DE2363064C3 - Verfahren zur Kohleverflüssigung durch Hydrierung von Kohle - Google Patents
Verfahren zur Kohleverflüssigung durch Hydrierung von KohleInfo
- Publication number
- DE2363064C3 DE2363064C3 DE2363064A DE2363064A DE2363064C3 DE 2363064 C3 DE2363064 C3 DE 2363064C3 DE 2363064 A DE2363064 A DE 2363064A DE 2363064 A DE2363064 A DE 2363064A DE 2363064 C3 DE2363064 C3 DE 2363064C3
- Authority
- DE
- Germany
- Prior art keywords
- coal
- product
- liquid
- coal liquefaction
- liquefaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003245 coal Substances 0.000 title claims description 111
- 238000000034 method Methods 0.000 title claims description 15
- 239000007788 liquid Substances 0.000 claims description 39
- 239000002904 solvent Substances 0.000 claims description 27
- 239000002198 insoluble material Substances 0.000 claims description 25
- 239000003575 carbonaceous material Substances 0.000 claims description 9
- 238000005984 hydrogenation reaction Methods 0.000 claims description 7
- 239000000047 product Substances 0.000 description 63
- 239000002956 ash Substances 0.000 description 45
- 238000009835 boiling Methods 0.000 description 29
- 238000000926 separation method Methods 0.000 description 21
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 18
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 18
- 229910052739 hydrogen Inorganic materials 0.000 description 18
- 239000001257 hydrogen Substances 0.000 description 18
- 238000004821 distillation Methods 0.000 description 15
- 229910052799 carbon Inorganic materials 0.000 description 13
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 12
- 239000000463 material Substances 0.000 description 12
- 239000003054 catalyst Substances 0.000 description 10
- 238000012512 characterization method Methods 0.000 description 9
- 239000003350 kerosene Substances 0.000 description 9
- 230000003197 catalytic effect Effects 0.000 description 8
- 239000003610 charcoal Substances 0.000 description 8
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 7
- 230000005484 gravity Effects 0.000 description 7
- 229930195733 hydrocarbon Natural products 0.000 description 7
- 150000002430 hydrocarbons Chemical class 0.000 description 7
- 239000000203 mixture Substances 0.000 description 7
- 238000011084 recovery Methods 0.000 description 7
- 239000011280 coal tar Substances 0.000 description 6
- 239000007858 starting material Substances 0.000 description 6
- 229910052717 sulfur Inorganic materials 0.000 description 6
- 239000011593 sulfur Substances 0.000 description 6
- 239000002802 bituminous coal Substances 0.000 description 5
- 239000003921 oil Substances 0.000 description 5
- 239000004215 Carbon black (E152) Substances 0.000 description 4
- KYYSIVCCYWZZLR-UHFFFAOYSA-N cobalt(2+);dioxido(dioxo)molybdenum Chemical compound [Co+2].[O-][Mo]([O-])(=O)=O KYYSIVCCYWZZLR-UHFFFAOYSA-N 0.000 description 4
- 239000012530 fluid Substances 0.000 description 4
- 239000000446 fuel Substances 0.000 description 4
- 150000002790 naphthalenes Chemical class 0.000 description 4
- 239000004033 plastic Substances 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- CXWXQJXEFPUFDZ-UHFFFAOYSA-N tetralin Chemical compound C1=CC=C2CCCCC2=C1 CXWXQJXEFPUFDZ-UHFFFAOYSA-N 0.000 description 4
- 125000004432 carbon atom Chemical group C* 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 230000001276 controlling effect Effects 0.000 description 3
- 239000010779 crude oil Substances 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical group CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- NNBZCPXTIHJBJL-UHFFFAOYSA-N decalin Chemical compound C1CCCC2CCCCC21 NNBZCPXTIHJBJL-UHFFFAOYSA-N 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- NLPVCCRZRNXTLT-UHFFFAOYSA-N dioxido(dioxo)molybdenum;nickel(2+) Chemical compound [Ni+2].[O-][Mo]([O-])(=O)=O NLPVCCRZRNXTLT-UHFFFAOYSA-N 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- DCAYPVUWAIABOU-UHFFFAOYSA-N hexadecane Chemical compound CCCCCCCCCCCCCCCC DCAYPVUWAIABOU-UHFFFAOYSA-N 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000012263 liquid product Substances 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- IIYFAKIEWZDVMP-UHFFFAOYSA-N tridecane Chemical compound CCCCCCCCCCCCC IIYFAKIEWZDVMP-UHFFFAOYSA-N 0.000 description 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- 235000002918 Fraxinus excelsior Nutrition 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000010883 coal ash Substances 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- KWKXNDCHNDYVRT-UHFFFAOYSA-N dodecylbenzene Chemical compound CCCCCCCCCCCCC1=CC=CC=C1 KWKXNDCHNDYVRT-UHFFFAOYSA-N 0.000 description 1
- 239000000386 donor Substances 0.000 description 1
- 239000012632 extractable Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000003502 gasoline Substances 0.000 description 1
- -1 generally bituminous Substances 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 239000000852 hydrogen donor Substances 0.000 description 1
- 239000003077 lignite Substances 0.000 description 1
- XOROUWAJDBBCRC-UHFFFAOYSA-N nickel;sulfanylidenetungsten Chemical compound [Ni].[W]=S XOROUWAJDBBCRC-UHFFFAOYSA-N 0.000 description 1
- 229940078552 o-xylene Drugs 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000003476 subbituminous coal Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 210000003462 vein Anatomy 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/06—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by destructive hydrogenation
- C10G1/065—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by destructive hydrogenation in the presence of a solvent
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/08—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal with moving catalysts
- C10G1/083—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal with moving catalysts in the presence of a solvent
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US00319637A US3852183A (en) | 1972-12-29 | 1972-12-29 | Coal liquefaction |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2363064A1 DE2363064A1 (de) | 1974-07-11 |
| DE2363064B2 DE2363064B2 (de) | 1977-09-15 |
| DE2363064C3 true DE2363064C3 (de) | 1982-01-07 |
Family
ID=23243092
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2363064A Expired DE2363064C3 (de) | 1972-12-29 | 1973-12-19 | Verfahren zur Kohleverflüssigung durch Hydrierung von Kohle |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US3852183A (en:Method) |
| JP (1) | JPS5443521B2 (en:Method) |
| AU (1) | AU469866B2 (en:Method) |
| BE (1) | BE808762A (en:Method) |
| CA (1) | CA1005383A (en:Method) |
| DE (1) | DE2363064C3 (en:Method) |
| FR (1) | FR2212414B1 (en:Method) |
| IT (1) | IT1009079B (en:Method) |
| LU (1) | LU69021A1 (en:Method) |
| NL (1) | NL174954C (en:Method) |
| ZA (1) | ZA739262B (en:Method) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3974073A (en) * | 1974-09-06 | 1976-08-10 | The Lummus Company | Coal liquefaction |
| US3932266A (en) * | 1973-12-12 | 1976-01-13 | The Lummus Company | Synthetic crude from coal |
| US3954595A (en) * | 1974-03-18 | 1976-05-04 | The Lummus Company | Coal liquefaction |
| US3947346A (en) * | 1974-09-20 | 1976-03-30 | The Lummus Company | Coal liquefaction |
| JPS5155301A (en) * | 1974-11-11 | 1976-05-15 | Nissho Iwai Co Ltd | Hinenketsutan mataha jakunenketsutanyorinenketsutanoseizosuru hoho |
| US3997425A (en) * | 1974-12-26 | 1976-12-14 | Universal Oil Products Company | Process for the liquefaction of coal |
| US4028219A (en) * | 1975-10-23 | 1977-06-07 | Kerr-Mcgee Corporation | Process for the production of deashed coal liquifaction products |
| US4075080A (en) * | 1976-02-18 | 1978-02-21 | Continental Oil Company | Coal liquefaction process with removal of agglomerated insolubles |
| US4090958A (en) * | 1976-02-23 | 1978-05-23 | Kerr-Mcgee Corporation | Coal processing system for producing a stream of flowable insoluble coal products |
| US4029567A (en) * | 1976-04-20 | 1977-06-14 | Canadian Patents And Development Limited | Solids recovery from coal liquefaction slurry |
| ZA773075B (en) * | 1976-06-01 | 1978-04-26 | Kerr Mc Gee Chem Corp | An improved separation technique in a coal deashing process |
| US4070267A (en) * | 1976-06-01 | 1978-01-24 | Kerr-Mcgee Corporation | Coal processing system for reducing the amount of insoluble coal products in a light fraction stream |
| US4090957A (en) * | 1976-06-01 | 1978-05-23 | Kerr-Mcgee Corporation | System for separating soluble and insoluble coal products from a feed mixture |
| US4070268A (en) * | 1976-06-01 | 1978-01-24 | Kerr-Mcgee Corporation | Solvent recovery in a coal deashing process |
| US4119524A (en) * | 1976-06-01 | 1978-10-10 | Kerr-Mcgee Corporation | Coal deashing process having improved solvent recovery techniques |
| DE2654635B2 (de) * | 1976-12-02 | 1979-07-12 | Ludwig Dr. 6703 Limburgerhof Raichle | Verfahren zur kontinuierlichen Herstellung von Kohlenwasserstoffölen aus Kohle durch spaltende Druckhydrierung |
| US4391699A (en) * | 1976-12-27 | 1983-07-05 | Chevron Research Company | Coal liquefaction process |
| US4162956A (en) * | 1978-03-20 | 1979-07-31 | Kerr-Mcgee Corporation | Coal deashing process having improved solvent recovery techniques |
| US4162958A (en) * | 1978-03-20 | 1979-07-31 | Kerr-Mcgee Corporation | Process for the discharge of ash concentrate from a coal deashing system |
| US4242102A (en) * | 1978-12-15 | 1980-12-30 | The Lummus Company | Production of gasified products from ash containing bitumen produced in coal liquefaction |
| US4410414A (en) * | 1980-01-18 | 1983-10-18 | Hybrid Energy Systems, Inc. | Method for hydroconversion of solid carbonaceous materials |
| US4338183A (en) * | 1980-10-14 | 1982-07-06 | Uop Inc. | Method of solvent extraction of coal by a heavy oil |
| ZA822056B (en) * | 1981-08-05 | 1983-02-23 | Lummus Co | Coal liquefaction |
| US4428820A (en) | 1981-12-14 | 1984-01-31 | Chevron Research Company | Coal liquefaction process with controlled recycle of ethyl acetate-insolubles |
| US4510037A (en) * | 1983-12-23 | 1985-04-09 | Hri, Inc. | Hydrogenation process for solid carbonaceous feed materials using thermal countercurrent flow reaction zone |
| JPH0819418B2 (ja) * | 1990-10-24 | 1996-02-28 | 日本褐炭液化株式会社 | 石炭の液化方法 |
| US8021259B2 (en) * | 2008-01-04 | 2011-09-20 | American Axle & Manufacturing, Inc. | Differential assembly with oil deflector shield |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US361746A (en) * | 1887-04-26 | Paper-bag machine | ||
| US2987465A (en) * | 1958-06-20 | 1961-06-06 | Hydrocarbon Research Inc | Gas-liquid contacting process |
| US3184401A (en) * | 1962-01-19 | 1965-05-18 | Consolidation Coal Co | Process for producing hydrogenenriched hydrocarbonaceous products from coal |
| US3617465A (en) * | 1969-11-20 | 1971-11-02 | Hydrocarbon Research Inc | Coal hydrogenation |
| US3660267A (en) * | 1970-10-14 | 1972-05-02 | Atlantic Richfield Co | Coal processing |
-
1972
- 1972-12-29 US US00319637A patent/US3852183A/en not_active Expired - Lifetime
-
1973
- 1973-12-05 ZA ZA739262A patent/ZA739262B/xx unknown
- 1973-12-14 AU AU63640/73A patent/AU469866B2/en not_active Expired
- 1973-12-17 FR FR7345043A patent/FR2212414B1/fr not_active Expired
- 1973-12-18 BE BE138979A patent/BE808762A/xx not_active IP Right Cessation
- 1973-12-18 LU LU69021A patent/LU69021A1/xx unknown
- 1973-12-19 DE DE2363064A patent/DE2363064C3/de not_active Expired
- 1973-12-28 CA CA189,107A patent/CA1005383A/en not_active Expired
- 1973-12-28 NL NLAANVRAGE7317800,A patent/NL174954C/xx not_active IP Right Cessation
- 1973-12-28 IT IT70903/73A patent/IT1009079B/it active
- 1973-12-28 JP JP744611A patent/JPS5443521B2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5443521B2 (en:Method) | 1979-12-20 |
| IT1009079B (it) | 1976-12-10 |
| AU469866B2 (en) | 1976-02-26 |
| NL174954C (nl) | 1984-09-03 |
| NL174954B (nl) | 1984-04-02 |
| DE2363064B2 (de) | 1977-09-15 |
| DE2363064A1 (de) | 1974-07-11 |
| ZA739262B (en) | 1974-10-30 |
| FR2212414A1 (en:Method) | 1974-07-26 |
| AU6364073A (en) | 1975-06-19 |
| CA1005383A (en) | 1977-02-15 |
| JPS4999604A (en:Method) | 1974-09-20 |
| NL7317800A (en:Method) | 1974-07-02 |
| FR2212414B1 (en:Method) | 1978-03-03 |
| BE808762A (fr) | 1974-04-16 |
| LU69021A1 (en:Method) | 1974-02-22 |
| US3852183A (en) | 1974-12-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |