DE60013197D1 - Verfahren zur Hemmung der Polymerisation von leicht polymerisierenden Substanzen - Google Patents
Verfahren zur Hemmung der Polymerisation von leicht polymerisierenden SubstanzenInfo
- Publication number
- DE60013197D1 DE60013197D1 DE60013197T DE60013197T DE60013197D1 DE 60013197 D1 DE60013197 D1 DE 60013197D1 DE 60013197 T DE60013197 T DE 60013197T DE 60013197 T DE60013197 T DE 60013197T DE 60013197 D1 DE60013197 D1 DE 60013197D1
- Authority
- DE
- Germany
- Prior art keywords
- inhibiting
- polymerization
- slightly
- polymerizing substances
- polymerizing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/50—Use of additives, e.g. for stabilisation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
- B01D3/148—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step in combination with at least one evaporator
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/16—Fractionating columns in which vapour bubbles through liquid
- B01D3/18—Fractionating columns in which vapour bubbles through liquid with horizontal bubble plates
- B01D3/20—Bubble caps; Risers for vapour; Discharge pipes for liquid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
- C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
- C07C57/03—Monocarboxylic acids
- C07C57/04—Acrylic acid; Methacrylic acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/22—Accessories
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11004399 | 1999-04-16 | ||
JP11004399 | 1999-04-16 |
Publications (2)
Publication Number | Publication Date |
---|---|
DE60013197D1 true DE60013197D1 (de) | 2004-09-30 |
DE60013197T2 DE60013197T2 (de) | 2005-08-11 |
Family
ID=14525674
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE60013197T Expired - Lifetime DE60013197T2 (de) | 1999-04-16 | 2000-04-14 | Verfahren zur Hemmung der Polymerisation von leicht polymerisierbaren Verbindungen |
Country Status (9)
Country | Link |
---|---|
US (1) | US6409886B1 (de) |
EP (1) | EP1044957B1 (de) |
JP (1) | JP3787261B2 (de) |
KR (1) | KR100423210B1 (de) |
CN (1) | CN1178893C (de) |
BR (1) | BR0001605A (de) |
DE (1) | DE60013197T2 (de) |
MY (1) | MY122586A (de) |
ZA (1) | ZA200001882B (de) |
Families Citing this family (42)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4759153B2 (ja) * | 2001-03-21 | 2011-08-31 | 株式会社日本触媒 | (メタ)アクリル酸溶液の蒸留方法 |
KR100382938B1 (ko) | 2001-06-21 | 2003-05-09 | 엘지전자 주식회사 | 보조 표시창이 포함된 폴더형 휴대폰 |
JP4233007B2 (ja) * | 2001-09-28 | 2009-03-04 | 株式会社日本触媒 | 低熱伝導性材料が付設されている精製装置 |
JP2003164817A (ja) * | 2001-12-03 | 2003-06-10 | Mitsubishi Chemicals Corp | 易重合性化合物の洗浄除去方法 |
CN1260198C (zh) * | 2001-10-09 | 2006-06-21 | 三菱化学株式会社 | 停止蒸馏塔运转的方法 |
CN1238326C (zh) | 2001-12-06 | 2006-01-25 | 三菱化学株式会社 | 氧化反应器和(甲基)丙烯酸类的制备方法 |
WO2003057658A1 (fr) * | 2002-01-08 | 2003-07-17 | Mitsubishi Chemical Corporation | Procede permettant d'empecher l'encrassement d'un appareil de manipulation de l'acide (meth)acrylique et de son ester |
WO2003064370A1 (en) * | 2002-01-30 | 2003-08-07 | Mitsubishi Chemical Corporation | Process for producing (meth)acrylic ester |
CN100379776C (zh) * | 2002-02-06 | 2008-04-09 | 株式会社日本触媒 | 在非稳定状态下冷却加热用换热器的方法 |
ATE496019T1 (de) | 2002-02-15 | 2011-02-15 | Chemtura Corp | Nitrosophenole und c-nitrosoaniline als polymerisationsinhibitoren |
JPWO2003078015A1 (ja) * | 2002-03-20 | 2005-07-14 | 三菱レイヨン株式会社 | 易重合性物質の精製装置および精製方法 |
TWI254648B (en) | 2002-05-01 | 2006-05-11 | Rohm & Haas | Process for manufacturing high purity methacrylic acid |
ZA200303241B (en) | 2002-05-01 | 2003-11-04 | Rohm & Haas | Improved process for methacrylic acid and methcrylic acid ester production. |
JP2004064039A (ja) * | 2002-06-07 | 2004-02-26 | Fuji Photo Film Co Ltd | パターン形成方法及びパターン形成装置 |
US6983758B2 (en) * | 2002-07-05 | 2006-01-10 | Rohm And Haas Company | Prevention of unwanted material accumulations |
EP1561521A3 (de) | 2002-07-05 | 2006-03-15 | Rohm And Haas Company | Apparat zur Vermeidung von unerwünschter Materialansammlung |
EP1640647A3 (de) | 2002-07-05 | 2006-04-12 | Rohm and Haas Company | Ventilmontagevorrichtung |
JP4440518B2 (ja) | 2002-07-16 | 2010-03-24 | 株式会社日本触媒 | アクリル酸の製造方法 |
US20040104108A1 (en) | 2002-12-03 | 2004-06-03 | Mason Robert Michael | High capacity purification of thermally unstable compounds |
DE10300499A1 (de) * | 2003-01-08 | 2003-10-23 | Basf Ag | Verfahren der rektifikativen Auftrennung von (Meth)acrylmonomere enthaltenden Fluiden |
DE10300816A1 (de) | 2003-01-10 | 2004-07-22 | Basf Ag | Thermisches Trennverfahren zwischen wenigstens einem gasförmigen und wenigstens einem flüssigen Stoffstrom, von denen wenigstens einer (Meth)acrylmonomere enthält |
DE10317436A1 (de) * | 2003-04-15 | 2004-10-28 | Basf Ag | Thermische Trennverfahren |
JP4510806B2 (ja) * | 2003-04-15 | 2010-07-28 | ビーエーエスエフ ソシエタス・ヨーロピア | 熱分離法及び分離塔 |
JP2004359616A (ja) | 2003-06-05 | 2004-12-24 | Asahi Glass Co Ltd | (メタ)アクリル酸ポリフルオロアルキルエステルの製造方法 |
JP2005060331A (ja) * | 2003-08-19 | 2005-03-10 | Mitsubishi Chemicals Corp | 易重合性物質の重合防止方法、易重合性物質の取り扱い装置及びトレイ |
WO2005046860A1 (ja) * | 2003-11-17 | 2005-05-26 | Mitsubishi Chemical Corporation | 易重合性化合物用の容器 |
JP3847754B2 (ja) * | 2004-02-03 | 2006-11-22 | 石油資源開発株式会社 | 蒸留塔を用いた水銀除去方法 |
JP4466190B2 (ja) * | 2004-05-17 | 2010-05-26 | 三菱化学株式会社 | 易重合性化合物の取り扱い装置及び製造装置 |
RU2443716C2 (ru) * | 2006-06-01 | 2012-02-27 | Джон О. БАРНЕТТ | Способ и аппарат для минимизации отложений полимера на технологическом оборудовании, в частности на защитных устройствах |
US8157969B2 (en) * | 2006-06-01 | 2012-04-17 | Rohm And Haas Company | Method and apparatus for minimizing accumulation of polymer on process equipment, especially safety devices |
KR101477491B1 (ko) | 2006-09-15 | 2014-12-31 | 알케마 인코포레이티드 | 아크릴산의 제조방법 |
US7799946B2 (en) * | 2007-02-14 | 2010-09-21 | Saudi Basic Industries Corporation | Process for separating methacrolein from methacrylic acid in a gas phase product from the partial oxidation of isobutene |
DE102009046310B4 (de) * | 2008-11-24 | 2018-10-25 | Basf Se | Verfahren zur destillativen Gewinnung von Rein-1,3-Butadien aus Roh-1,3-Butadien |
FR3008899B1 (fr) | 2013-07-25 | 2017-04-21 | Arkema France | Methode et systeme pour la distribution d'un liquide dans des capacites pour la preparation de monomeres (meth)acryliques |
DE102014215437A1 (de) * | 2014-08-05 | 2015-11-05 | Basf Se | Kolonne zur thermischen Behandlung eines Fluids |
DE102015213493A1 (de) * | 2015-07-17 | 2016-09-15 | Basf Se | Kolonne zur thermischen Behandlung von fluiden Gemischen, insbesondere solchen, die (Meth)acrylmonomere enthalten |
DE102015213490A1 (de) * | 2015-07-17 | 2016-09-15 | Basf Se | Kolonne zur thermischen Behandlung von fluiden Gemischen, insbesondere solchen, die (Meth)acrylmonomere enthalten |
JP2017051892A (ja) * | 2015-09-08 | 2017-03-16 | レール・リキード−ソシエテ・アノニム・プール・レテュード・エ・レクスプロワタシオン・デ・プロセデ・ジョルジュ・クロード | 気液混合装置および気液混合方法 |
CN110372486B (zh) * | 2019-08-16 | 2021-03-30 | 中国科学院过程工程研究所 | 一种抑制管道聚合反应的阻聚剂添加装置 |
KR20210084901A (ko) * | 2019-12-30 | 2021-07-08 | 한화솔루션 주식회사 | 트레이형 증류장치 |
WO2023210075A1 (ja) * | 2022-04-27 | 2023-11-02 | 株式会社日本触媒 | 易重合性物質の取り扱い装置 |
CN115155093B (zh) * | 2022-08-09 | 2023-07-18 | 山东蓝湾新材料有限公司 | 一种丙烯酸二甲胺基乙酯生产用蒸馏塔 |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS506449B1 (de) * | 1969-06-24 | 1975-03-14 | ||
US4256675A (en) * | 1977-07-28 | 1981-03-17 | Celanese Corporation | Method for generating super atmospheric pressures of sensitive materials in a gas stream |
US4365081A (en) * | 1980-05-20 | 1982-12-21 | Nippon Shokubai Kagaku Kogyo Co. Ltd. | Process for producing 2-hydroxyalkyl acrylates or methacrylates |
US4369097A (en) | 1980-08-29 | 1983-01-18 | Asahi Kasei Kogyo Kabushiki Kaisha | Method and apparatus of distillation for readily polymerizable liquid |
US4614827A (en) * | 1983-07-20 | 1986-09-30 | Rohm Gmbh | Method for isolating vinyl salt compounds from aqueous solutions |
CA1316545C (en) * | 1987-06-27 | 1993-04-20 | Morimasa Kuragano | Quenching process of reaction product gas containing methacrylic acid and treatment method of quenched liquid |
DE3843843A1 (de) | 1988-12-24 | 1990-07-05 | Henkel Kgaa | Verfahren zur verbesserten herstellung von (meth)acrylsaeureestern mehrwertiger alkohole (iv) |
US5062927A (en) * | 1990-01-05 | 1991-11-05 | T And G Technologies, Inc. | Method of operating a still |
FR2727964B1 (fr) * | 1994-12-12 | 1997-01-24 | Atochem Elf Sa | Procede de recuperation des produits nobles legers contenus dans les residus de distillation des procedes de fabrication de l'acide acrylique et de ses esters |
DE19638093A1 (de) | 1996-09-18 | 1998-03-19 | Basf Ag | Verfahren zur Vermeidung, Entfernung oder Verminderung von Ablagerungen an Apparateteilen bei der Veresterung von Acryl- oder Methacrylsäure |
JPH10212249A (ja) * | 1997-01-31 | 1998-08-11 | Nippon Shokubai Co Ltd | 易重合性有機化合物の精製方法および精製装置 |
JPH11226301A (ja) | 1998-02-20 | 1999-08-24 | Nippon Shokubai Co Ltd | 蒸留方法及び蒸留装置 |
-
2000
- 2000-04-12 JP JP2000111308A patent/JP3787261B2/ja not_active Expired - Lifetime
- 2000-04-13 ZA ZA200001882A patent/ZA200001882B/xx unknown
- 2000-04-14 DE DE60013197T patent/DE60013197T2/de not_active Expired - Lifetime
- 2000-04-14 KR KR10-2000-0019458A patent/KR100423210B1/ko active IP Right Grant
- 2000-04-14 US US09/549,531 patent/US6409886B1/en not_active Expired - Lifetime
- 2000-04-14 CN CNB001056638A patent/CN1178893C/zh not_active Expired - Lifetime
- 2000-04-14 EP EP00107932A patent/EP1044957B1/de not_active Revoked
- 2000-04-14 MY MYPI20001604A patent/MY122586A/en unknown
- 2000-04-14 BR BR0001605-5A patent/BR0001605A/pt not_active Application Discontinuation
Also Published As
Publication number | Publication date |
---|---|
KR100423210B1 (ko) | 2004-03-19 |
MY122586A (en) | 2006-04-29 |
US6409886B1 (en) | 2002-06-25 |
ZA200001882B (en) | 2000-10-30 |
JP2000355570A (ja) | 2000-12-26 |
KR20010029642A (ko) | 2001-04-06 |
DE60013197T2 (de) | 2005-08-11 |
CN1178893C (zh) | 2004-12-08 |
EP1044957A1 (de) | 2000-10-18 |
JP3787261B2 (ja) | 2006-06-21 |
CN1270950A (zh) | 2000-10-25 |
EP1044957B1 (de) | 2004-08-25 |
BR0001605A (pt) | 2000-11-14 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8363 | Opposition against the patent |