DE270663C - - Google Patents
Info
- Publication number
- DE270663C DE270663C DENDAT270663D DE270663DA DE270663C DE 270663 C DE270663 C DE 270663C DE NDAT270663 D DENDAT270663 D DE NDAT270663D DE 270663D A DE270663D A DE 270663DA DE 270663 C DE270663 C DE 270663C
- Authority
- DE
- Germany
- Prior art keywords
- xylidine
- diaminodi
- xylylmethane
- water
- formaldehyde
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- WSFSSNUMVMOOMR-UHFFFAOYSA-N formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 10
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical class Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- UACOVYUOWMWQPJ-UHFFFAOYSA-N NC(C1=C(C(=CC=C1)C)C)(C1=C(C(=CC=C1)C)C)N Chemical compound NC(C1=C(C(=CC=C1)C)C)(C1=C(C(=CC=C1)C)C)N UACOVYUOWMWQPJ-UHFFFAOYSA-N 0.000 claims description 4
- QAOWNCQODCNURD-UHFFFAOYSA-L sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 2
- 239000000203 mixture Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 239000002585 base Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000010446 mirabilite Substances 0.000 description 3
- RSIJVJUOQBWMIM-UHFFFAOYSA-L sodium sulfate decahydrate Chemical class O.O.O.O.O.O.O.O.O.O.[Na+].[Na+].[O-]S([O-])(=O)=O RSIJVJUOQBWMIM-UHFFFAOYSA-L 0.000 description 3
- VOWZNBNDMFLQGM-UHFFFAOYSA-N 2,5-Xylidine Chemical group CC1=CC=C(C)C(N)=C1 VOWZNBNDMFLQGM-UHFFFAOYSA-N 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 230000000875 corresponding Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 150000004992 toluidines Chemical class 0.000 description 2
- -1 Glauber's salt Sulphates Chemical class 0.000 description 1
- NMCUIPGRVMDVDB-UHFFFAOYSA-L Iron(II) chloride Chemical compound Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 description 1
- 230000001476 alcoholic Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 1
- 239000000987 azo dye Substances 0.000 description 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N benzene Substances C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE270663C true DE270663C (ja) |
Family
ID=527386
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT270663D Active DE270663C (ja) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE270663C (ja) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2818433A (en) * | 1955-09-19 | 1957-12-31 | Monsanto Chemicals | Process for making methylenedianilines |
| US2974168A (en) * | 1955-09-19 | 1961-03-07 | Monsanto Chemicals | Process for making methylenedianiline |
-
0
- DE DENDAT270663D patent/DE270663C/de active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2818433A (en) * | 1955-09-19 | 1957-12-31 | Monsanto Chemicals | Process for making methylenedianilines |
| US2974168A (en) * | 1955-09-19 | 1961-03-07 | Monsanto Chemicals | Process for making methylenedianiline |
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