DE60106306D1 - Verfahren und Vorrichtung zur Herstellung von Ammoniak - Google Patents

Verfahren und Vorrichtung zur Herstellung von Ammoniak

Info

Publication number
DE60106306D1
DE60106306D1 DE2001606306 DE60106306T DE60106306D1 DE 60106306 D1 DE60106306 D1 DE 60106306D1 DE 2001606306 DE2001606306 DE 2001606306 DE 60106306 T DE60106306 T DE 60106306T DE 60106306 D1 DE60106306 D1 DE 60106306D1
Authority
DE
Germany
Prior art keywords
synthesis gas
ammonia
feed stream
stream
catalyst beds
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE2001606306
Other languages
English (en)
Other versions
DE60106306T2 (de
Inventor
Erik Andreas Gam
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Topsoe AS
Original Assignee
Haldor Topsoe AS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Haldor Topsoe AS filed Critical Haldor Topsoe AS
Publication of DE60106306D1 publication Critical patent/DE60106306D1/de
Application granted granted Critical
Publication of DE60106306T2 publication Critical patent/DE60106306T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/04Preparation of ammonia by synthesis in the gas phase
    • C01C1/0405Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0449Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
    • B01J8/0453Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being superimposed one above the other
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0461Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical annular shaped beds
    • B01J8/0465Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical annular shaped beds the beds being concentric
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/04Preparation of ammonia by synthesis in the gas phase
    • C01C1/0405Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
    • C01C1/0417Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst characterised by the synthesis reactor, e.g. arrangement of catalyst beds and heat exchangers in the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00106Controlling the temperature by indirect heat exchange
    • B01J2208/00168Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212Plates; Jackets; Cylinders
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/52Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Catalysts (AREA)
DE60106306T 2000-02-10 2001-01-24 Verfahren und Vorrichtung zur Herstellung von Ammoniak Expired - Lifetime DE60106306T2 (de)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DKPA200000207 2000-02-10
DK200000207 2000-02-17
DK200000248 2000-02-17
DKPA200000248 2000-02-17

Publications (2)

Publication Number Publication Date
DE60106306D1 true DE60106306D1 (de) 2004-11-18
DE60106306T2 DE60106306T2 (de) 2006-02-23

Family

ID=26068762

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60106306T Expired - Lifetime DE60106306T2 (de) 2000-02-10 2001-01-24 Verfahren und Vorrichtung zur Herstellung von Ammoniak

Country Status (11)

Country Link
US (1) US6540971B2 (de)
EP (1) EP1123899B1 (de)
JP (1) JP5046437B2 (de)
KR (1) KR100445253B1 (de)
CN (1) CN1205123C (de)
AT (1) ATE279374T1 (de)
CA (1) CA2335384C (de)
DE (1) DE60106306T2 (de)
NO (1) NO331614B1 (de)
RU (1) RU2262482C2 (de)
TW (1) TWI281458B (de)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5373410B2 (ja) 2009-01-09 2013-12-18 トヨタ自動車株式会社 アンモニア合成方法
AU2010336467B2 (en) 2009-12-23 2013-09-05 Colgate-Palmolive Company Oral care compositions
RU2567791C2 (ru) 2010-12-22 2015-11-10 Колгейт-Палмолив Компани Композиции для ухода за полостью рта
CN102502700B (zh) * 2011-10-21 2014-12-24 山西省霍州市化学工业有限责任公司 一种合成系统更换触媒的方法
CN102500427A (zh) * 2011-10-21 2012-06-20 山西省霍州市化学工业有限责任公司 一种新触媒的硫化方法
JP5821777B2 (ja) * 2012-05-21 2015-11-24 トヨタ自動車株式会社 アンモニア合成方法
EP3115338A1 (de) * 2015-07-07 2017-01-11 Casale SA Verfahren zur modernisierung eines ammoniakwandlers
DK3423407T3 (da) 2016-03-01 2022-09-12 Starfire Energy Elektrisk forbedret haber-bosch (eehb) vandfri ammoniaksyntese
US11325105B2 (en) 2017-05-15 2022-05-10 Starfire Energy Metal-decorated barium calcium aluminum oxide and related materials for NH3 catalysis
WO2018218144A2 (en) * 2017-05-26 2018-11-29 Starfire Energy Removal of gaseous nh3 from an nh3 reactor product stream
EP3917668A4 (de) 2019-01-31 2022-11-23 Starfire Energy Metallverzierter barium-calcium-aluminiumoxid-katalysator für nh3-synthese und kracken und verfahren zu dessen herstellung
US12053536B2 (en) 2021-04-08 2024-08-06 Colgate-Palmolive Company Oral care compositions
CN114307869A (zh) * 2021-12-17 2022-04-12 南京敦先化工科技有限公司 一种氨合成反应器

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3721532A (en) * 1971-02-08 1973-03-20 Braun Co C Ammonia synthesis system
GB1574723A (en) 1976-03-10 1980-09-10 Haldor Topsoe As Apparatus for the synthesis of ammonia
EP0007743B1 (de) * 1978-07-17 1985-01-02 The M. W. Kellogg Company Ammoniaksynthesis und Umwandler-System dafür
EP0026057B1 (de) * 1979-09-14 1984-03-14 Imperial Chemical Industries Plc Synthesereaktor und Verfahren
FR2473032A1 (fr) * 1980-01-07 1981-07-10 Banquy David Procede de production d'ammoniac et du gaz de synthese correspondant
DE3363367D1 (en) * 1982-04-14 1986-06-12 Ici Plc Ammonia production process
US4518574A (en) * 1983-03-07 1985-05-21 Exxon Research & Engineering Co. Catalytic gas synthesis process
CH666198A5 (it) * 1985-09-13 1988-07-15 Ammonia Casale Sa Reattore per sintesi catalitiche dell'ammoniaca, metanolo ed alcoli superiori.
US4867959A (en) * 1986-11-20 1989-09-19 Santa Fe Braun, Inc. Process for synthesizing ammonia
DE3725564A1 (de) * 1987-08-01 1989-02-09 Uhde Gmbh Verfahren und anlage zur durchfuehrung einer synthese, insbesondere zur synthese von ammoniak
KR940008073Y1 (ko) * 1990-08-31 1994-11-21 삼성항공산업 주식회사 수평다관절 로보트 공구단의 구동장치
DE69111820T2 (de) * 1990-09-24 1995-12-14 Braun C F Inc Ammoniaksynthese mit hohem umwandlungsgrad.
DK173023B1 (da) * 1997-04-21 1999-11-15 Topsoe Haldor As Fremgangsmåde og reaktor til fremstilling af ammoniak
DE69732781T2 (de) 1997-11-28 2006-02-02 Ammonia Casale S.A. Verfahren zur in-situ Modernisierung eines heterogenen exothermen Synthesereaktors

Also Published As

Publication number Publication date
NO331614B1 (no) 2012-02-06
EP1123899B1 (de) 2004-10-13
ATE279374T1 (de) 2004-10-15
DE60106306T2 (de) 2006-02-23
TWI281458B (en) 2007-05-21
NO20010690L (no) 2001-08-13
RU2262482C2 (ru) 2005-10-20
CN1309083A (zh) 2001-08-22
CA2335384C (en) 2008-12-30
US6540971B2 (en) 2003-04-01
EP1123899A1 (de) 2001-08-16
KR20010082120A (ko) 2001-08-29
US20010018039A1 (en) 2001-08-30
NO20010690D0 (no) 2001-02-09
CN1205123C (zh) 2005-06-08
JP5046437B2 (ja) 2012-10-10
CA2335384A1 (en) 2001-08-10
KR100445253B1 (ko) 2004-08-21
JP2001240412A (ja) 2001-09-04

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