DE3511687C2 - Verfahren und Vorrichtung zum Bestimmen von organischem Kohlenstoff in Wasser - Google Patents
Verfahren und Vorrichtung zum Bestimmen von organischem Kohlenstoff in WasserInfo
- Publication number
- DE3511687C2 DE3511687C2 DE19853511687 DE3511687A DE3511687C2 DE 3511687 C2 DE3511687 C2 DE 3511687C2 DE 19853511687 DE19853511687 DE 19853511687 DE 3511687 A DE3511687 A DE 3511687A DE 3511687 C2 DE3511687 C2 DE 3511687C2
- Authority
- DE
- Germany
- Prior art keywords
- water
- carrier gas
- carbon dioxide
- amount
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 93
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 24
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 24
- 238000000034 method Methods 0.000 title claims description 13
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 65
- 239000012159 carrier gas Substances 0.000 claims abstract description 38
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 30
- 239000000126 substance Substances 0.000 claims abstract description 24
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 22
- 230000003647 oxidation Effects 0.000 claims abstract description 18
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 18
- 239000000203 mixture Substances 0.000 claims description 24
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims description 17
- 239000001307 helium Substances 0.000 claims description 15
- 229910052734 helium Inorganic materials 0.000 claims description 15
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 14
- 239000012295 chemical reaction liquid Substances 0.000 claims description 14
- 239000003595 mist Substances 0.000 claims description 6
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 claims description 6
- 230000001590 oxidative effect Effects 0.000 abstract description 4
- 239000007789 gas Substances 0.000 description 13
- 238000006243 chemical reaction Methods 0.000 description 10
- 239000000243 solution Substances 0.000 description 10
- 239000007788 liquid Substances 0.000 description 8
- 238000005070 sampling Methods 0.000 description 6
- 238000000605 extraction Methods 0.000 description 5
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
- 238000009792 diffusion process Methods 0.000 description 4
- 238000002156 mixing Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 239000003463 adsorbent Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000011088 calibration curve Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- IWZKICVEHNUQTL-UHFFFAOYSA-M potassium hydrogen phthalate Chemical compound [K+].OC(=O)C1=CC=CC=C1C([O-])=O IWZKICVEHNUQTL-UHFFFAOYSA-M 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229910021642 ultra pure water Inorganic materials 0.000 description 1
- 239000012498 ultrapure water Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/18—Water
- G01N33/1826—Organic contamination in water
- G01N33/1846—Total carbon analysis
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/005—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods investigating the presence of an element by oxidation
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Molecular Biology (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6476984A JPS60207057A (ja) | 1984-03-30 | 1984-03-30 | 水中有機炭素の測定装置 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3511687A1 DE3511687A1 (de) | 1985-10-03 |
| DE3511687C2 true DE3511687C2 (de) | 1987-01-08 |
Family
ID=13267732
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19853511687 Expired DE3511687C2 (de) | 1984-03-30 | 1985-03-29 | Verfahren und Vorrichtung zum Bestimmen von organischem Kohlenstoff in Wasser |
Country Status (2)
| Country | Link |
|---|---|
| JP (1) | JPS60207057A (US20100268047A1-20101021-C00003.png) |
| DE (1) | DE3511687C2 (US20100268047A1-20101021-C00003.png) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01318955A (ja) * | 1988-06-20 | 1989-12-25 | Tokico Ltd | 炭素量測定装置 |
| JPH0291569A (ja) * | 1988-09-29 | 1990-03-30 | Japan Organo Co Ltd | 炭素量測定装置 |
| GB9203642D0 (en) * | 1992-02-19 | 1992-04-08 | Fluid Dynamics Sales Ltd | Carbon analyser |
| JP3265830B2 (ja) * | 1994-05-27 | 2002-03-18 | 株式会社島津製作所 | 全有機体炭素計 |
| US8181544B2 (en) * | 2008-11-18 | 2012-05-22 | Picarro, Inc. | Liquid sample evaporator for vapor analysis |
| KR102156150B1 (ko) * | 2018-12-28 | 2020-09-15 | (주)휴마스 | 비례제어 시료정밀주입방식과 이중냉각 기액분리를 이용한 연소산화 총유기탄소 측정방법 및 장치 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3854881A (en) * | 1971-09-13 | 1974-12-17 | A Cohen | Apparatus for determining organic carbon content of polluted liquids |
| JPS5236090A (en) * | 1975-09-17 | 1977-03-19 | Kawatetsu Keiryoki Kk | Method of measuring total organic carbon and total carbon in water |
-
1984
- 1984-03-30 JP JP6476984A patent/JPS60207057A/ja active Granted
-
1985
- 1985-03-29 DE DE19853511687 patent/DE3511687C2/de not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0532699B2 (US20100268047A1-20101021-C00003.png) | 1993-05-17 |
| DE3511687A1 (de) | 1985-10-03 |
| JPS60207057A (ja) | 1985-10-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OP8 | Request for examination as to paragraph 44 patent law | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8328 | Change in the person/name/address of the agent |
Free format text: STREHL, P., DIPL.-ING. DIPL.-WIRTSCH.-ING. SCHUEBEL-HOPF, U., DIPL.-CHEM. DR.RER.NAT., PAT.-ANWAELTE, 8000 MUENCHEN |
|
| 8339 | Ceased/non-payment of the annual fee |