DE69011325D1 - Verfahren zur herstellung von dinitrotoluol unter verwendung eines anorganischen salzes als phasentrennmittel. - Google Patents

Verfahren zur herstellung von dinitrotoluol unter verwendung eines anorganischen salzes als phasentrennmittel.

Info

Publication number
DE69011325D1
DE69011325D1 DE69011325T DE69011325T DE69011325D1 DE 69011325 D1 DE69011325 D1 DE 69011325D1 DE 69011325 T DE69011325 T DE 69011325T DE 69011325 T DE69011325 T DE 69011325T DE 69011325 D1 DE69011325 D1 DE 69011325D1
Authority
DE
Germany
Prior art keywords
dinitrotoluol
producing
release agent
inorganic salt
phase release
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69011325T
Other languages
English (en)
Other versions
DE69011325T2 (de
Inventor
Robert Mason
Peter Imm
Kent Bordelon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Olin Corp
Original Assignee
Olin Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Olin Corp filed Critical Olin Corp
Application granted granted Critical
Publication of DE69011325D1 publication Critical patent/DE69011325D1/de
Publication of DE69011325T2 publication Critical patent/DE69011325T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/06—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/16—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE69011325T 1989-04-21 1990-02-09 Verfahren zur herstellung von dinitrotoluol unter verwendung eines anorganischen salzes als phasentrennmittel. Expired - Fee Related DE69011325T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US07/341,447 US4918250A (en) 1989-04-21 1989-04-21 Process for the production of dinitrotoluene using an inorganic salt as a phase separation agent
PCT/US1990/000654 WO1990012781A1 (en) 1989-04-21 1990-02-09 Process for the production of dinitrotoluene using an inorganic salt as a phase separation agent

Publications (2)

Publication Number Publication Date
DE69011325D1 true DE69011325D1 (de) 1994-09-08
DE69011325T2 DE69011325T2 (de) 1994-12-08

Family

ID=23337614

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69011325T Expired - Fee Related DE69011325T2 (de) 1989-04-21 1990-02-09 Verfahren zur herstellung von dinitrotoluol unter verwendung eines anorganischen salzes als phasentrennmittel.

Country Status (10)

Country Link
US (1) US4918250A (de)
EP (1) EP0468968B1 (de)
JP (1) JPH04504844A (de)
KR (1) KR920701119A (de)
CN (1) CN1027446C (de)
AU (1) AU5156090A (de)
DE (1) DE69011325T2 (de)
MX (1) MX163846B (de)
PT (1) PT93174B (de)
WO (1) WO1990012781A1 (de)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5012019A (en) * 1990-01-26 1991-04-30 Olin Corporation Process for purifying aromatic nitration products
US5099079A (en) * 1990-07-26 1992-03-24 Olin Corporation Process for separating acid from nitro substituted aromatics using a molten nitrate salt
US5057632A (en) * 1990-10-22 1991-10-15 Olin Corporation Process for preparing dinitrotoluene
US5099078A (en) * 1990-12-21 1992-03-24 Olin Corporation Process for preparing dinitrotoluene
US5099080A (en) * 1991-03-08 1992-03-24 Olin Corporation Process for preparing dinitrotoluene
US5245092A (en) * 1991-03-15 1993-09-14 Olin Corporation Process for preparing dinitrotoluene with low by-product content
DE4216416C1 (de) * 1992-05-18 1993-05-13 Bayer Ag, 5090 Leverkusen, De
US5302763A (en) * 1993-03-01 1994-04-12 Olin Corporation Process for preparing dinitrotoluene
DE4437047A1 (de) 1994-10-17 1996-04-18 Bayer Ag Verfahren zur Dinitrierung von aromatischen Verbindungen
DE102006033722A1 (de) * 2006-07-21 2008-01-24 Bayer Materialscience Ag Verfahren zur Herstellung von Dinitrotoluol
KR102029504B1 (ko) * 2011-08-09 2019-10-07 바스프 에스이 미정제 방향족 니트로 화합물의 재처리로부터의 폐수 정제 방법
CN110655513A (zh) * 2019-10-23 2020-01-07 浙江南郊化学有限公司 一种丙炔氟草胺的合成方法

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2362743A (en) * 1943-02-10 1944-11-14 Hercules Powder Co Ltd Manufacture of dinitrotoluene
US2739174A (en) * 1951-09-08 1956-03-20 Eastman Kodak Co Nitrating aromatic hydrocarbons with only nitric acid
US2864871A (en) * 1956-07-20 1958-12-16 Goodrich Co B F Method of producing dinitro-tetra alkyl benzenes
DE1468362A1 (de) * 1964-10-23 1968-11-28 Meissner Fa Josef Zweistufige Anlage zur Nitrierung von aromatischen Kohlenwasserstoffen
US3293310A (en) * 1966-02-08 1966-12-20 Jean P Picard Preparation of dinitrotoluene and trinitrotoluene with boron trifluoride and nitric acid
US3780116A (en) * 1972-06-15 1973-12-18 Zaverchand & Co Method for nitration of aromatic hydrocarbon compounds
US3928395A (en) * 1972-10-05 1975-12-23 Ciba Geigy Ag Process for the nitration of aromatic compounds
US3976704A (en) * 1975-01-06 1976-08-24 Varen Technology Nitration process
DE2521891B2 (de) * 1975-05-16 1980-02-28 Bayer Ag, 5090 Leverkusen Verfahren zum Abstoppen von Nitrierungen durch Destillation
DE2622313C3 (de) * 1976-05-19 1980-09-25 Bayer Ag, 5090 Leverkusen Verfahren zur kontinuierlichen Herstellung von Mononitroaromaten
DE2704680A1 (de) * 1977-02-04 1978-08-10 Bayer Ag Verfahren zur gewinnung von aromatischen dinitroverbindungen
US4123466A (en) * 1977-12-12 1978-10-31 The Upjohn Company Process for nitrating aromatic hydrocarbons
US4418230A (en) * 1978-06-21 1983-11-29 Aktiebolaget Bofors Method for gaseous phase nitration of aromatics
US4426543A (en) * 1980-11-26 1984-01-17 Monsanto Company Vapor phase nitration of aromatic hydrocarbons
US4415744A (en) * 1981-10-21 1983-11-15 Monsanto Company Vapor phase nitration of aromatic compounds
JPS58180460A (ja) * 1982-04-16 1983-10-21 Sumitomo Chem Co Ltd ニトロ化方法
US4465876A (en) * 1983-02-07 1984-08-14 Air Products And Chemicals, Inc. Nitration of aromatics with nitrogen oxides in trifluoroacetic acid
US4469904A (en) * 1983-07-05 1984-09-04 W. R. Grace & Co. Preparation of nitro compounds by vapor phase nitration of carboxylic acids
US4482769A (en) * 1983-09-16 1984-11-13 Air Products And Chemicals, Inc. Reducing 2,4-dinitroortho-cresol in effluent stream from dinitrotoluene process
US4621157A (en) * 1984-05-07 1986-11-04 Jerome A. Gross Nitration processes
US4618733A (en) * 1984-11-14 1986-10-21 Monsanto Company Vapor phase nitration of aromatic compounds
US4628131A (en) * 1984-11-14 1986-12-09 Monsanto Company Vapor phase nitration of aromatic compounds
US4600702A (en) * 1984-11-14 1986-07-15 Monsanto Company Vapor phase nitration catalysts
US4804792A (en) * 1988-01-28 1989-02-14 Olin Corporation Nitration of benzene or toluene in a molten nitrate salt

Also Published As

Publication number Publication date
US4918250A (en) 1990-04-17
AU5156090A (en) 1990-11-16
PT93174B (pt) 1995-12-29
EP0468968A1 (de) 1992-02-05
CN1027446C (zh) 1995-01-18
JPH04504844A (ja) 1992-08-27
KR920701119A (ko) 1992-08-11
MX163846B (es) 1992-06-25
EP0468968B1 (de) 1994-08-03
EP0468968A4 (en) 1992-05-20
DE69011325T2 (de) 1994-12-08
WO1990012781A1 (en) 1990-11-01
PT93174A (pt) 1990-11-20
CN1046521A (zh) 1990-10-31

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee