DE60013970D1 - Verfahren mit verbesserter Kapazität zur Herstellung und Reinigung von Acrylsäure aus Propylen - Google Patents
Verfahren mit verbesserter Kapazität zur Herstellung und Reinigung von Acrylsäure aus PropylenInfo
- Publication number
- DE60013970D1 DE60013970D1 DE60013970T DE60013970T DE60013970D1 DE 60013970 D1 DE60013970 D1 DE 60013970D1 DE 60013970 T DE60013970 T DE 60013970T DE 60013970 T DE60013970 T DE 60013970T DE 60013970 D1 DE60013970 D1 DE 60013970D1
- Authority
- DE
- Germany
- Prior art keywords
- propylene
- purification
- production
- acrylic acid
- improved capacity
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Revoked
Links
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 title 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 title 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 title 1
- 238000000746 purification Methods 0.000 title 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
- C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US14530899P | 1999-07-23 | 1999-07-23 | |
US145308P | 1999-07-23 |
Publications (2)
Publication Number | Publication Date |
---|---|
DE60013970D1 true DE60013970D1 (de) | 2004-10-28 |
DE60013970T2 DE60013970T2 (de) | 2005-03-31 |
Family
ID=22512500
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE60013970T Revoked DE60013970T2 (de) | 1999-07-23 | 2000-07-20 | Verfahren mit verbesserter Kapazität zur Herstellung und Reinigung von Acrylsäure aus Propylen |
Country Status (9)
Country | Link |
---|---|
US (1) | US6639106B1 (de) |
EP (1) | EP1070700B1 (de) |
JP (1) | JP2001064227A (de) |
KR (1) | KR100735873B1 (de) |
CN (1) | CN1269787C (de) |
BR (1) | BR0003117A (de) |
DE (1) | DE60013970T2 (de) |
MX (1) | MXPA00007106A (de) |
TW (1) | TWI226326B (de) |
Families Citing this family (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2003040079A1 (fr) * | 2001-11-06 | 2003-05-15 | Mitsubishi Chemical Corporation | Procede d'extraction d'acide acrylique |
JP3908118B2 (ja) | 2002-08-08 | 2007-04-25 | 株式会社日本触媒 | アクリル酸の製造方法 |
US20040104108A1 (en) | 2002-12-03 | 2004-06-03 | Mason Robert Michael | High capacity purification of thermally unstable compounds |
DE10351269A1 (de) | 2003-10-31 | 2005-06-02 | Basf Ag | Verfahren zum Langzeitbetrieb einer heterogen katalysierten Gasphasenpartialoxidation von Propen zu Acrylsäure |
US7393976B2 (en) | 2003-11-26 | 2008-07-01 | Rohm And Haas Company | Process for manufacturing reduced water content (meth)acrylic acid |
US20050137422A1 (en) * | 2003-12-19 | 2005-06-23 | Saudi Basic Industries Corporation | Process for producing an unsaturated carboxylic acid from an alkane |
JP5006507B2 (ja) * | 2004-01-30 | 2012-08-22 | 株式会社日本触媒 | アクリル酸の製造方法 |
US7592483B2 (en) | 2004-07-01 | 2009-09-22 | Basf Aktiengesellschaft | Preparation of acrolein or acrylic acid or a mixture thereof by heterogeneously catalyzed partial gas phase oxidation of propylene |
US7414149B2 (en) * | 2004-11-22 | 2008-08-19 | Rohm And Haas Company | Non-routine reactor shutdown method |
DE102005019911A1 (de) | 2005-04-27 | 2006-11-02 | Basf Ag | Verfahren der rektifikativen Auftrennung einer Acrylsäure und/oder Methacrylsäure enthaltenden Flüssigkeit |
DE102006022014A1 (de) * | 2006-05-10 | 2007-11-15 | Degussa Gmbh | Verfahren zur Herstellung von Cyclododecatrien |
DE102006036177B4 (de) * | 2006-07-21 | 2013-05-08 | Evonik Degussa Gmbh | Vorrichtung und Verfahren zur Herstellung von Acrylsäure mit verminderter Autoxidationsneigung |
JP2009263351A (ja) * | 2008-03-31 | 2009-11-12 | Mitsubishi Chemicals Corp | (メタ)アクリル酸の製造方法 |
JP5407486B2 (ja) * | 2008-03-31 | 2014-02-05 | 三菱化学株式会社 | (メタ)アクリル酸および/または(メタ)アクロレインの製造方法 |
JP5507111B2 (ja) * | 2008-05-30 | 2014-05-28 | ローム アンド ハース カンパニー | 水性(メタ)アクリル酸の製造方法 |
EP2346585A4 (de) | 2008-10-15 | 2012-08-08 | Arkema Inc | Verfahren zur rückgewinnung von carboxylsäuren aus verdünnten wässrigen strömen |
US9156769B2 (en) * | 2008-10-15 | 2015-10-13 | Arkema Inc. | Method of recovering carboxylic acids from dilute aqueous streams |
JP2011121048A (ja) * | 2009-12-09 | 2011-06-23 | Rohm & Haas Co | 固体触媒物質をブレンドし、管状構造物に装填する方法 |
CA2781246A1 (en) * | 2011-07-14 | 2013-01-14 | Rohm And Haas Company | Method for removal of organic compounds from waste water streams in a process for production of (meth)acrylic acid |
US9440903B2 (en) | 2012-09-24 | 2016-09-13 | Arkema Inc. | Shell and tube oxidation reactor with improved resistance to fouling |
SG11201607867PA (en) * | 2014-03-24 | 2016-10-28 | Arkema Inc | Method of recovering carboxylic acids from dilute aqueous streams |
CN105061193B (zh) * | 2015-08-10 | 2017-03-22 | 蓝星(北京)技术中心有限公司 | 蛋氨酸生产废水处理中回收有机物的方法 |
EP3768658B1 (de) * | 2018-03-21 | 2024-06-26 | Rohm and Haas Company | Verfahren zur herstellung von acrylsäure |
CN110551020A (zh) * | 2018-05-30 | 2019-12-10 | 中国石油集团东北炼化工程有限公司吉林设计院 | 一种回收废水中丙烯酸的方法 |
KR20220078274A (ko) * | 2020-12-03 | 2022-06-10 | 주식회사 엘지화학 | 아크릴산의 제조 공정 |
CN113582830A (zh) * | 2021-09-30 | 2021-11-02 | 山东蓝湾新材料有限公司 | 一种高效剥离杂质提纯丙烯酸的方法 |
EP4234531A1 (de) * | 2022-02-25 | 2023-08-30 | Evonik Superabsorber GmbH | Abtrennung von acrylsäure mit hilfe von membrankontaktoren |
Family Cites Families (25)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5129124B1 (de) | 1971-04-27 | 1976-08-24 | ||
BE783549A (fr) * | 1972-05-16 | 1972-09-18 | Mines Fond Zinc Vieille | Procede de purification de solutions de sulfate de zinc provenant de lalixiviation des minerais de zinc. |
US3893951A (en) | 1973-02-22 | 1975-07-08 | Standard Oil Co | Catalysts for oxidation reactions |
JPS5246208B2 (de) | 1973-03-22 | 1977-11-22 | ||
JPS5223589A (en) | 1975-08-18 | 1977-02-22 | Mitsubishi Petrochem Co Ltd | Catalyst for producing alpha,beta-unsaturaded carboxylic acid |
US4203906A (en) | 1977-07-13 | 1980-05-20 | Nippon Shokubai Kagaku Kogyo Co., Ltd. | Process for catalytic vapor phase oxidation |
JPS6054939B2 (ja) * | 1977-08-04 | 1985-12-03 | 住友化学工業株式会社 | 粗製アクリル酸の精製方法 |
JPS55102536A (en) | 1979-01-30 | 1980-08-05 | Mitsubishi Petrochem Co Ltd | Preparation of acrylic acid |
JPS5673041A (en) | 1979-11-19 | 1981-06-17 | Mitsubishi Petrochem Co Ltd | Preparation of acrylic acid |
US5198578A (en) | 1986-07-17 | 1993-03-30 | Union Carbide Chemicals | Anhydrous diluents for the propylene oxidation reaction to acrolein and acrolein oxidation to acrylic acid |
CA1299193C (en) * | 1986-07-17 | 1992-04-21 | Gordon Gene Harkreader | Anhydrous diluents for the propylene oxidation reaction to acrolein and acrolein oxidation to acrylic acid |
JPH0813777B2 (ja) * | 1986-12-11 | 1996-02-14 | 三菱化学株式会社 | アクリル酸の製造法 |
AU606160B2 (en) | 1987-05-27 | 1991-01-31 | Nippon Shokubai Kagaku Kogyo Co. Ltd. | Process for production of acrylic acid |
JPH0686399B2 (ja) * | 1987-05-27 | 1994-11-02 | 株式会社日本触媒 | アクリル酸の製造方法 |
KR950003119B1 (ko) | 1989-11-06 | 1995-04-01 | 니혼 쇼꾸바이 가가꾸 고오교 가부시끼가이샤 | 아크릴산의 제조방법 |
DE4023239A1 (de) | 1990-07-21 | 1992-01-23 | Basf Ag | Verfahren zur katalytischen gasphasenoxidation von propen oder iso-buten zu acrolein oder methacrolein |
EP0487900A1 (de) * | 1990-11-27 | 1992-06-03 | Kabushiki Kaisha Toshiba | Tragbarer Rechner für Rückstellung eines Wiederaufnahmefehlers, verursacht durch Veränderung einer HDD-geladenen Bedingung und BS-Start |
DE4132263A1 (de) * | 1991-09-27 | 1993-04-01 | Basf Ag | Verfahren zur katalytischen gasphasenoxidation von acrolein zu acrylsaeure |
DE4302991A1 (de) | 1993-02-03 | 1994-08-04 | Basf Ag | Multimetalloxidmassen |
JP3937462B2 (ja) | 1994-08-04 | 2007-06-27 | 三菱化学株式会社 | アクリル酸精製法 |
DE4431949A1 (de) * | 1994-09-08 | 1995-03-16 | Basf Ag | Verfahren zur katalytischen Gasphasenoxidation von Acrolein zu Acrylsäure |
JP3299424B2 (ja) * | 1994-11-14 | 2002-07-08 | 株式会社日本触媒 | アクリル酸製造用触媒およびその製造法 |
EP0811597B1 (de) | 1994-11-14 | 2000-08-23 | Nippon Shokubai Co., Ltd. | Verfahren zur Herstellung von Acrylsäure |
ATE219480T1 (de) | 1996-04-01 | 2002-07-15 | Union Carbide Chem Plastic | Verfahren zur oxidation von alkanen |
KR20010104053A (ko) * | 2000-05-12 | 2001-11-24 | 성재갑 | 프로필렌의 기상 산화 반응에 의한 아크롤레인의 제조 방법 |
-
2000
- 2000-07-19 US US09/619,403 patent/US6639106B1/en not_active Expired - Lifetime
- 2000-07-20 TW TW089114533A patent/TWI226326B/zh not_active IP Right Cessation
- 2000-07-20 DE DE60013970T patent/DE60013970T2/de not_active Revoked
- 2000-07-20 MX MXPA00007106A patent/MXPA00007106A/es unknown
- 2000-07-20 EP EP00306172A patent/EP1070700B1/de not_active Revoked
- 2000-07-21 KR KR1020000041994A patent/KR100735873B1/ko active IP Right Grant
- 2000-07-24 JP JP2000222102A patent/JP2001064227A/ja active Pending
- 2000-07-24 BR BR0003117-8A patent/BR0003117A/pt not_active Application Discontinuation
- 2000-07-24 CN CNB00121697XA patent/CN1269787C/zh not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
EP1070700B1 (de) | 2004-09-22 |
TWI226326B (en) | 2005-01-11 |
CN1282727A (zh) | 2001-02-07 |
JP2001064227A (ja) | 2001-03-13 |
BR0003117A (pt) | 2001-03-13 |
US6639106B1 (en) | 2003-10-28 |
CN1269787C (zh) | 2006-08-16 |
EP1070700A2 (de) | 2001-01-24 |
DE60013970T2 (de) | 2005-03-31 |
EP1070700A3 (de) | 2003-01-02 |
KR20010049838A (ko) | 2001-06-15 |
KR100735873B1 (ko) | 2007-07-06 |
MXPA00007106A (es) | 2002-06-04 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8363 | Opposition against the patent | ||
8331 | Complete revocation |