DE2906698C3 - Verfahren zur Gewinnung von Ethylenoxid, das von Aldehydverunreinigungen und Wasser praktisch frei ist - Google Patents

Verfahren zur Gewinnung von Ethylenoxid, das von Aldehydverunreinigungen und Wasser praktisch frei ist

Info

Publication number
DE2906698C3
DE2906698C3 DE2906698A DE2906698A DE2906698C3 DE 2906698 C3 DE2906698 C3 DE 2906698C3 DE 2906698 A DE2906698 A DE 2906698A DE 2906698 A DE2906698 A DE 2906698A DE 2906698 C3 DE2906698 C3 DE 2906698C3
Authority
DE
Germany
Prior art keywords
fractionation
liquid
withdrawn
ethylene oxide
distillation section
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE2906698A
Other languages
German (de)
English (en)
Other versions
DE2906698B2 (de
DE2906698A1 (de
Inventor
Brian John New York N.Y. Ozero
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Scientific Design Co Inc
Original Assignee
Halcon Research and Development Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Halcon Research and Development Corp filed Critical Halcon Research and Development Corp
Publication of DE2906698A1 publication Critical patent/DE2906698A1/de
Publication of DE2906698B2 publication Critical patent/DE2906698B2/de
Application granted granted Critical
Publication of DE2906698C3 publication Critical patent/DE2906698C3/de
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/32—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/38—Steam distillation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/20—Power plant

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Epoxy Compounds (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
DE2906698A 1978-02-21 1979-02-21 Verfahren zur Gewinnung von Ethylenoxid, das von Aldehydverunreinigungen und Wasser praktisch frei ist Expired DE2906698C3 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US05/879,544 US4134797A (en) 1978-02-21 1978-02-21 Process for recovery of ethylene oxide containing low levels of aldehydic impurities

Publications (3)

Publication Number Publication Date
DE2906698A1 DE2906698A1 (de) 1979-08-23
DE2906698B2 DE2906698B2 (de) 1981-02-19
DE2906698C3 true DE2906698C3 (de) 1982-03-18

Family

ID=25374362

Family Applications (1)

Application Number Title Priority Date Filing Date
DE2906698A Expired DE2906698C3 (de) 1978-02-21 1979-02-21 Verfahren zur Gewinnung von Ethylenoxid, das von Aldehydverunreinigungen und Wasser praktisch frei ist

Country Status (17)

Country Link
US (1) US4134797A (US06623731-20030923-C00052.png)
JP (1) JPS54132510A (US06623731-20030923-C00052.png)
KR (1) KR840002431B1 (US06623731-20030923-C00052.png)
AR (1) AR230992A1 (US06623731-20030923-C00052.png)
AU (1) AU523074B2 (US06623731-20030923-C00052.png)
BE (1) BE874308A (US06623731-20030923-C00052.png)
BR (1) BR7901039A (US06623731-20030923-C00052.png)
CA (1) CA1101877A (US06623731-20030923-C00052.png)
DE (1) DE2906698C3 (US06623731-20030923-C00052.png)
ES (1) ES477942A1 (US06623731-20030923-C00052.png)
FR (1) FR2417509A1 (US06623731-20030923-C00052.png)
GB (1) GB2015514B (US06623731-20030923-C00052.png)
IT (1) IT1117212B (US06623731-20030923-C00052.png)
MX (1) MX151397A (US06623731-20030923-C00052.png)
NL (1) NL176456C (US06623731-20030923-C00052.png)
NO (1) NO155008C (US06623731-20030923-C00052.png)
SE (1) SE448299B (US06623731-20030923-C00052.png)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2453166A1 (fr) * 1979-04-06 1980-10-31 Propylox Sa Procede pour l'epuration d'oxydes d'olefines
DE3038497C2 (de) * 1980-10-11 1983-11-10 Bayer Ag, 5090 Leverkusen Verfahren und Vorrichtung zur Trennung von ein Azeotrop bildenden Gemischen
FR2553771B1 (fr) * 1983-10-19 1986-01-17 Atochem Procede et dispositif pour concentrer des solutions aqueuses d'oxyde d'ethylene
FR2558069B1 (fr) * 1984-01-17 1986-04-25 Atochem Procede d'elimination de gaz dissous dans une solution aqueuse d'oxyde d'ethylene
US4778567A (en) * 1985-07-03 1988-10-18 Nippon Shokubai Kagaku Kogyo Co. Method for purification of ethylene oxide and recovery of heat thereof
JPS642549U (US06623731-20030923-C00052.png) * 1987-06-22 1989-01-09
FR2624859B1 (fr) * 1987-12-22 1991-03-22 Atochem Procede pour separer l'oxyde d'ethylene d'impuretes aldehydiques
DE3811524A1 (de) * 1988-04-06 1989-10-19 Solvay Werke Gmbh Verfahren und vorrichtung zur herstellung von reinst-epichlorhydrin
US5529667A (en) * 1994-12-01 1996-06-25 Hoechst Celanese Corporation Process for recovering ethylene oxide
DE19542829A1 (de) * 1995-11-17 1997-05-22 Basf Ag Verfahren zur Destillation von Ethylenoxid
DE19703627A1 (de) 1997-01-31 1998-08-06 Basf Ag Verfahren zur Ehtylenoxid-Reindestillation
US6306263B1 (en) * 1999-03-31 2001-10-23 Arco Chemical Technology, L.P. Impurities separation by distillation
FR2833951A1 (fr) * 2001-12-21 2003-06-27 Bp Chemicals Snc Procede de fabrication et de recuperation d'oxyde d'ethylene
WO2005032687A2 (en) * 2003-09-30 2005-04-14 Clark Arthur F Method for separating volatile components by dilutive distillation
US7404834B2 (en) * 2005-02-11 2008-07-29 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Lenbachplatz 6 Ethylene oxide plant operation
TWI402093B (zh) * 2005-05-10 2013-07-21 Shell Int Research 環氧乙烷之製備
EP2154521B1 (en) * 2007-04-17 2012-08-22 ARKRAY, Inc. Method and apparatus for measuring substrate concentration
WO2009094103A1 (en) 2008-01-25 2009-07-30 Dow Technology Investments Llc Reflux condenser
US7569710B1 (en) 2008-02-23 2009-08-04 Brian Ozero Ethylene oxide recovery process
US8845863B2 (en) * 2008-07-31 2014-09-30 Dow Technology Investments Llc Alkylene oxide purification processes and systems
BR112016012516B1 (pt) * 2013-12-06 2021-03-09 Shell Internationale Research Maatschappij B.V. métodos para separar impurezas de óxido de propileno impuro e para produzir óxido de propileno
US10035782B2 (en) 2014-10-01 2018-07-31 Shell Oil Company Relating to ethylene oxide recovery
EP3801803A4 (en) * 2018-06-04 2022-03-16 Brian Ozero PROCESS FOR RECOVERING ETHYLENE OXIDE
US11608305B2 (en) 2019-09-16 2023-03-21 Petron Scientech, Inc. Ethylene oxide purification
US20220289702A1 (en) * 2021-03-11 2022-09-15 Scientific Design Company, Inc. Epoxidation process with increased cycle water absorption

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2615901A (en) * 1949-05-11 1952-10-28 Jefferson Chem Co Inc Process of producing ethylene oxide substantially free of acetaldehyde
US3398062A (en) * 1965-02-10 1968-08-20 Lummus Co Olefin oxide purification by fractional distillation followed by side stream stripping
US3418338A (en) * 1966-02-28 1968-12-24 Halcon International Inc Water extractive distillation of an ethylene oxide stream containing formaldehyde
US3531376A (en) * 1968-12-23 1970-09-29 Mitsubishi Chem Ind Purification of acetone by extractive distillation and rectification with simultaneous alkali-containing acetone solution contact and halogen impurity side stream removal
US4008131A (en) * 1975-12-11 1977-02-15 Monsanto Company Purification of acetic acid

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
NICHTS-ERMITTELT

Also Published As

Publication number Publication date
JPS6251958B2 (US06623731-20030923-C00052.png) 1987-11-02
NO790572L (no) 1979-08-22
DE2906698B2 (de) 1981-02-19
KR830000537A (ko) 1983-04-16
IT7948072A0 (it) 1979-02-21
GB2015514B (en) 1982-08-04
FR2417509B1 (US06623731-20030923-C00052.png) 1982-10-22
AU4425479A (en) 1980-08-28
BR7901039A (pt) 1979-10-02
NO155008C (no) 1987-01-28
SE448299B (sv) 1987-02-09
GB2015514A (en) 1979-09-12
NL176456C (nl) 1985-04-16
AU523074B2 (en) 1982-07-08
DE2906698A1 (de) 1979-08-23
SE7901564L (sv) 1980-08-22
IT1117212B (it) 1986-02-17
KR840002431B1 (ko) 1984-12-27
NO155008B (no) 1986-10-20
ES477942A1 (es) 1980-04-01
NL7901073A (nl) 1979-08-23
JPS54132510A (en) 1979-10-15
FR2417509A1 (fr) 1979-09-14
CA1101877A (en) 1981-05-26
AR230992A1 (es) 1984-08-31
MX151397A (es) 1984-11-14
BE874308A (fr) 1979-08-20
US4134797A (en) 1979-01-16

Similar Documents

Publication Publication Date Title
DE2906698C3 (de) Verfahren zur Gewinnung von Ethylenoxid, das von Aldehydverunreinigungen und Wasser praktisch frei ist
EP0850923B1 (de) Verfahren zur Auftrennung des Produktgasgemisches der katalytischen Synthese von Methylmercaptan
DE2223541A1 (de) Verfahren zur reinigung von monocarbonsaeure-stroemen
DE2635935A1 (de) Verfahren zur reinigung von essigsaeure
DE19606877A1 (de) Verfahren zur Reinigung von Acrylsäure und Methacrylsäure
DE2449780B2 (de) Verfahren zum Abtrennen schwer- oder nichtfluchtiger Nebenprodukte der Propylen- und/oder Acroleinoxidation von den fur die Absorbtion der Acrylsäure aus den Reaktionsgasen verwendeten Losungsmitteln
DE69623543T2 (de) Verfahren zur Reinigung von einem Acrolein enthaltenden Gasstromes
WO2001089989A1 (de) Verfahren zur herstellung konzentrierter salpetersäure sowie anlage zur durchführung eines solchen verfahrens
DD146588A5 (de) Verfahren zur rueckgewinnung von acrylsaeure
DE3879142T2 (de) Verfahren zur abtrennung von aldehydischen verunreinigungen aus ethylenoxid.
DE1593357A1 (de) Verfahren zur Entfernung von Acrolein aus Acrylnitril
EP0962444B1 (de) Verfahren zur Aufarbeitung von rohem, flüssigem Vinylacetat
WO1998033785A1 (de) Verfahren zur ethylenoxid-reindestillation
DE19843697A1 (de) Verfahren zur Herstellung von hochreinem Monoethylenglykol
DE2343541A1 (de) Verfahren zum reinigen von methanol
DE2117978C2 (US06623731-20030923-C00052.png)
DE2045984C2 (de) Verfahren zur Entfernung von CO↓2↓ und/oder H↓2↓ S aus Gasgemischen
EP0072484B1 (de) Verfahren zur Aufarbeitung von rohem, flüssigem Vinylacetat
DE1520569C3 (de) Verfahren zur Gewinnung eines im wesentlichen von Waschlösung befreiten Polypropylens
DE3002660A1 (de) Verfahren zur gewinnung von methacrolein
EP0520316B1 (de) Verfahren zur selektiven H2S-Auswaschung
DE2855630C2 (de) Verfahren zur kontinuierlichen Abtrennung von Phthalsäureanhydrid aus den Reaktionsgasen der katalytischen Oxidation von o-Xylol und/oder Naphthalin
DE2838880C3 (de) Verfahren zur Gewinnung von Methacrolein
DE1668766C3 (de) Verfahren zur Abtrennung von Acrylsäure und Acrolein aus einem gasförmigen Propylenoxidationsprodukt
DE3726698C2 (de) Verfahren zum Reinigen von Trifluralin

Legal Events

Date Code Title Description
OAP Request for examination filed
OD Request for examination
C3 Grant after two publication steps (3rd publication)
8328 Change in the person/name/address of the agent

Free format text: SPOTT, G., DIPL.-CHEM. DR.RER.NAT., PAT.-ANW., 8000 MUENCHEN

8327 Change in the person/name/address of the patent owner

Owner name: SCIENTIFIC DESIGN CO., INC., HOUSTON, TEX., US

8328 Change in the person/name/address of the agent

Free format text: SPOTT, G., DIPL.-CHEM. DR.RER.NAT. PUSCHMANN, H., DIPL.-ING. (FH), PAT.-ANWAELTE, 8000 MUENCHEN

8328 Change in the person/name/address of the agent

Free format text: SPOTT, G., DIPL.-CHEM. DR.RER.NAT., PAT.-ANW., 8000 MUENCHEN

8328 Change in the person/name/address of the agent

Free format text: ZUMSTEIN, F., DIPL.-CHEM. DR.RER.NAT. KLINGSEISEN, F., DIPL.-ING., PAT.-ANWAELTE, 8000 MUENCHEN

8339 Ceased/non-payment of the annual fee