DE3227001C1 - Verfahren zur Gewinnung von mit Phosphatidylcholin hochangereicherten ethanolischen Phosphatidfraktionen - Google Patents
Verfahren zur Gewinnung von mit Phosphatidylcholin hochangereicherten ethanolischen PhosphatidfraktionenInfo
- Publication number
- DE3227001C1 DE3227001C1 DE3227001A DE3227001A DE3227001C1 DE 3227001 C1 DE3227001 C1 DE 3227001C1 DE 3227001 A DE3227001 A DE 3227001A DE 3227001 A DE3227001 A DE 3227001A DE 3227001 C1 DE3227001 C1 DE 3227001C1
- Authority
- DE
- Germany
- Prior art keywords
- phosphatidylcholine
- phosphatide
- ethanolic
- highly enriched
- aluminum oxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- WTJKGGKOPKCXLL-RRHRGVEJSA-N phosphatidylcholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCCC=CCCCCCCCC WTJKGGKOPKCXLL-RRHRGVEJSA-N 0.000 title claims abstract description 11
- 238000000034 method Methods 0.000 title claims abstract description 10
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000000469 ethanolic extract Substances 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims abstract description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 239000007787 solid Substances 0.000 claims description 13
- 235000013311 vegetables Nutrition 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000010792 warming Methods 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 9
- JZNWSCPGTDBMEW-UHFFFAOYSA-N Glycerophosphorylethanolamin Natural products NCCOP(O)(=O)OCC(O)CO JZNWSCPGTDBMEW-UHFFFAOYSA-N 0.000 description 8
- 150000008104 phosphatidylethanolamines Chemical class 0.000 description 8
- 239000000203 mixture Substances 0.000 description 7
- RYCNUMLMNKHWPZ-SNVBAGLBSA-N 1-acetyl-sn-glycero-3-phosphocholine Chemical compound CC(=O)OC[C@@H](O)COP([O-])(=O)OCC[N+](C)(C)C RYCNUMLMNKHWPZ-SNVBAGLBSA-N 0.000 description 6
- 239000000284 extract Substances 0.000 description 6
- 239000000126 substance Substances 0.000 description 5
- 235000010469 Glycine max Nutrition 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- 239000011435 rock Substances 0.000 description 4
- 244000068988 Glycine max Species 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 229910052593 corundum Inorganic materials 0.000 description 3
- 229910001845 yogo sapphire Inorganic materials 0.000 description 3
- 238000000746 purification Methods 0.000 description 2
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 239000012675 alcoholic extract Substances 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 150000003905 phosphatidylinositols Chemical class 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
- C07F9/09—Esters of phosphoric acids
- C07F9/10—Phosphatides, e.g. lecithin
- C07F9/103—Extraction or purification by physical or chemical treatment of natural phosphatides; Preparation of compositions containing phosphatides of unknown structure
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J7/00—Phosphatide compositions for foodstuffs, e.g. lecithin
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Biochemistry (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Food Science & Technology (AREA)
- Saccharide Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicines Containing Plant Substances (AREA)
- Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
- Fats And Perfumes (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3227001A DE3227001C1 (de) | 1982-07-20 | 1982-07-20 | Verfahren zur Gewinnung von mit Phosphatidylcholin hochangereicherten ethanolischen Phosphatidfraktionen |
| DE8383106895T DE3363059D1 (en) | 1982-07-20 | 1983-07-14 | Process for winning phosphatide ethanolic fractions highly enriched with phosphatidyl choline |
| EP83106895A EP0100902B1 (de) | 1982-07-20 | 1983-07-14 | Verfahren zur Gewinnung von mit Phosphatidylcholin hochangereicherten ethanolischen Phosphatidfraktionen |
| AT83106895T ATE19182T1 (de) | 1982-07-20 | 1983-07-14 | Verfahren zur gewinnung von mit phosphatidylcholin hochangereicherten ethanolischen phosphatidfraktionen. |
| US06/514,003 US4528139A (en) | 1982-07-20 | 1983-07-15 | Process for obtaining ethanolic phosphatide fractions highly enriched with phosphatidylcholine |
| JP58130392A JPS5929694A (ja) | 1982-07-20 | 1983-07-19 | エタノ−ル性ホスフアチド画分を取得する方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3227001A DE3227001C1 (de) | 1982-07-20 | 1982-07-20 | Verfahren zur Gewinnung von mit Phosphatidylcholin hochangereicherten ethanolischen Phosphatidfraktionen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3227001C1 true DE3227001C1 (de) | 1983-07-07 |
Family
ID=6168796
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE3227001A Expired DE3227001C1 (de) | 1982-07-20 | 1982-07-20 | Verfahren zur Gewinnung von mit Phosphatidylcholin hochangereicherten ethanolischen Phosphatidfraktionen |
| DE8383106895T Expired DE3363059D1 (en) | 1982-07-20 | 1983-07-14 | Process for winning phosphatide ethanolic fractions highly enriched with phosphatidyl choline |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE8383106895T Expired DE3363059D1 (en) | 1982-07-20 | 1983-07-14 | Process for winning phosphatide ethanolic fractions highly enriched with phosphatidyl choline |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4528139A (enExample) |
| EP (1) | EP0100902B1 (enExample) |
| JP (1) | JPS5929694A (enExample) |
| AT (1) | ATE19182T1 (enExample) |
| DE (2) | DE3227001C1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19828799A1 (de) * | 1998-06-27 | 1999-12-30 | Meyer Lucas Gmbh & Co | Extraktion von Pflanzenlecithin |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5453523A (en) * | 1993-06-16 | 1995-09-26 | Emulsion Technology, Inc. | Process for obtaining highly purified phosphatidylcholine |
| US10561674B2 (en) | 2012-12-02 | 2020-02-18 | Lipogen Ltd. | Processes for the preparation of phospholipid-enriched dairy products as neutraceuticals for the formulation of functional foods |
| US10392410B2 (en) | 2014-12-05 | 2019-08-27 | Archer Daniels Midland Company | Processes for fractionating phospholipids |
| CN106632457B (zh) * | 2016-11-18 | 2018-04-03 | 福建花巷营养科技股份有限公司 | 一种通过破乳精制高纯度蛋黄卵磷脂的方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2945869A (en) * | 1956-04-30 | 1960-07-19 | Upjohn Co | Phosphatide emulsifying agent and process of preparing same |
| US3031478A (en) * | 1957-07-09 | 1962-04-24 | Nattermann A & Cie | Process for the production of natural phospholipids and substances produced thereby |
| DE2718797A1 (de) * | 1977-04-27 | 1978-11-02 | Nattermann A & Cie | Verfahren zur gewinnung von oelhaltigen hochgereinigten phosphatidylcholinen |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2724649A (en) * | 1951-03-23 | 1955-11-22 | Glidden Co | Margarine |
| US2727046A (en) * | 1951-12-17 | 1955-12-13 | Charles R Scholfield | Purification of phosphatides |
| FR1274363A (fr) * | 1956-04-30 | 1961-10-27 | Upjohn Co | Procédé de préparation d'un agent émulsionnant à base de phosphatides |
| DE1617679A1 (de) * | 1967-08-21 | 1971-03-18 | Nattermann A & Cie | Verfahren zur Gewinnung von hochgereinigtem Phosphatidylcholin |
| US3661946A (en) * | 1967-09-19 | 1972-05-09 | Lever Brothers Ltd | Phosphatide extraction |
| JPS5562010A (en) * | 1978-10-31 | 1980-05-10 | Ajinomoto Co Inc | Fat emulsion for intravenous injection |
| DE3047048A1 (de) * | 1980-12-13 | 1982-07-29 | A. Nattermann & Cie GmbH, 5000 Köln | Verfahren zur abtrennung von oel und/oder phosphatidylethanolamin aus diese enthaltenden alkoholloeslichen phosphatidylcholin-produkten |
-
1982
- 1982-07-20 DE DE3227001A patent/DE3227001C1/de not_active Expired
-
1983
- 1983-07-14 AT AT83106895T patent/ATE19182T1/de not_active IP Right Cessation
- 1983-07-14 DE DE8383106895T patent/DE3363059D1/de not_active Expired
- 1983-07-14 EP EP83106895A patent/EP0100902B1/de not_active Expired
- 1983-07-15 US US06/514,003 patent/US4528139A/en not_active Expired - Lifetime
- 1983-07-19 JP JP58130392A patent/JPS5929694A/ja active Granted
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2945869A (en) * | 1956-04-30 | 1960-07-19 | Upjohn Co | Phosphatide emulsifying agent and process of preparing same |
| US3031478A (en) * | 1957-07-09 | 1962-04-24 | Nattermann A & Cie | Process for the production of natural phospholipids and substances produced thereby |
| DE2718797A1 (de) * | 1977-04-27 | 1978-11-02 | Nattermann A & Cie | Verfahren zur gewinnung von oelhaltigen hochgereinigten phosphatidylcholinen |
Non-Patent Citations (7)
| Title |
|---|
| Encyclopedia a.a.o., Bd. 12, 1954, 356 * |
| Encyclopedia of Chemical Technology, Bd. 1, 1947, S. 224 * |
| I. Lipid Res., Bd. 3, 1962, S. 181-183 * |
| Int.Symp.Chromatogr., Bd. 5, 1986, S. 268-278 * |
| Lexikon d. Hilfsstoffe für Pharmazie, 1971, S. 43, 306 * |
| Physical Chemistry, 1979, S. 833-835 * |
| The Propertiers of Gases and Liquids, 3. Aufl., 1977, S. 587, 548 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19828799A1 (de) * | 1998-06-27 | 1999-12-30 | Meyer Lucas Gmbh & Co | Extraktion von Pflanzenlecithin |
Also Published As
| Publication number | Publication date |
|---|---|
| EP0100902A2 (de) | 1984-02-22 |
| US4528139A (en) | 1985-07-09 |
| EP0100902B1 (de) | 1986-04-16 |
| DE3363059D1 (en) | 1986-05-22 |
| ATE19182T1 (de) | 1986-05-15 |
| JPH0416477B2 (enExample) | 1992-03-24 |
| JPS5929694A (ja) | 1984-02-16 |
| EP0100902A3 (en) | 1984-05-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8100 | Publication of patent without earlier publication of application | ||
| D1 | Grant (no unexamined application published) patent law 81 | ||
| 8363 | Opposition against the patent | ||
| 8330 | Complete renunciation |