DE203145C - - Google Patents
Info
- Publication number
- DE203145C DE203145C DENDAT203145D DE203145DA DE203145C DE 203145 C DE203145 C DE 203145C DE NDAT203145 D DENDAT203145 D DE NDAT203145D DE 203145D A DE203145D A DE 203145DA DE 203145 C DE203145 C DE 203145C
- Authority
- DE
- Germany
- Prior art keywords
- soluble
- blue
- red
- acid
- insoluble
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- WQGWDDDVZFFDIG-UHFFFAOYSA-N Pyrogallol Chemical compound OC1=CC=CC(O)=C1O WQGWDDDVZFFDIG-UHFFFAOYSA-N 0.000 claims description 16
- 229940079877 Pyrogallol Drugs 0.000 claims description 8
- LSNNMFCWUKXFEE-UHFFFAOYSA-N sulfonic acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 claims description 6
- 238000009833 condensation Methods 0.000 claims description 5
- 230000005494 condensation Effects 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 239000011780 sodium chloride Substances 0.000 claims description 2
- 239000003085 diluting agent Substances 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 239000000975 dye Substances 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 210000002268 Wool Anatomy 0.000 description 6
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 6
- LNTHITQWFMADLM-UHFFFAOYSA-N Gallic acid Chemical compound OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 5
- 239000002253 acid Substances 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- UCMYJOPIPDLTRT-UHFFFAOYSA-N N,N-diethyl-2-nitrosoaniline Chemical compound CCN(CC)C1=CC=CC=C1N=O UCMYJOPIPDLTRT-UHFFFAOYSA-N 0.000 description 4
- 238000004043 dyeing Methods 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- VMHLLURERBWHNL-UHFFFAOYSA-M sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 3
- 239000001632 sodium acetate Substances 0.000 description 3
- 235000017281 sodium acetate Nutrition 0.000 description 3
- 239000001187 sodium carbonate Substances 0.000 description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 description 3
- 229940074391 Gallic acid Drugs 0.000 description 2
- LGDPTPLJZGPOJL-UHFFFAOYSA-N N,N-dimethyl-2-nitrosoaniline Chemical compound CN(C)C1=CC=CC=C1N=O LGDPTPLJZGPOJL-UHFFFAOYSA-N 0.000 description 2
- UBUCNCOMADRQHX-UHFFFAOYSA-N N-Nitrosodiphenylamine Chemical compound C=1C=CC=CC=1N(N=O)C1=CC=CC=C1 UBUCNCOMADRQHX-UHFFFAOYSA-N 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M NaHCO3 Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- 240000000358 Viola adunca Species 0.000 description 2
- 235000005811 Viola adunca Nutrition 0.000 description 2
- 235000013487 Viola odorata Nutrition 0.000 description 2
- 235000002254 Viola papilionacea Nutrition 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 235000004515 gallic acid Nutrition 0.000 description 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 2
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 2
- BCHZICNRHXRCHY-UHFFFAOYSA-N 2H-oxazine Chemical compound N1OC=CC=C1 BCHZICNRHXRCHY-UHFFFAOYSA-N 0.000 description 1
- HLVGXGQCLASQJU-UHFFFAOYSA-N 3,4,5-trihydroxy-N-phenylbenzamide Chemical compound OC1=C(O)C(O)=CC(C(=O)NC=2C=CC=CC=2)=C1 HLVGXGQCLASQJU-UHFFFAOYSA-N 0.000 description 1
- ANRHNWWPFJCPAZ-UHFFFAOYSA-M CHEMBL593252 Chemical compound [Cl-].C1=CC(N)=CC2=[S+]C3=CC(N)=CC=C3N=C21 ANRHNWWPFJCPAZ-UHFFFAOYSA-M 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- IYFLJHHTPTYWEE-UHFFFAOYSA-N ClO.N(=O)C1=C(N(C)C)C=CC=C1 Chemical compound ClO.N(=O)C1=C(N(C)C)C=CC=C1 IYFLJHHTPTYWEE-UHFFFAOYSA-N 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- NIKFYOSELWJIOF-UHFFFAOYSA-O Fuchsine Chemical compound Cl.C1=C(N)C(C)=CC(C(=C2C=CC(=[NH2+])C=C2)C=2C=CC(N)=CC=2)=C1 NIKFYOSELWJIOF-UHFFFAOYSA-O 0.000 description 1
- -1 Gallanilide sulfonic acids Chemical class 0.000 description 1
- XJKYOTQCYIFCFW-UHFFFAOYSA-N N(=O)CCC1=C(N(S(=O)(=O)O)CC2=CC=CC=C2)C=CC=C1 Chemical compound N(=O)CCC1=C(N(S(=O)(=O)O)CC2=CC=CC=C2)C=CC=C1 XJKYOTQCYIFCFW-UHFFFAOYSA-N 0.000 description 1
- NKLNCTMFAUIJRH-UHFFFAOYSA-N N(=O)CCNC=1C(=CC=CC1)C Chemical compound N(=O)CCNC=1C(=CC=CC1)C NKLNCTMFAUIJRH-UHFFFAOYSA-N 0.000 description 1
- DFUBSHNAHQZNRS-UHFFFAOYSA-N N(=O)CNC=1C(=CC=CC1)C Chemical compound N(=O)CNC=1C(=CC=CC1)C DFUBSHNAHQZNRS-UHFFFAOYSA-N 0.000 description 1
- IGGLGCKFQJPQPU-UHFFFAOYSA-N N(=O)NC1=CC=C(C=C1)CC Chemical compound N(=O)NC1=CC=C(C=C1)CC IGGLGCKFQJPQPU-UHFFFAOYSA-N 0.000 description 1
- XQBIUYUUHUNLGP-UHFFFAOYSA-N N-(4-methylphenyl)nitrous amide Chemical compound CC1=CC=C(NN=O)C=C1 XQBIUYUUHUNLGP-UHFFFAOYSA-N 0.000 description 1
- WXRXVZXYLBWKRG-UHFFFAOYSA-N N-ethyl-N-phenylnitrous amide Chemical compound CCN(N=O)C1=CC=CC=C1 WXRXVZXYLBWKRG-UHFFFAOYSA-N 0.000 description 1
- MWHUIOFIRPAVBJ-UHFFFAOYSA-N N-methyl-N-(2-methylphenyl)nitrous amide Chemical compound O=NN(C)C1=CC=CC=C1C MWHUIOFIRPAVBJ-UHFFFAOYSA-N 0.000 description 1
- MAXCWSIJKVASQC-UHFFFAOYSA-N N-methyl-N-phenylnitrous amide Chemical compound O=NN(C)C1=CC=CC=C1 MAXCWSIJKVASQC-UHFFFAOYSA-N 0.000 description 1
- 240000007651 Rubus glaucus Species 0.000 description 1
- 235000011034 Rubus glaucus Nutrition 0.000 description 1
- 235000009122 Rubus idaeus Nutrition 0.000 description 1
- 241000519995 Stachys sylvatica Species 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 150000002832 nitroso derivatives Chemical class 0.000 description 1
- 150000004893 oxazines Chemical class 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000002639 sodium chloride Nutrition 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000006277 sulfonation reaction Methods 0.000 description 1
- 150000003460 sulfonic acids Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B19/00—Oxazine dyes
- C09B19/005—Gallocyanine dyes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE203145C true DE203145C (fr) |
Family
ID=465580
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT203145D Active DE203145C (fr) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE203145C (fr) |
-
0
- DE DENDAT203145D patent/DE203145C/de active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE203145C (fr) | ||
| DE576076C (de) | Verfahren zur Herstellung von festen, fuer das Faerben von Acetylcellulose geeigneten Praeparaten von unloeslichen Farbstoffen | |
| DE2458580A1 (de) | Stabile konzentrierte loesungen sulfonsaeuregruppenhaltiger farbstoffe, verfahren zu ihrer herstellung und ihre verwendung | |
| DE746839C (de) | Verfahren zur Herstellung von metallhaltigen Farbstoffgemischen | |
| DE294447C (fr) | ||
| DE87935C (fr) | ||
| DE579633C (de) | Verfahren zur Herstellung von Kondensationsprodukten der Anthrachinonreihe | |
| DE172464C (fr) | ||
| DE589566C (de) | Verfahren zur Darstellung von gelben Beizenfarbstoffen | |
| DE736931C (de) | Verfahren zur Herstellung wasserloeslicher Ester schwer- bis unloeslicher oxalkylgruppenhaltiger Farbstoffe | |
| DE196752C (fr) | ||
| DE148792C (fr) | ||
| DE77120C (de) | Verfahren zur Darstellung von blauen beizenfärbenden Oxazinfarbstoffe^ | |
| DE731425C (de) | Verfahren zur Herstellung von wasserloeslichen Anthrachinonfarbstoffen | |
| DE646301C (de) | Verfahren zur Darstellung von Beizenfarbstoffen | |
| DE179020C (fr) | ||
| DE86222C (fr) | ||
| DE117587C (fr) | ||
| DE657628C (de) | Herstellung von Farbstoffen | |
| DE246337C (fr) | ||
| DE116765C (fr) | ||
| DE58415C (de) | Verfahren zur Darstellung secundärer Disazofarbstoffe für Druck und Färberei aus der Amidophtalsäure | |
| DE49139C (de) | Neuerung in dem Verfahren zur Darstellung von gelb- bis braunrothen, im alkalischen Bade färbenden Azofarbstoffen aus Chrysoidin. | |
| DE1769078C (de) | In Wasser schwerlöslicher Rhodaminfarbstoff und dessen Verwendung | |
| DE80434C (fr) |