aerogels and their preparation
US4851150A (en) * 1984-02-27 1989-07-25 University Of Florida Drying control chemical additives for rapid production of large sol-gel derived silicon, boron and sodium containing monoliths
GB8501882D0 (en) * 1985-01-25 1985-02-27 Atomic Energy Authority Uk Materials
US4851373A (en) * 1985-02-25 1989-07-25 University Of Florida Large sol-gel SiO2 monoliths containing transition metal and their production
US4610863A (en) * 1985-09-04 1986-09-09 The United States Of America As Represented By The United States Department Of Energy Process for forming transparent aerogel insulating arrays
US4776867A (en) * 1986-08-15 1988-10-11 Gte Laboratories Incorporated Process for molding optical components of silicate glass to a near net shape optical precision
GB2196621A (en) * 1986-10-23 1988-05-05 Plessey Co Plc Particulate oxide materials
US4927560A (en) * 1987-02-25 1990-05-22 Nippon Shokubai Kagaku Kogyo Co., Ltd. Method for production of inorganic minute globular particles
SE459731B (sv) * 1987-06-29 1989-07-31 Eka Nobel Ab Silikapartiklar, foerfarande foer deras framstaellning samt anvaendning av partiklarna
US4845056A (en) * 1987-10-09 1989-07-04 Allied-Signal Inc. Continuous process for production of fine particulate ceramics
DE3834774C2 (de) * 1988-10-12 1995-01-05 Fraunhofer Ges Forschung Verfahren zur Herstellung einer kugelförmige Oxidteilchen enthaltenden Suspension
IT1240613B (it) * 1990-03-26 1993-12-17 Enichem Anic Spa Catalizzatore supportato per la polimerizzazione e la copolimerizzazione di composti olefinicamente insaturi, e procedimento di (co) polimerizzazione impiegante lo stesso

Also Published As

Publication number Publication date
IT1240673B (it) 1993-12-17
EP0454239B1 (de) 1997-01-22
GR3022986T3 (en) 1997-06-30
EP0454239A2 (de) 1991-10-30
US5391364A (en) 1995-02-21
IT9020126A0 (it) 1990-04-24
DK0454239T3 (da) 1997-04-28
IT9020126A1 (it) 1991-10-24
ATE148080T1 (de) 1997-02-15
DE69124282T2 (de) 1997-07-10
ES2097179T3 (es) 1997-04-01
EP0454239A3 (en) 1992-10-28

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Legal Events

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