DE2364803C3 - Verfahren zur Herstellung eines Schmelzoxidglases mit wenigstens einem der Oxide P↓2↓O↓5↓, GeO↓2↓, TeO↓2↓, Sb↓2↓O↓3↓ durch Flammhydrolyse - Google Patents
Verfahren zur Herstellung eines Schmelzoxidglases mit wenigstens einem der Oxide P↓2↓O↓5↓, GeO↓2↓, TeO↓2↓, Sb↓2↓O↓3↓ durch FlammhydrolyseInfo
- Publication number
- DE2364803C3 DE2364803C3 DE2364803A DE2364803A DE2364803C3 DE 2364803 C3 DE2364803 C3 DE 2364803C3 DE 2364803 A DE2364803 A DE 2364803A DE 2364803 A DE2364803 A DE 2364803A DE 2364803 C3 DE2364803 C3 DE 2364803C3
- Authority
- DE
- Germany
- Prior art keywords
- geo
- glass
- oxide
- sio
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 13
- 238000000034 method Methods 0.000 title claims description 11
- 230000007062 hydrolysis Effects 0.000 title claims description 7
- 238000006460 hydrolysis reaction Methods 0.000 title claims description 7
- 239000000075 oxide glass Substances 0.000 title claims description 6
- 239000011521 glass Substances 0.000 claims description 54
- 229910005793 GeO 2 Inorganic materials 0.000 claims description 42
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 33
- 239000002245 particle Substances 0.000 claims description 13
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 11
- YBMRDBCBODYGJE-UHFFFAOYSA-N germanium dioxide Chemical compound O=[Ge]=O YBMRDBCBODYGJE-UHFFFAOYSA-N 0.000 claims description 10
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 claims description 4
- 229910001413 alkali metal ion Inorganic materials 0.000 claims description 3
- 238000004031 devitrification Methods 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 239000005373 porous glass Substances 0.000 claims description 3
- 238000005245 sintering Methods 0.000 claims description 3
- 230000002542 deteriorative effect Effects 0.000 claims description 2
- 229910003069 TeO2 Inorganic materials 0.000 claims 1
- ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Inorganic materials O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- LAJZODKXOMJMPK-UHFFFAOYSA-N tellurium dioxide Chemical compound O=[Te]=O LAJZODKXOMJMPK-UHFFFAOYSA-N 0.000 claims 1
- YEAUATLBSVJFOY-UHFFFAOYSA-N tetraantimony hexaoxide Chemical compound O1[Sb](O2)O[Sb]3O[Sb]1O[Sb]2O3 YEAUATLBSVJFOY-UHFFFAOYSA-N 0.000 claims 1
- 239000000203 mixture Substances 0.000 description 18
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 10
- 238000007596 consolidation process Methods 0.000 description 9
- 239000005350 fused silica glass Substances 0.000 description 8
- 239000004071 soot Substances 0.000 description 8
- 239000007789 gas Substances 0.000 description 7
- 229910052760 oxygen Inorganic materials 0.000 description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 6
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 6
- 239000001301 oxygen Substances 0.000 description 6
- 239000012159 carrier gas Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 229910003902 SiCl 4 Inorganic materials 0.000 description 4
- 230000002349 favourable effect Effects 0.000 description 4
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- 229910052787 antimony Inorganic materials 0.000 description 3
- 238000013459 approach Methods 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000003345 natural gas Substances 0.000 description 3
- 235000012239 silicon dioxide Nutrition 0.000 description 3
- 239000005049 silicon tetrachloride Substances 0.000 description 3
- IEXRMSFAVATTJX-UHFFFAOYSA-N tetrachlorogermane Chemical compound Cl[Ge](Cl)(Cl)Cl IEXRMSFAVATTJX-UHFFFAOYSA-N 0.000 description 3
- 229910004028 SiCU Inorganic materials 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 150000001805 chlorine compounds Chemical group 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 239000001307 helium Substances 0.000 description 2
- 229910052734 helium Inorganic materials 0.000 description 2
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 2
- 230000003993 interaction Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004606 Fillers/Extenders Substances 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- LCKIEQZJEYYRIY-UHFFFAOYSA-N Titanium ion Chemical compound [Ti+4] LCKIEQZJEYYRIY-UHFFFAOYSA-N 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 239000006105 batch ingredient Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052681 coesite Inorganic materials 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- -1 germanium chloride-antimony chloride Chemical compound 0.000 description 1
- 239000003365 glass fiber Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052863 mullite Inorganic materials 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 229910052682 stishovite Inorganic materials 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
- 238000004017 vitrification Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/062—Glass compositions containing silica with less than 40% silica by weight
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/097—Glass compositions containing silica with 40% to 90% silica, by weight containing phosphorus, niobium or tantalum
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/12—Silica-free oxide glass compositions
- C03C3/16—Silica-free oxide glass compositions containing phosphorus
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/12—Silica-free oxide glass compositions
- C03C3/16—Silica-free oxide glass compositions containing phosphorus
- C03C3/21—Silica-free oxide glass compositions containing phosphorus containing titanium, zirconium, vanadium, tungsten or molybdenum
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/12—Silica-free oxide glass compositions
- C03C3/253—Silica-free oxide glass compositions containing germanium
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Glass Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US32110973A | 1973-01-04 | 1973-01-04 | |
| US05/675,959 US4042404A (en) | 1973-01-04 | 1976-04-12 | Fused P2 O5 type glasses |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2364803A1 DE2364803A1 (de) | 1974-07-11 |
| DE2364803B2 DE2364803B2 (de) | 1979-01-04 |
| DE2364803C3 true DE2364803C3 (de) | 1986-10-23 |
Family
ID=26982820
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2364803A Expired DE2364803C3 (de) | 1973-01-04 | 1973-12-27 | Verfahren zur Herstellung eines Schmelzoxidglases mit wenigstens einem der Oxide P↓2↓O↓5↓, GeO↓2↓, TeO↓2↓, Sb↓2↓O↓3↓ durch Flammhydrolyse |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4042404A (enExample) |
| CA (1) | CA967173A (enExample) |
| DE (1) | DE2364803C3 (enExample) |
| FR (1) | FR2213243B1 (enExample) |
| GB (1) | GB1415141A (enExample) |
| NL (1) | NL7400069A (enExample) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3884550A (en) * | 1973-01-04 | 1975-05-20 | Corning Glass Works | Germania containing optical waveguide |
| DE2746418B2 (de) * | 1976-11-02 | 1980-05-22 | Fujitsu Ltd., Kawasaki, Kanagawa (Japan) | seiner Herstellung, aus ihm hergestellte optische Übertraglingsleitungen sowie Verfahren zum Herstellen einer optischen Übertragungsleitung |
| JPS5927728B2 (ja) * | 1977-08-11 | 1984-07-07 | 日本電信電話株式会社 | 煤状ガラスロッドの製造方法 |
| US4358181A (en) * | 1977-09-29 | 1982-11-09 | Corning Glass Works | Gradient index optical waveguide and method of making |
| GB2071644B (en) * | 1980-02-22 | 1984-03-14 | Sumitomo Electric Industries | Radiation resistant optical fibres and a process for the production thereof |
| US4298365A (en) * | 1980-07-03 | 1981-11-03 | Corning Glass Works | Method of making a soot preform compositional profile |
| US4363647A (en) * | 1981-05-14 | 1982-12-14 | Corning Glass Works | Method of making fused silica-containing material |
| GB8334014D0 (en) * | 1983-12-21 | 1984-02-01 | Gen Electric Co Plc | Optical fibre preforms |
| US5043002A (en) | 1990-08-16 | 1991-08-27 | Corning Incorporated | Method of making fused silica by decomposing siloxanes |
| US20020186942A1 (en) * | 2001-05-01 | 2002-12-12 | Bubnov Mikhail M. | Low-loss highly phosphorus-doped fibers for Raman amplification |
| US7421174B2 (en) * | 2006-08-28 | 2008-09-02 | Furakawa Electric North America; Inc. | Multi-wavelength, multimode optical fibers |
| GB0921451D0 (en) | 2009-12-08 | 2010-01-20 | Univ St Andrews | Membrane |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2268589A (en) * | 1934-07-07 | 1942-01-06 | Heany Ind Ceramic Corp | Method of producing vitreous silica articles |
| US2272342A (en) * | 1934-08-27 | 1942-02-10 | Corning Glass Works | Method of making a transparent article of silica |
| US2863782A (en) * | 1955-07-22 | 1958-12-09 | Minnesota Mining & Mfg | Low-melting high-expansion glass |
| FR1357696A (fr) * | 1963-02-25 | 1964-04-10 | Verre optique | |
| US3423324A (en) * | 1964-11-20 | 1969-01-21 | Owens Illinois Inc | Apparatus and method for producing silica and other oxides |
| DE1496561B2 (de) * | 1965-02-15 | 1972-09-21 | Ir-durchlaessiges, tellur-glas | |
| DE1596881B2 (de) * | 1966-12-31 | 1971-08-05 | Ernst Leitz Gmbh, 6330 Wetzlar | Infrarotdurchlaessiges optisches glas mit sehr hohen brechzahlen im infrarot spektralbereich und extrem opti scher lage im sichtbaren spektralbereich und verfahren zu seiner herstellung |
| US3542572A (en) * | 1968-06-24 | 1970-11-24 | Corning Glass Works | Germania-silica glasses |
| US3644607A (en) * | 1969-12-18 | 1972-02-22 | Texas Instruments Inc | Use of vapor phase deposition to make fused silica articles having titanium dioxide in the surface layer |
| US3711262A (en) * | 1970-05-11 | 1973-01-16 | Corning Glass Works | Method of producing optical waveguide fibers |
| US3849344A (en) * | 1972-03-31 | 1974-11-19 | Carborundum Co | Solid diffusion sources containing phosphorus and silicon |
-
1973
- 1973-08-28 CA CA179,855A patent/CA967173A/en not_active Expired
- 1973-12-27 DE DE2364803A patent/DE2364803C3/de not_active Expired
-
1974
- 1974-01-03 NL NL7400069A patent/NL7400069A/xx not_active Application Discontinuation
- 1974-01-03 FR FR7400175A patent/FR2213243B1/fr not_active Expired
- 1974-01-04 GB GB45474A patent/GB1415141A/en not_active Expired
-
1976
- 1976-04-12 US US05/675,959 patent/US4042404A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE2364803A1 (de) | 1974-07-11 |
| GB1415141A (en) | 1975-11-26 |
| CA967173A (en) | 1975-05-06 |
| FR2213243B1 (enExample) | 1977-09-09 |
| US4042404A (en) | 1977-08-16 |
| DE2364803B2 (de) | 1979-01-04 |
| NL7400069A (enExample) | 1974-07-08 |
| FR2213243A1 (enExample) | 1974-08-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8281 | Inventor (new situation) |
Free format text: SCHULTZ, PETER CHARLES, PAINTED POST, N.Y., US |
|
| C3 | Grant after two publication steps (3rd publication) |