DE2643251A1 - Verfahren zur herstellung von cyanurfluorid - Google Patents
Verfahren zur herstellung von cyanurfluoridInfo
- Publication number
- DE2643251A1 DE2643251A1 DE19762643251 DE2643251A DE2643251A1 DE 2643251 A1 DE2643251 A1 DE 2643251A1 DE 19762643251 DE19762643251 DE 19762643251 DE 2643251 A DE2643251 A DE 2643251A DE 2643251 A1 DE2643251 A1 DE 2643251A1
- Authority
- DE
- Germany
- Prior art keywords
- fluoride
- reaction
- cyanuric
- temperature
- cyanuric fluoride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000004519 manufacturing process Methods 0.000 title description 4
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 title 1
- VMKJWLXVLHBJNK-UHFFFAOYSA-N cyanuric fluoride Chemical compound FC1=NC(F)=NC(F)=N1 VMKJWLXVLHBJNK-UHFFFAOYSA-N 0.000 claims description 17
- 238000006243 chemical reaction Methods 0.000 claims description 14
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 9
- 239000003054 catalyst Substances 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 239000003701 inert diluent Substances 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 9
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 9
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 9
- 238000003682 fluorination reaction Methods 0.000 description 8
- 238000009835 boiling Methods 0.000 description 4
- 238000010992 reflux Methods 0.000 description 4
- FKEWHNNXQZSQFI-UHFFFAOYSA-N 4-chloro-5,6-difluorotriazine Chemical compound FC1=NN=NC(Cl)=C1F FKEWHNNXQZSQFI-UHFFFAOYSA-N 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000000375 suspending agent Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- HIMMCCJEMMCUJS-UHFFFAOYSA-N 4-fluorotriazine Chemical group FC1=CC=NN=N1 HIMMCCJEMMCUJS-UHFFFAOYSA-N 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- BGXXZJYFKBXPOU-UHFFFAOYSA-N chlorobenzene;nitrobenzene Chemical compound ClC1=CC=CC=C1.[O-][N+](=O)C1=CC=CC=C1 BGXXZJYFKBXPOU-UHFFFAOYSA-N 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000000985 reactive dye Substances 0.000 description 1
- 238000007614 solvation Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/28—Only halogen atoms, e.g. cyanuric chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Glass Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19762643251 DE2643251A1 (de) | 1976-09-25 | 1976-09-25 | Verfahren zur herstellung von cyanurfluorid |
| GB3932777A GB1532388A (en) | 1976-09-25 | 1977-09-21 | Process for the preparation of cyanuric fluoride |
| JP11346477A JPS5340790A (en) | 1976-09-25 | 1977-09-22 | Production of cyanuric acid phthalide |
| FR7728749A FR2365561A1 (fr) | 1976-09-25 | 1977-09-23 | Procede de preparation du fluorure de cyanuryle |
| BE181152A BE858995A (fr) | 1976-09-25 | 1977-09-23 | Procede de preparation de fluorure de cyanuryle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19762643251 DE2643251A1 (de) | 1976-09-25 | 1976-09-25 | Verfahren zur herstellung von cyanurfluorid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2643251A1 true DE2643251A1 (de) | 1978-03-30 |
Family
ID=5988851
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19762643251 Withdrawn DE2643251A1 (de) | 1976-09-25 | 1976-09-25 | Verfahren zur herstellung von cyanurfluorid |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JPS5340790A (enExample) |
| BE (1) | BE858995A (enExample) |
| DE (1) | DE2643251A1 (enExample) |
| FR (1) | FR2365561A1 (enExample) |
| GB (1) | GB1532388A (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0035704A1 (de) * | 1980-03-08 | 1981-09-16 | Bayer Ag | Verfahren zur Herstellung von 2,4,6-Trifluortriazin-(1,3,5) |
-
1976
- 1976-09-25 DE DE19762643251 patent/DE2643251A1/de not_active Withdrawn
-
1977
- 1977-09-21 GB GB3932777A patent/GB1532388A/en not_active Expired
- 1977-09-22 JP JP11346477A patent/JPS5340790A/ja active Pending
- 1977-09-23 FR FR7728749A patent/FR2365561A1/fr active Granted
- 1977-09-23 BE BE181152A patent/BE858995A/xx unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0035704A1 (de) * | 1980-03-08 | 1981-09-16 | Bayer Ag | Verfahren zur Herstellung von 2,4,6-Trifluortriazin-(1,3,5) |
Also Published As
| Publication number | Publication date |
|---|---|
| BE858995A (fr) | 1978-03-23 |
| FR2365561A1 (fr) | 1978-04-21 |
| GB1532388A (en) | 1978-11-15 |
| FR2365561B1 (enExample) | 1981-02-27 |
| JPS5340790A (en) | 1978-04-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8130 | Withdrawal |